IP Library Granted Patent US 11,794,177
Granted Patent B2
US 11,794,177 · App. 16/988,236 · Granted Oct 24, 2023

Surface-modified light upconversion silica particles

Inventors: Jason T. Wertz (Pleasant Valley, NY); Brandon M. Kobilka (Fishkill, NY); Sarah K. Czaplewski-Campbell (Rochester, MN); Eric J. Campbell (Rochester, MN)
Assignee: International Business Machines Corporation
B01J31/183B01J21/08B01J31/0271B01J31/1815B01J35/004B01J35/0006B01J37/0217B01J37/0221B01J37/0228B01J2231/005B01J2531/008B01J2531/824B01J2531/828
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Quick Facts
Patent No.
US 11,794,177
App. No.
16/988,236
Granted
Oct 24, 2023
Kind
B2
Abstract

A composition, method, and article of manufacture are disclosed. The composition includes a silica particle with light upconversion molecules bound to its surface. The method includes obtaining silica particles and light upconversion molecules having sidechains with reactive functional groups. The method further includes binding the light upconversion molecules to surfaces of the silica particles. The article of manufacture includes the composition.

Claims (30)

1. A composition, comprising:

a silica particle; and

light upconversion molecules bound to a surface of the silica particle.

2. The composition of claim 1 , wherein the light upconversion molecules comprise molecular sensitizers.

3. The composition of claim 1 , wherein the light upconversion molecules comprise molecular annihilators.

4. The composition of claim 1 , wherein the light upconversion molecules comprise molecular annihilators and molecular sensitizers.

5. The composition of claim 1 , wherein the surface of the silica particle includes a first face and a second face.

6. The composition of claim 5 , wherein the light upconversion molecules comprise molecular sensitizers bound to the first face of the silica particle.

7. The composition of claim 6 , wherein the light upconversion molecules comprise molecular annihilators bound to the second face of the silica particle.

8. A method of forming surface-modified particles, comprising:

obtaining silica particles;

obtaining light upconversion molecules having sidechains with reactive functional groups; and

binding the light upconversion molecules to surfaces of the silica particles.

9. The method of claim 8 , wherein the reactive functional groups are silyl groups.

10. The method of claim 8 , further comprising forming a reaction environment, the reaction environment comprising:

the surface-modified particles;

a photocatalyst; and

a substrate.

11. The method of claim 8 , wherein the silica particles are Janus particles.

12. The method of claim 8 , wherein the light upconversion molecules comprise a molecular sensitizer and a molecular annihilator.

13. The method of claim 12 , wherein the molecular sensitizer is a platinum complex of a porphyrin or a palladium complex of a phthalocyanine.

14. The method of claim 12 , wherein the molecular annihilator is a furanyldiketopyrrolopyrrole or a perylene.

15. An article of manufacture, comprising:

a silica particle; and

light upconversion molecules bound to a surface of the silica particle.

16. The article of manufacture of claim 15 , wherein the light upconversion molecules comprise a molecular sensitizer.

17. The article of manufacture of claim 16 , wherein the molecular sensitizer is a platinum complex of a porphyrin or a palladium complex of a phthalocyanine.

18. The article of manufacture of claim 15 , wherein the light upconversion molecules comprise a molecular annihilator.

19. The article of manufacture of claim 18 , wherein the molecular annihilator is a furanyldiketopyrrolopyrrole or a perylene.

20. The article of manufacture of claim 15 , further comprising a photocatalyst.

Assignments (5)
RELEASE OF SECURITY INTEREST Recorded Aug 2, 2022
From: IMPERIAL FINANCIAL SERVICES B.V.
To: SEVEN BRIDGES GENOMICS INC.
Reel/Frame 061055/0078 →
RELEASE OF SECURITY INTEREST Recorded May 24, 2022
From: IMPERIAL FINANCIAL SERVICES B.V.
To: SEVEN BRIDGES GENOMICS INC.
Reel/Frame 060173/0792 →
SECURITY INTEREST Recorded May 24, 2022
From: SEVEN BRIDGES GENOMICS INC.
To: IMPERIAL FINANCIAL SERVICES B.V.
Reel/Frame 060173/0803 →
SECURITY INTEREST Recorded Mar 30, 2022
From: SEVEN BRIDGES GENOMICS INC.
To: IMPERIAL FINANCIAL SERVICES B.V.
Reel/Frame 059554/0165 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 7, 2020
From: WERTZ, JASON T.; KOBILKA, BRANDON M.; CZAPLEWSKI-CAMPBELL, SARAH K.; CAMPBELL, ERIC J.
To: INTERNATIONAL BUSINESS MACHINES CORPORATION
Reel/Frame 053436/0136 →
Continuity (1)
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