IP Library Granted Patent US 11,920,081
Granted Patent B2
US 11,920,081 · App. 17/190,690 · Granted Mar 5, 2024

Modified acid compositions as alternatives to conventional acids in the oil and gas industry

Inventors: Clay Purdy (Medicine Hat, CA); Markus Weissenberger (Calgary, CA)
Assignee: DORF KETAL CHEMICALS FZE
C09K8/52A23C21/00A23J1/00A23J1/202B01D15/203B01J49/50B01J49/60B08B3/08B09C1/08C02F1/50C02F1/66C04B41/009C04B41/5315C04B41/5353C04B41/72C05B11/04C05B15/00C05B17/00C05C11/00C05D9/00C05G3/80C05G5/23C09K8/54C09K8/72C09K13/06C09K17/40C09K17/42C09K17/48C11D3/30C11D7/08C11D7/3218C23F11/04C23F11/142E21B37/06C02F5/125C09K2208/32
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Quick Facts
Patent No.
US 11,920,081
App. No.
17/190,690
Granted
Mar 5, 2024
Kind
B2
Abstract

An aqueous modified acid composition for industrial activities, said composition comprising: an alkanolamine and strong acid in a molar ratio of not less than 1:15, preferably not less than 1:10; it can also further comprise a metal iodide or iodate. Said composition demonstrates advantages over known conventional acids and modified acids.

Claims (30)

1. A method of use of a modified acid composition comprising:

providing an aqueous modified acid composition comprising a mineral acid and an alkanolamine in a molar ratio ranging from 3:1 to not more than 15:1 and having a pH of less than 1;

contacting a surface of the aqueous modified acid composition;

allowing the aqueous modified acid composition to act upon said surface;

removing the acid composition when an exposure time has been determined to be sufficient for the operation to be complete or sufficiently complete; and

wherein said method of use includes at least one of etching concrete or cleaning concrete from equipment and buildings.

2. The method according to claim 1 , wherein the mineral acid is selected from the group consisting of: HCl, nitric acid, sulfuric acid, sulfonic acid, phosphoric acid, and combinations thereof.

3. The method according to claim 1 , wherein the mineral acid is hydrochloric acid.

4. The method according to claim 1 , wherein the hydrochloric acid and alkanolamine are present in a molar ratio of not more than 10:1.

5. The method according to claim 1 , wherein the hydrochloric acid and alkanolamine are present in a molar ratio of not more than 7.0:1.

6. The method according to claim 1 , wherein the hydrochloric acid and alkanolamine are present in a molar ratio of not more than 4.1:1.

7. The method according to claim 1 , wherein the alkanolamine is selected from the group consisting of: monoethanolamine; diethanolamine; triethanolamine and combinations thereof.

8. The method according to claim 1 , wherein the alkanolamine is monoethanolamine.

9. The method according to claim 1 , wherein the alkanolamine is diethanolamine.

10. The method according to claim 1 , wherein the modified acid composition further comprises a corrosion inhibitor comprising a α,β-unsaturated aldehyde with no methyl group at the alpha position.

11. A method of use of a modified acid composition comprising:

providing an aqueous modified acid composition comprising a mineral acid and an alkanolamine in a molar ratio ranging from 3:1 to not more than 15:1 and having a pH of less than 1;

contacting a surface of the aqueous modified acid composition;

allowing the aqueous modified acid composition to act upon said surface;

removing the acid composition when an exposure time has been determined to be sufficient for the operation to be complete or sufficiently complete; and

wherein said method of use includes at least one of descaling pipelines and related equipment or descaling facilities.

12. The method according to claim 11 , wherein the mineral acid is selected from the group consisting of: HCl, nitric acid, sulfuric acid, sulfonic acid, phosphoric acid, and combinations thereof.

13. The method according to claim 11 , wherein the mineral acid is hydrochloric acid.

14. The method according to claim 11 , wherein the hydrochloric acid and alkanolamine are present in a molar ratio of not more than 10:1.

15. The method according to claim 11 , wherein the hydrochloric acid and alkanolamine are present in a molar ratio of not more than 7.0:1.

16. The method according to claim 11 , wherein the hydrochloric acid and alkanolamine are present in a molar ratio of not more than 4.1:1.

17. The method according to claim 11 , wherein the alkanolamine is selected from the group consisting of: monoethanolamine; diethanolamine; triethanolamine and combinations thereof.

18. The method according to claim 11 , wherein the alkanolamine is monoethanolamine.

19. The method according to claim 11 , wherein the alkanolamine is diethanolamine.

20. The method according to claim 11 , wherein the modified acid composition further comprises a corrosion inhibitor comprising a α, β-unsaturated aldehyde with no methyl group at the alpha position.

Assignments (4)
SECURITY INTEREST Recorded Dec 12, 2023
From: DORF KETAL CHEMICALS FZE
To: HSBC BANK MIDDLE EAST LIMITED
Reel/Frame 065878/0104 →
CORRECTIVE ASSIGNMENT TO CORRECT THE PRIOR ERRONEOUS RECORDATION OF ASSIGNMENT APPLICATION NUMBERS: 15614284, 17148881 PREVIOUSLY RECORDED ON REEL 063118 FRAME 0689. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded May 17, 2023
From: FLUID ENERGY GROUP LTD.
To: DORF KETAL CHEMICALS FZE
Reel/Frame 063695/0522 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 20, 2023
From: FLUID ENERGY GROUP LTD.
To: DORF KETAL CHEMICALS FZE
Reel/Frame 063118/0689 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 22, 2021
From: PURDY, CLAY; WEISSENBERGER, MARKUS
To: FLUID ENERGY GROUP LTD
Reel/Frame 056003/0880 →
Priority Claims (1)
CA 2969174 · Jun 2, 2017 · national
Continuity (3)
Division 16691815 · Nov 22, 2019
Continuation 15992951 · May 30, 2018
Related Publication 20210207017A1 · Jul 8, 2021