ECAE materials for high strength aluminum alloys
Disclosed herein is a method of forming a high strength aluminum alloy. The method comprises heating an aluminum material to a solutionizing temperature for a solutionizing time such that the magnesium and zinc are dispersed throughout the extruded aluminum material to form a solutionized aluminum material. The method includes quenching the solutionized aluminum material to form a quenched aluminum material. The method also includes aging the quenched aluminum material to form an aluminum alloy, then subjecting the aluminum alloy to an ECAE process to form a high strength aluminum alloy.
1. A method of forming a high strength aluminum alloy, the method comprising:
heating an aluminum material containing magnesium, zinc and less than 0.5 wt. % copper to a solutionizing temperature such that the magnesium and zinc are dispersed throughout the aluminum material to form a solutionized aluminum material;
quenching the solutionized aluminum material to below about room temperature such that the magnesium and zinc remain dispersed throughout the solutionized aluminum material to form a quenched aluminum material;
aging the quenched aluminum material to form an aluminum alloy, wherein the aging step includes heating the quenched aluminum material to a temperature from about 88° C. to about 92° C. for from about seven hours to about nine hours followed by heating the aluminum alloy to a temperature from about 110° C. to about 120° C. for from about 35 hours to about 45 hours; and
subjecting the aluminum alloy to an equal channel angular extrusion (ECAE) process while maintaining the aluminum alloy at a temperature to produce a high strength aluminum alloy having a yield strength from about 400 MPa to about 650 MPa.
2. The method of claim 1 , wherein the heating step includes heating the aluminum material to a temperature from about 400° C. to about 550° C. for from about 3 hours to about 24 hours.
3. The method of claim 1 , wherein the aluminum material contains aluminum as a primary component, from about 0.5 wt. % to about 4.0 wt. % Magnesium and from about 2.0 wt. % to about 7.5 wt. % Zinc.
4. The method of claim 1 , wherein the high strength aluminum alloy has an average grain size from about 0.2 μm to about 0.8 μm.
5. The method of claim 1 , wherein the ECAE process includes at least two ECAE passes.
6. The method of claim 1 , further comprising subjecting the aluminum material to a first ECAE process before the heating step, wherein the aluminum material is maintained at a temperature from about 100° C. to about 400° C. during the ECAE process.
7. The method of claim 1 , wherein the high strength aluminum alloy has a grain size less than 1 micron in diameter.
8. A method of forming a high strength aluminum alloy, the method comprising:
subjecting an aluminum material containing magnesium, zinc and less than 0.5 wt. % copper to a first equal channel angular extrusion (ECAE) process, wherein the aluminum material is maintained at a temperature from about 100° C. to about 400° C. during the first ECAE process;
after the first ECAE process, heating the aluminum material to a solutionizing temperature such that the magnesium and zinc are dispersed throughout the aluminum material to form a solutionized aluminum material;
quenching the solutionized aluminum material to below about room temperature such that the magnesium and zinc remain dispersed throughout the solutionized aluminum material to form a quenched aluminum material; and
subjecting the quenched aluminum material to an additional ECAE process while maintaining the aluminum material at a temperature from about 20° C. to about 150° C. to produce a high strength aluminum alloy having a yield strength from about 400 MPA to about 650 MPa.
9. The method of claim 8 , wherein the heating step includes heating the aluminum material to a temperature from about 400° C. to about 550° C. for from about 3 hours to about 24 hours.
10. The method of claim 8 , wherein the aluminum material contains aluminum as a primary component, from about 0.5 wt. % to about 4.0 wt. % Magnesium and from about 2.0 wt. % to about 7.5 wt. % Zinc.
11. The method of claim 8 , further comprising aging the quenched aluminum material prior to the additional ECAE process, wherein the aging step includes heating the aluminum material to a temperature from about 80° C. to about 100° C. for from about one hour to about eight hours followed by heating the aluminum alloy to a temperature from about 110° C. to about 120° C. for from about 35 hours to about 45 hours.
12. The method of claim 8 , wherein the high strength aluminum alloy has an average grain size from about 0.2 μm to about 0.8 μm.
13. A method of forming a high strength aluminum alloy, the method comprising:
heating an aluminum material containing magnesium, zinc and less than 0.5 wt. % copper to a solutionizing temperature such that the magnesium and zinc are dispersed throughout the aluminum material to form a solutionized aluminum material;
quenching the solutionized aluminum material to below about room temperature such that the magnesium and zinc remain dispersed throughout the solutionized aluminum material to form a quenched aluminum material;
aging the quenched aluminum material to form an aluminum alloy, wherein the aging step includes heating the quenched aluminum material to a temperature from about 88° C. to about 92° C. for from about seven hours to about nine hours followed by heating the aluminum alloy to a temperature from about 110° C. to about 120° C. for from about 35 hours to about 45 hours; and
subjecting the aluminum alloy to an equal channel angular extrusion (ECAE) process while maintaining the aluminum material at a temperature from about 20° C. to about 150° C. to produce a high strength aluminum alloy having a yield strength from about 400 MPA to about 650 MPa.
14. The method of claim 13 , further comprising subjecting the aluminum material to an additional ECAE process before the heating step, wherein the aluminum material is maintained at a temperature from about 100° C. to about 400° C. during the additional ECAE process.
15. The method of claim 13 , wherein the aluminum material contains aluminum as a primary component, from about 0.5 wt. % to about 4.0 wt. % Magnesium and from about 2.0 wt. % to about 7.5 wt. % Zinc.
16. The method of claim 13 , wherein the high strength aluminum alloy has an average grain size from about 0.2 μm to about 0.8 μm.
17. The method of claim 13 , wherein the high strength aluminum alloy has a grain size less than 1 micron in diameter.
18. The method of claim 13 , wherein the ECAE process includes at least two ECAE passes.
19. The method of claim 13 , wherein the high strength aluminum alloy has a yield strength from about 420 MPa to about 500 MPa.
20. The method of claim 13 , wherein the high strength aluminum alloy has a yield strength from about 420 MPa to about 500 MPa.