IP Library Granted Patent US 11,819,789
Granted Patent B2
US 11,819,789 · App. 17/039,527 · Granted Nov 21, 2023

Stable filter media including nanofibers

Inventors: Abdoulaye Doucouré (Roanoke, VA); Randall B. Keisler (Clifton Park, NY)
Assignee: Hollingsworth & Vose Company
B01D39/1623B01D39/2017B01D39/2065B01D2239/0421B01D2239/0428B01D2239/065B01D2239/0622B01D2239/0631B01D2239/1216B01D2239/1233B01D2239/1291C02F1/44
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Quick Facts
Patent No.
US 11,819,789
App. No.
17/039,527
Granted
Nov 21, 2023
Kind
B2
Abstract

Filter media comprising nanofibers and related components, systems, and methods associated therewith are provided. In some embodiments, a filter media may comprise a first fiber web and a second fiber web designed to impart beneficial properties to the filter media. For instance, in some embodiments, the first fiber web may provide high particulate efficiency and the second fiber web may provide suitable capacity. In some embodiments, the first and second fiber webs may have certain properties (e.g., water contact angle, surface energy) that are similar or substantially the same. The similarities between the first and second fiber webs may serve to enhance the structural stability of the filter media under various conditions (e.g., high temperature, high pressure, steam sterilization) and/or permeability to certain fluids (e.g., water). Filter media, as described herein, may be particularly well-suited for applications that involve liquid filtration.

Claims (24)

1. A filter media, comprising:

a first fiber web having an average fiber diameter of less than or equal to about 0.5 microns; and

a second fiber web having a maximum pore size of greater than or equal to about 3 microns and less than or equal to about 70 microns;

wherein a critical wetting surface tension of the first fiber web and a critical wetting surface tension of the second fiber web differ by less than or equal to about 15 dynes/cm;

wherein the second fiber web comprises meltblown fibers; and

wherein the first fiber web has a surface area of greater than or equal to about 5 m 2 /g and a water contact angle of greater than 90 degrees.

2. The filter media of claim 1 , wherein the first fiber web has a surface area of greater than or equal to about 10 m 2 /g.

3. The filter media of claim 1 , wherein a water contact angle of the second fiber web and the water contact angle of the first fiber web differ by less than or equal to about 20 degrees.

4. The filter media of claim 1 , wherein the filter media is steam sterilized.

5. The filter media of claim 4 , wherein the filter media has a water bubble point after steam sterilization of greater than or equal to about 70 psi and less than or equal to about 120 psi.

6. The filter media of claim 1 , wherein the second fiber web has a water contact angle of greater than 90 degrees.

7. The filter media of claim 1 , wherein the water contact angle of the second fiber web and the water contact angle of the first fiber web differ by greater than 0 degrees.

8. The filter media of claim 1 , wherein the first fiber web and the second fiber web are directly adjacent.

9. The filter media of claim 8 , wherein the first fiber web and the second fiber web have a peel strength of greater than or equal to about 0.01 lb/in and less than or equal to about 10 lb/in.

10. The filter media of claim 1 , wherein the first fiber web has a surface area of less than or equal to 350 m 2 /g.

11. The filter media of claim 2 , wherein the first fiber web has a surface area of less than or equal to 350 m 2 /g.

12. The filter media of claim 1 , wherein the first fiber web comprises polyethersulfone fibers.

13. The filter media of claim 1 , wherein the second fiber web comprises polyamide, polyvinylidene fluoride, and/or polybutylene terephthalate fibers.

14. The filter media of claim 4 , wherein a water bubble point of the filter media after steam sterilization is higher than a water bubble point of the filter media before steam sterilization.

15. The filter media of claim 4 , wherein a water bubble point of the filter media after steam sterilization is less than or equal to 50% higher than a water bubble point of the filter media before steam sterilization.

16. The filter media of claim 1 , wherein the filter media has a water permeability of greater than or equal to about 0.1 ml/min·cm 2 ·psi and less than or equal to about 10 ml/min·cm 2 ·psi.

17. The filter media of claim 1 , wherein the first fiber web comprises polyvinylidene fluoride fibers.

18. The filter media of claim 1 , wherein the water contact angle of the first fiber web is greater than or equal to 100 degrees.

19. The filter media of claim 1 , wherein the water contact angle of the first fiber web is greater than or equal to 110 degrees.

Assignments (2)
NOTICE OF GRANT OF SECURITY INTEREST IN PATENTS Recorded Jan 4, 2022
From: HOLLINGSWORTH & VOSE COMPANY
To: BANK OF AMERICA, N.A., AS COLLATERAL AGENT
Reel/Frame 058649/0109 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 22, 2020
From: DOUCOURÉ, ABDOULAYE; KEISLER, RANDALL B.
To: HOLLINGSWORTH & VOSE COMPANY
Reel/Frame 054724/0546 →
Continuity (2)
Continuation 14690345 · Apr 17, 2015
Related Publication 20210093989A1 · Apr 1, 2021