IP Library Granted Patent US 11,401,597
Granted Patent B2
US 11,401,597 · App. 17/239,616 · Granted Aug 2, 2022

Method for manufacturing nickel-based alloy high-temperature component

Inventors: Atsuo Ota (Yokohama, JP); Shinya Imano (Yokohama, JP)
Assignee: Mitsubishi Heavy Industries, Ltd.
C22F1/10B21J5/00C22C19/055
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Quick Facts
Patent No.
US 11,401,597
App. No.
17/239,616
Granted
Aug 2, 2022
Kind
B2
Abstract

This method for manufacturing a high-temperature component formed of a Ni-based alloy includes a step of subjecting a workpiece of the Ni-based alloy to hot die forging using predetermined dies to form a forge-molded article, the step including: a die/workpiece co-heating substep of heating the workpiece interposed between the dies to a forging temperature; and a hot forging substep of taking out the workpiece and the dies into a room temperature environment and immediately performing hot forging on the workpiece using a press machine. The predetermined dies are formed of another Ni-based superalloy comprising γ and γ′ phases, and have features in that: a solvus temperature of the γ′ phase is 1050-1250° C.; and the γ′ phase precipitates at least 10 vol. % at 1050° C. and has two kinds of forms of intra-grain γ′ phase precipitations within the γ phase grains and inter-grain γ′ phase precipitations between/among the γ phase grains.

Claims (34)

1. A method for repairing a die formed of a precipitation-strengthened Ni-based superalloy,

the die having a composition in which a γ′ phase is capable of precipitating in an amount of 10 volume % or more with respect to a γ phase as a matrix at 1050° C., and a solvus temperature of the γ′ phase is higher than 1050° C. and lower than 1250° C., and

the die having a structure in which the γ′ phase has two precipitation forms of intra-grain γ′ phase crystal particles that precipitate within crystal grains of the γ phase and inter-grain γ′ phase crystal particles that precipitate between or among crystal grains of the γ phase, and the inter-grain γ′ phase crystal particles precipitate in an amount of 10 volume % or more,

the method comprising the steps of:

subjecting the die being damaged to a softening heat treatment in which the die is heated up to 1000° C. or more but less than the solvus temperature of the γ′ phase so that the intra-grain γ′ phase crystal particles are decreased and followed by slow cooling the die to 500° C. at a rate of 100° C./h or less so that the inter-grain γ′ phase crystal particles grow;

subjecting the die being softening heat treated to a forming process in order to correct a shape of the die;

subjecting the die being shape corrected to a partial solution/aging treatment so that the inter-grain γ′ phase crystal particles remain in an amount of 10 volume % or more and the intra-grain γ′ phase crystal particles precipitate; and

subjecting the die being partial solution/aging treated to a finishing process.

2. The method for repairing the die formed of the precipitation-strengthened Ni-based superalloy according to claim 1 , wherein the precipitation-strengthened Ni-based superalloy has a composition of: by mass,

10 to 25% of Cr;

more than 0% and 30% or less of Co;

1 to 6% of Al;

2.5 to 7% of Ti and 3 to 9% in total of Ti, Nb and Ta;

4% or less of Mo;

4% or less of W;

0.08% or less of Zr;

10% or less of Fe;

0.03% or less of B;

0.1% or less of C;

2% or less of Hf;

5% or less of Re; and

a balance of Ni with inevitable impurities.

3. The method for repairing the die formed of the precipitation-strengthened Ni-based superalloy according to claim 1 , wherein

the die being softening heat treated has a Vickers hardness of 350 Hv or less.

4. The method for repairing the die formed of the precipitation-strengthened Ni-based superalloy according to claim 2 , wherein

the die being softening heat treated has a Vickers hardness of 350 Hv or less.

5. The method for repairing the die formed of the precipitation-strengthened Ni-based superalloy according to claim 1 , wherein

the die has a tensile strength of 450 MPa or more at 900° C.

6. The method for repairing the die formed of the precipitation-strengthened Ni-based superalloy according to claim 2 , wherein

the die has a tensile strength of 450 MPa or more at 900° C.

7. The method for repairing the die formed of the precipitation-strengthened Ni-based superalloy according to claim 3 , wherein

the die being partial solution/aging treated has a tensile strength of 450 MPa or more at 900° C.

8. The method for repairing the die formed of the precipitation-strengthened Ni-based superalloy according to claim 4 , wherein

the die being partial solution/aging treated has a tensile strength of 450 MPa or more at 900° C.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 22, 2022
From: MITSUBISHI POWER, LTD.
To: MITSUBISHI HEAVY INDUSTRIES, LTD.
Reel/Frame 059342/0723 →
Continuity (2)
Continuation 16348774
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