IP Library Granted Patent US 12,509,611
Granted Patent B2
US 12,509,611 · App. 17/152,986 · Granted Dec 30, 2025

Anaerobically curable compositions containing alpha-methylene-lactones

Inventors: Adrian Brandt (Essen, DE); Horst Beck (Neuss, DE); Andreas Taden (Düsseldorf, DE); Ralph Nemitz (Juechen, DE); Alexander Kux (Monheim, DE); Nigel Sweeney (Dublin, IE); David Birkett (Kildare, IE); Brendan Kneafsey (Dublin, IE); James A. Houlihan (Dublin, IE); Michael Doherty (Kildare, IE)
Assignee: Henkel AG & Co. KGaA
C09J4/00C08F220/286C08F222/102C09J4/06C09J133/14
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Quick Facts
Patent No.
US 12,509,611
App. No.
17/152,986
Granted
Dec 30, 2025
Kind
B2
Abstract

The present invention relates to anaerobically curable compositions made from renewable materials. In particular, an alpha-methylene-lactone is used with a (meth)acrylate component and a cure system to form an anaerobically curable composition.

Claims (10)

1 . An anaerobically curable composition comprising:

polyethylene glycol dimethacrylate;

α-methylene-γ-valerolactone; and

an anaerobic cure system comprising saccharin, 1,4-napthoquinone, and N,N-diethyl-p-toluidine,

wherein:

the polyethylene glycol dimethacrylate is present in an amount of from 20 to 50 percent by weight, based on the total weight of the anaerobically curable composition,

the α-methylene-γ-valerolactone is present in an amount of from 5 to 50 percent by weight, based on the total weight of the anaerobically curable composition, and

the anaerobic cure system is present in an amount of from 0.2 to 2 percent by weight, based on the total weight of the anaerobically curable composition.

2 . The composition of claim 1 , wherein the α-methylene-γ-valerolactone is present in an amount of about 30 percent by weight, based on the total weight of the anaerobically curable composition.

3 . The composition of claim 1 , wherein the composition further comprises ethylene-diamine tetra acetic acid, present in an amount of from about 0.001 to about 0.1 percent by weight, based on the total weight of the anaerobically curable composition.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 19, 2023
From: BRANDT, ADRIAN; BECK, HORST; TADEN, ANDREAS; NEMITZ, RALPH; KUX, ALEXANDER
To: HENKEL AG & CO. KGAA
Reel/Frame 062417/0932 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 19, 2023
From: SWEENEY, NIGEL; BIRKETT, DAVID; KNEAFSEY, BRENDAN; HOULIHAN, JAMES A.; DOHERTY, MICHAEL
To: HENKEL IRELAND OPERATIONS AND RESEARCH LIMITED
Reel/Frame 062417/0990 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 19, 2023
From: HENKEL IRELAND OPERATIONS & RESEARCH LIMITED
To: HENKEL IP & HOLDING GMBH
Reel/Frame 062418/0157 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 22, 2022
From: HENKEL IP & HOLDING GMBH
To: HENKEL AG & CO. KGAA
Reel/Frame 059207/0627 →