IP Library Granted Patent US 11,686,657
Granted Patent B1
US 11,686,657 · App. 17/076,189 · Granted Jun 27, 2023

Method for testing a proppant

Inventor: Matthew D. Bryant (Charlotte, NC)
Assignee: True Crush Testing, LLC
G01N3/12G01M3/00G01N15/0272G01N33/00
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Quick Facts
Patent No.
US 11,686,657
App. No.
17/076,189
Granted
Jun 27, 2023
Kind
B1
Abstract

In the specification and drawings a method for testing a proppant is described and shown that involves: obtaining a proppant sample; separating the proppant sample into a plurality of sub-samples according to grain size; subjecting each sub-sample to a pressure that is sufficient to crush at least a portion of the proppant within at least one of the plurality of sub-samples; and independently analyzing each sub-sample to determine at least one of: i) the amount of proppant that was crushed within each sub-sample; and ii) the amount of proppant that was not crushed within each sub-sample.

Claims (42)

1. A method of testing proppant comprising:

a. obtaining a plurality of pre-pressure subjected proppant samples;

b. measuring the amount of at least two of the pre-pressure subjected proppant samples to determine a pre-pressure subjected proppant sample value for each of the at least two pre-pressure subjected proppant samples;

c. subjecting each of the at least two pre-pressure subjected proppant samples to a pressure, resulting in a corresponding post-pressure subjected proppant sample for each of the at least two pre-pressure subjected proppant samples;

d. determining a post-pressure subjected proppant sample value for each of the at least two post-pressure subjected proppant samples by measuring at least one of:

i) the amount of proppant that experienced a change, if any, within each of the at least two post-pressure subjected proppant samples due to said subjecting the at least two pre-pressure subjected proppant samples to a pressure; and

ii) the amount of proppant that did not experience a change, if any, within each of the at least two post-pressure subjected proppant samples due to said subjecting the at least two pre-pressure subjected proppant samples to a pressure.

2. The method of claim 1 further comprising comparing each post-pressure subjected proppant sample value to each corresponding pre-pressure subjected proppant sample value.

3. The method of claim 2 further comprising reporting results of said comparing each post-pressure subjected proppant sample value to each corresponding pre-pressure subjected proppant sample value.

4. The method of claim 3 wherein said reporting results of said comparing each post-pressure subjected proppant sample value to each corresponding pre-pressure subjected proppant sample value comprises reporting results to a third party.

5. The method of claim 1 wherein said subjecting each of the at least two pre-pressure subjected proppant samples to a pressure further comprises subjecting each of the at least two pre-pressure subjected proppant samples to a pressure that is sufficient to crush at least a portion of the proppant within at least one of the at least two pre-pressure subjected proppant samples.

6. A method of testing proppant comprising:

a. obtaining a proppant sample;

b. separating the proppant sample into a plurality of sub-samples;

c. subjecting each sub-sample to a pressure;

d. independently analyzing each sub-sample; and

e. measuring at least one of:

i) the amount of proppant that experienced a change, if any, within each sub-sample due to said subjecting each sub-sample to a pressure; and

ii) the amount of proppant that did not experience a change, if any, within each sub-sample due to said subjecting each sub-sample to a pressure.

7. The method of claim 6 wherein said measuring at least one of:

i) the amount of proppant that experienced a change, if any, within each sub-sample due to said subjecting each sub-sample to a pressure; and

ii) the amount of proppant that did not experience a change, if any, within each sub-sample due to said subjecting each sub-sample to a pressure;

further comprises determining the amount of proppant that was crushed for each sub-sample.

8. The method of claim 6 further comprising determining a score for said proppant sample based on results of said measuring at least one of:

i) the amount of proppant that experienced a change, if any, within each sub-sample due to said subjecting each sub-sample to a pressure; and

ii) the amount of proppant that did not experience a change, if any, within each sub-sample due to said subjecting each sub-sample to a pressure.

9. The method of claim 8 wherein said determining a score for said proppant sample further comprises determining a weighted average of the amount of proppant that was crushed for each sub-sample.

10. The method of claim 9 further comprising reporting said score for said proppant sample.

11. The method of claim 10 wherein said reporting said score for said proppant sample comprises reporting said score for said proppant sample to a third party.

12. The method of claim 6 further comprising determining the amount of proppant that was crushed for each sub-sample during said subjecting each sub-sample to a pressure.

13. The method of claim 6 wherein said subjecting each sub-sample to a pressure comprises separately subjecting each sub-sample to a pressure.

14. The method of claim 6 wherein said subjecting each sub-sample to a pressure further comprises subjecting each sub-sample to a pressure that is sufficient to crush at least a portion of the proppant within at least one of the plurality of sub-samples.

15. The method of claim 6 wherein said subjecting each sub-sample to a pressure further comprises subjecting each sub-sample to a pressure of about 6,000 pounds per square inch.

16. A method of testing proppant comprising:

a. obtaining a proppant sample;

b. separating the proppant sample into a plurality of sub-samples;

c. subjecting each sub-sample to a pressure; and

d. independently analyzing each sub-sample to determine whether a change to the proppant occurred within each sub-sample.

17. The method of claim 16 further comprising reporting the results of said independently analyzing each sub-sample to determine whether a change to the proppant occurred within each sub-sample.

18. The method of claim 17 wherein said reporting the results comprises reporting the results to a third party.

19. The method of claim 16 wherein said separating the proppant sample into a plurality of sub-samples comprises sieving the proppant sample over a plurality of sieves, at least two of said plurality of sieves having a different mesh size.

20. The method of claim 16 wherein said subjecting each sub-sample to a pressure further comprises subjecting each sub-sample to a pressure of about 6,000 pounds per square inch.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 16, 2023
From: BRYANT, MATTHEW
To: TRUE CRUSH TESTING, LLC
Reel/Frame 062720/0023 →
Continuity (3)
Continuation 16358789 · Mar 20, 2019
Continuation 15625817 · Jun 16, 2017
Provisional Application 62351774 · Jun 17, 2016