IP Library Granted Patent US 11,365,359
Granted Patent B2
US 11,365,359 · App. 17/023,605 · Granted Jun 21, 2022

Renewable hydrocarbon lighter fluid

Inventors: Ramin Abhari (Bixby, OK); H. Lynn Tomlinson (Leonard, OK); Nate Green (Ames, IA)
Assignee: REG Synthetic Fuels, LLC
C10G65/12C10L11/04C10G2300/1003C10G2300/1014C10G2300/1018C10G2300/202C10G2300/207C10G2300/304C10G2300/308C10L2200/0484C10L2230/06C10L2270/08
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Quick Facts
Patent No.
US 11,365,359
App. No.
17/023,605
Granted
Jun 21, 2022
Kind
B2
Abstract

The present technology relates to hydrocarbon fluids, and more particularly, a hydrocarbon lighter fluid derived from renewable sources. Specifically, renewable fatty acids/glycerides are converted to a charcoal lighter fluid with the same or better performance than a petroleum middle distillate derived charcoal lighter fluid.

Claims (11)

1. A method for producing a hydrocarbon lighter fluid comprising the steps of

(a) hydrotreating a renewable feedstock to produce a heavy hydrocarbon fraction comprising C 12 -C 24 hydrocarbons;

(b) hydrocracking the heavy hydrocarbon fraction to a C 3 -C 18 + hydrocarbon distribution; and

(c) fractionating the C 3 -C 18 + hydrocarbon distribution to recover a hydrocarbon lighter fluid

wherein the lighter fluid comprises a ratio of iso-paraffins to n-paraffins of about 0.9:1 to about 1.1:1 and at least 82 wt % C 9 -C 10 paraffins, has a cetane number greater than 60, provides an ash coverage of 90% or higher, and has total hydrocarbon emissions of 0.28 lb/start or less according to the South Coast Air Quality Management District Rule 1174 at a dosage level of 80 g/kg or less.

2. The method of claim 1 wherein the renewable feedstock is pretreated to remove phosphorus, silicon, and metal contaminants to less than 10 wppm total.

3. The method of claim 1 wherein the hydrotreating takes place in a reactor comprising a nickel-molybdenum catalyst, at a temperature from about 550 F to about 650 F, under 1,000 to 2,000 psig pressure, and a ratio of hydrogen to renewable feed between 4,000 to 12,000 SCF/bbl.

4. The method of claim 1 wherein the hydrocracking takes place in a reactor comprising a noble metal catalyst on a crystalline support at a temperature from about 580 F to about 750 F, and a ratio of hydrogen to heavy hydrocarbon between 1,000 to 15,000 SCF/bbl.

5. The method of claim 1 wherein the renewable feedstock comprises monoglycerides, diglycerides, triglycerides, free fatty acids, or combinations thereof.

6. The method of claim 5 wherein the renewable feedstock is selected from the group consisting of animal fats, animal oils, poultry fats, poultry oil, vegetable fats, vegetable oils, rendered fats, rendered oils, restaurant grease, brown grease, yellow grease, waste industrial frying oils, fish oils, fish fats, algal oils, microbial oils, and combinations of any two or more thereof.

7. The method of claim 1 wherein the hydrocarbon lighter fluid has a carbon intensity of 30 gCO 2e /MJ or less according to California Air Resource Board CA-GREET3.0 model.

Assignments (3)
RELEASE OF SECURITY INTEREST Recorded Jul 1, 2022
From: UMB BANK, N.A., AS COLLATERAL TRUSTEE
To: REG SYNTHETIC FUELS, LLC; RENEWABLE ENERGY GROUP, INC.; REG SENECA, LLC; REG BIOFUELS, LLC
Reel/Frame 060562/0428 →
PATENT SECURITY AGREEMENT Recorded Jun 19, 2021
From: REG SYNTHETIC FUELS, LLC
To: UMB BANK, N.A., AS COLLATERAL TRUSTEE
Reel/Frame 056628/0673 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 17, 2020
From: ABHARI, RAMIN; TOMLINSON, H. LYNN; GREEN, NATE
To: REG SYNTHETIC FUELS, LLC
Reel/Frame 053801/0899 →
Continuity (2)
Provisional Application 62903388 · Sep 20, 2019
Related Publication 20210087480A1 · Mar 25, 2021