IP Library Granted Patent US 12,134,082
Granted Patent B2
US 12,134,082 · App. 17/142,416 · Granted Nov 5, 2024

Ultra-low surface charge biogenic silica filtration media

Inventor: George Asante-Nyamekye (Reno, NV)
Assignee: EP Minerals LLC
B01J20/14B01J20/041B01J20/28011B01J20/3078C02F1/281
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Quick Facts
Patent No.
US 12,134,082
App. No.
17/142,416
Granted
Nov 5, 2024
Kind
B2
Abstract

A diatomite filtration product includes flux-calcined diatomaceous earth, wherein the diatomite filtration product has: (1) an intricate and porous structure of diatomite, (2) a zeta potential in a range of from about −1.0 mV to about −6.0 mV within a pH range of from about 3.0 to about 8.0, and (3) a centrifuged wet density in a range of from about 0.176 g/ml to about 0.256 g/ml.

Claims (13)

1. A diatomite filtration product comprising flux- calcined diatomaceous earth, wherein the diatomite filtration product has:

(1) an intricate and porous structure of diatomite,

(2) a zeta potential in a range of from about −1.0 mV to about −6.0 mV within a pH range of from about 3.0 to about 8.0, and

(3) a centrifuged wet density in a range of from about 0.176 g/ml to about 0.256 g/ml,

wherein the filtration product is generated by preparing a blend by blending dried diatomaceous earth comprising a centrifuged wet density of not greater than 0.256 g/ml with about 6 weight percent to about 12 weight percent of a fluxing agent based on the total weight of the blend and thermally sintering the blend to form the flux-calcined diatomaceous earth,

wherein the blend comprises a stoichiometric ratio of fluxing agent to silicon dioxide of at least 5.0%, wherein water is introduced into the blend in an amount of 7-15 weight percent based on the total weight of the blend to form a dispersion of diatomaceous earth, water, and fluxing agent.

2. The filtration product of claim 1 having a permeability in a range of from about 450 millidarcys to about 20,000 millidarcys.

3. The filtration product of claim 1 , wherein the blend has a stoichiometric ratio of sodium oxide to silicon dioxide in a range of from about 5.0% to about 8.0%.

4. The filtration product of claim 1 , wherein the fluxing agent is selected from the group consisting of sodium oxide, sodium carbonate, and sodium bicarbonate.

5. The filtration product of claim 1 having USP extractable lead (Pb) of less than about 1 mg/kg of filtration product.

6. The filtration product of claim 1 having USP extractable arsenic (As) of less than about 1 mg/kg of filtration product.

7. The filtration product of claim 1 having USP extractable iron (Fe) of less than about 10 mg/kg filtration product.

8. The filtration product of claim 1 , wherein the dried diatomaceous earth comprises a centrifuged wet density in the range from about 0.144 g/ml to about 0.240 g/ml.

Assignments (2)
NOTICE OF GRANT OF SECURITY INTEREST IN INTELLECTUAL PROPERTY (FIRST LIEN) Recorded Jul 31, 2024
From: EP MINERALS, LLC
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 068312/0958 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 6, 2021
From: ASANTE-NYAMEKYE, GEORGE
To: EP MINERALS LLC
Reel/Frame 054825/0174 →
Continuity (1)
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