DUAL PHASE CHANGE MATERIAL LIQUID SUSPENSION AND METHOD OF MAKING THE SAME
A dual PCM liquid suspension is formed by blending a liquid phase change material having a first phase change temperature, a microencapsulated phase change material having a second phase change temperature, a thickening agent, and a surfactant and heating the blended materials for a period of time to form a permanent liquid suspension. PCM liquid suspension behaves as a viscous liquid and may be filled in PCM bottles with conventional liquid filling equipment. The PCM liquid suspension may be preconditioned and stored at a single temperature.
1 . A phase change material comprising:
a first phase change material in liquid form having a first phase change temperature;
a second phase change material in microencapsulated form having a second phase change temperature;
a thickening agent; and
a surfactant,
wherein said first and second phase change materials, said thickening agent and said surfactant are blended in a homogenous mixture and heated for a period of time.
2 . The phase change material of claim 1 wherein said first phase change material is selected from the group consisting of: water-based PCMs; plant-based organic PCMs, paraffin based PCMs and salt hydrate based PCM's.
3 . The phase change material of claim 1 wherein said second PCM material comprises a plant-based organic PCM microencapsulated in an acrylic shell.
4 . The phase change material of claim 2 wherein said second PCM material comprises a plant-based organic PCM microencapsulated in an acrylic shell.
5 . The phase change material of claim 1 wherein said first phase change material has a phase change temperature of about 9.5° C.
6 . The phase change material of claim 1 wherein said second phase change material has a phase change temperature of about 37° C.
7 . The phase change material of claim 5 wherein said second phase change material has a phase change temperature of about 37° C.
8 . The phase change material of claim 2 wherein said liquid PCM comprises an organic ester.
9 . The phase change material of claim 4 wherein said liquid PCM comprises an organic ester.
10 . The phase change material of claim 1 wherein said surfactant is polysorbate 80.
11 . The phase change material of claim 4 wherein said surfactant is polysorbate 80.
12 . A method for making a dual phase change material liquid suspension comprising the steps of:
providing a first phase change material in liquid form having a first phase change temperature;
providing a second phase change material in microencapsulated form having a second phase change temperature;
providing a thickening agent;
providing a surfactant;
stirring the first phase change material;
adding the thickening agent to the first phase change material and stirring until evenly dispersed;
heating the first change material and thickening agent to a predetermined temperature while stirring;
adding the second phase change material while stirring and maintaining said temperature;
adding the surfactant while stirring and maintaining said temperature; and
cooling to ambient temperature.
13 . The method of claim 12 wherein the predetermined temperature is about 60° C.
14 . The method of claim 12 wherein said surfactant is polysorbate 80.
15 . The method of claim 13 wherein said surfactant is polysorbate 80.
16 . A method for making a dual phase change material liquid suspension comprising the steps of:
providing a first phase change material in liquid form having a first phase change temperature;
providing a second phase change material in microencapsulated form having a second phase change temperature;
providing a thickening agent;
providing a surfactant;
stirring the first phase change material;
adding the thickening agent to the first phase change material and stirring until evenly dispersed;
adding the surfactant and stirring until evenly dispersed;
adding the second phase change material and stirring until evenly dispersed;
heating the dispersed materials to predetermined temperature while stirring;
maintaining said temperature while stirring for a period of time and cooling to ambient temperature.
17 . The method of claim 16 wherein the predetermined temperature is about 60° C.
18 . The method of claim 16 wherein said surfactant is polysorbate 80.
19 . The method of claim 17 wherein said surfactant is polysorbate 80.