IP Library Granted Patent US 11,458,427
Granted Patent B2
US 11,458,427 · App. 17/095,292 · Granted Oct 4, 2022

Fine fiber filter media and processes

Inventors: Stephen T. Cox (Nashua, NH); William S. Freeman (Roanoke, VA); Abdoulaye Doucouré (Roanoke, VA); John A. Wertz (Hollis, NH)
Assignee: Hollingsworth & Vose Company
B01D39/1623B32B5/022B32B5/26D04H3/16B01D2239/1216B01D2239/1233B01D2239/1258B01D2239/1266
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Quick Facts
Patent No.
US 11,458,427
App. No.
17/095,292
Granted
Oct 4, 2022
Kind
B2
Abstract

Fine fiber products including fiber webs, as well as related assemblies, systems and methods, are described. In some embodiments, fiber webs described herein may include fine fibers and relatively low amounts of degraded polymer formed during a fiber extrusion process. The fiber webs may be used for filter media applications.

Claims (27)

1. A filter media comprising:

a fiber web comprising a plurality of meltblown fibers having an average fiber diameter between about 0.1 microns and about 1.5 microns, wherein the fiber web has:

a mean pore size of greater than about 0.1 microns and less than about 5.0 microns;

a surface area of greater than or equal to about 1.5 m 2 /g;

a water permeability of greater than about 0.2 ml/min·cm 2 ·psi, wherein determining the water permeability comprises passing deionized water through the fiber web at a pressure of 20 psi until 1,000 ml of permeate has been collected;

a permeate turbidity of less than about 8 NTU, wherein determining the permeate turbidity comprises passing a dispersion of ISO 12103-1-A2 silica fine test dust in deionized water at a concentration of 1,500 ppm through the fiber web at a pressure of 30 psi until 50 ml of permeate is collected, and measuring turbidity of the collected permeate;

a basis weight between about 1 g/m 2 and about 200 g/m 2 ; and

a thickness between about 0.002 inches and about 0.02 inches,

wherein the fiber web has a bubble point between about 0.1 microns and about 30 microns, wherein the bubble point is measured according to the standard ASTM F-316-80 Method B, BS6410.

2. The filter media of claim 1 , wherein the fiber web has a consistency of basis weight across the fiber web of about 3.0 standard deviations or less.

3. The filter media of claim 1 , wherein the fiber web has a consistency of thickness across the fiber web of about 3.0 standard deviations or less.

4. The filter media of claim 1 , wherein the average fiber diameter of the plurality of meltblown fibers is less than about 1.0 microns.

5. The filter media of claim 1 , wherein the average fiber diameter of the plurality of meltblown fibers is less than about 0.6 microns.

6. The filter media of claim 1 , comprising a solidity of greater than or equal to about 10% and less than about 70%.

7. The filter media of claim 1 , comprising a solidity of greater than or equal to about 25% and less than about 55%.

8. The filter media of claim 1 , wherein the fiber web comprises a first layer and a second layer, wherein each of the first layer and second layers comprises the plurality of meltblown fibers having an average fiber diameter between about 0.1 microns and about 1.5 microns, and wherein the second layer has the same composition as the first layer.

9. The filter media of claim 1 , wherein the fiber web has an air permeability of greater than about 2 CFM and less than about 35 CFM.

10. The filter media of claim 1 , wherein the water permeability of the fiber web is greater than about 0.2 ml/min·cm 2 ·psi and less than about 4 ml/min·cm 2 ·psi.

11. The filter media of claim 1 , wherein the fiber web has an initial permeate flux greater than about 5 ml/min·cm 2 and less than about 200 ml/min·cm 2 .

12. The filter media of claim 1 , wherein the fiber web has an initial permeate flux greater than about 5 ml/min·cm 2 and less than about 60 ml/min·cm 2 .

13. The filter media of claim 1 , wherein the fiber web has a final permeate flux greater than about 1.5 ml/min·cm 2 and less than about 100 ml/min·cm 2 .

14. The filter media of claim 1 , wherein the fiber web has a final permeate flux greater than about 2 ml/min·cm 2 and less than about 30 ml/min·cm 2 .

15. The filter media of claim 1 , wherein the permeate turbidity of the fiber web is less than about 5 NTU.

16. The filter media of claim 1 , wherein the permeate turbidity of the fiber web is less than about 2.5 NTU.

17. The filter media of claim 1 , wherein the surface area of the fiber web is greater than about 2.0 m 2 /g and less than or equal to about 6 m 2 /g.

18. A filter element comprising the filter media of claim 1 .

19. A method comprising passing a liquid through the filter media of claim 1 .

Assignments (2)
NOTICE OF GRANT OF SECURITY INTEREST IN PATENTS Recorded Jan 4, 2022
From: HOLLINGSWORTH & VOSE COMPANY
To: BANK OF AMERICA, N.A., AS COLLATERAL AGENT
Reel/Frame 058649/0109 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 23, 2020
From: COX, STEPHEN T.; FREEMAN, WILLIAM S.; DOUCOURÉ, ABDOULAYE; WERTZ, JOHN A.
To: HOLLINGSWORTH & VOSE COMPANY
Reel/Frame 054736/0276 →
Continuity (5)
Continuation 16170350 · Oct 25, 2018
Continuation 13528796 · Jun 20, 2012
Continuation In Part 12971594 · Dec 17, 2010
Continuation In Part 12971539 · Dec 17, 2010
Related Publication 20210129061A1 · May 6, 2021