IP Library Granted Patent US 12,000,006
Granted Patent B2
US 12,000,006 · App. 17/248,953 · Granted Jun 4, 2024

3D printable hard ferrous metallic alloys for powder bed fusion

Inventors: Charles D. Tuffile (Swansea, MA); Harald Lemke (Franklin, MA)
Assignee: MACLEAN-FOGG COMPANY
C21D1/18B22F10/00B22F10/20B22F10/28B22F10/32B22F10/36B22F12/17B23K26/0006B33Y10/00B33Y40/00B33Y70/00C21D1/613C21D6/002C21D6/004C21D6/005C21D6/008C21D8/0257C22C38/001C22C38/02C22C38/04C22C38/20C22C38/22C22C38/26C22C38/40C22C38/42C22C38/44C22C38/48C23C8/22C23C8/54B22F1/05B22F2003/241B22F2003/248B22F9/082B22F2201/02B22F2201/30B22F2998/10B22F2999/00C22C33/0278Y02P10/25
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Quick Facts
Patent No.
US 12,000,006
App. No.
17/248,953
Granted
Jun 4, 2024
Kind
B2
Abstract

Alloy compositions for 3D metal printing procedures which provide metallic parts with high hardness, tensile strengths, yield strengths, and elongation. The alloys include Fe, Cr and Mo and at least three or more elements selected from C, Ni, Cu, Nb, Si and N. As built parts indicate a tensile strength of at least 1000 MPa, yield strength of at least 640 MPa, elongation of at least 3.0% and hardness (HV) of at least 375.

Claims (20)

1. A 3D printed metallic part comprising: one or more iron based metallic alloy layers including the elements C, Cr and Mo, wherein C is present at 0.1 wt. % to 0.35 wt. %, Cr is present at 10.0 wt. % to 19.0 wt. %, and Mo is present at 0.5 wt. % to 3.0 wt. %; and at least two elements from Ni, Cu, Nb, Si and N, wherein if present, Ni is present at 0 to 5.0 wt. %, if present, Cu is present at 0 to 5.0 wt. %, if present, Nb is present at 0 to 1.0 wt. %, if present, Si is present at 0 to 1.0 wt. %, and if present, N is present at 0 to 0.25 wt. %, and the balance of the alloy composition contains Fe; the layers each having thickness in the range of 2.0 microns to 200.0 microns; and the printed metallic part is an as-built part without post-heat treatment wherein the as-built part without post-heat treatment has tensile strength of at least 1000 MPa, a yield strength of at least 640 MPa, an elongation of at least 3.0%, and a hardness (HV) of at least 375.

2. The printed metallic part of claim 1 wherein Cr is present at 10.0 wt. % to 18.3 wt. %, Mo is present at 0.89 wt. % to 2.5 wt. %, C is present at 0.1 wt. % to 0.30 wt. %, Ni is present at 0 to 2.5 wt. %, Cu is present at 0 to 2.56 wt. %, Nb is present at 0 to 0.7 wt. %, Si is present at 0 to 0.7 wt. % and N is present at 0 to 0.25 wt. %, the balance Fe.

3. The printed metallic part of claim 1 , wherein the alloy includes at least three elements selected from Ni, Cu, Nb, Si and N.

4. The printed metallic part of claim 1 , wherein the alloy includes at least four elements selected from Ni, Cu, Nb, Si and N.

5. The printed metallic part of claim 1 , wherein the alloy includes Ni, Cu, Nb, Si and N.

6. The printed metallic part of claim 1 , wherein the as-built part without post-heat treatment has the tensile strength of 1000 MPa to 1900 MPa, the yield strength of 640 MPa to 1500 MPa, the elongation of 3.0% to 25.0%, and the hardness (HV) of 375 to 600.

7. The printed metallic part of claim 1 , wherein the part is heat-treated and comprises the hardness (HV) of at least 475.

8. The printed metallic part of claim 1 , wherein C is present at 0.1 wt. % to 0.30 wt. %, Cr is present at 10.5 wt. % to 12.0 wt. %.

9. The printed metallic part of claim 1 , wherein the as-built part without post-heat treatment has the yield strength of at least 800 MPa.

10. The printed metallic part of claim 1 , wherein the as-built part without post-heat treatment has the elongation of at least 7%.

11. The printed metallic part of claim 1 , wherein the as-built part without post-heat treatment has the hardness (HV) of at least 400.

12. A 3D printed metallic part comprising: one or more layers of an iron based metallic alloy including the elements C, Cr and Mo, wherein C is present at 0.1 wt. % to 0.35 wt. %, Cr is present at 10.0 wt. % to 19.0 wt. %, and Mo is present at 0.5 wt. % to 3.0 wt. %; and at least two elements from Ni, Cu, Nb, Si and N, wherein if present, Ni is present at 0 to 5.0 wt. %, if present, Cu is present at 0 to 5.0 wt. %, if present, Nb is present at 0 to 1.0 wt. %, if present Si is present at 0 to 1.0 wt. %, if present, N is present at 0 to 0.25 wt. %, and the balance of the alloy composition contains Fe; the layers each having thickness in the range of 2.0 microns to 200.0 microns; and the printed metallic part is an as-built part wherein the as-built part, has a tensile strength of at least 1000 MPa, a yield strength of at least 640 MPa, an elongation of at least 3.0%, and a hardness (HV) of at least 400.

13. The printed metallic part of claim 12 , wherein Cr is present at 10.0 wt. % to 18.3 wt. %, Mo is present at 0.89 wt. % to 2.5 wt. %, C is present at 0.1 to 0.30 wt. %, Ni is present at 0 to 2.5 wt. %, Cu is present at 0 wt. % to 2.56 wt. %, Nb is present at 0 to 0.7 wt. %, Si is present at 0 to 0.7 wt. % and N is present at 0 to 0.25 wt. %, the balance Fe.

14. The printed metallic part of claim 12 , wherein the alloy includes at least three elements selected from Ni, Cu, Nb, Si and N.

15. The printed metallic part of claim 12 , wherein the alloy includes at least four elements selected from Ni, Cu, Nb, Si and N.

16. The printed metallic part of claim 12 , wherein the alloy includes Ni, Cu, Nb, Si and N.

17. The printed metallic part of claim 12 , wherein the as-built part without post-heat treatment, has the tensile strength of 1000 MPa to 1900 MPa, the yield strength of 640 MPa to 1500 MPa, the elongation of 3.0% to 25.0%, and the hardness (HV) of 375 to 600.

18. The printed metallic part of claim 12 , wherein the as-built part does not have a post-heat treatment.

19. The printed metallic part of claim 12 , wherein the part is heat-treated and has the hardness (HV) of at least 475.

20. The printed metallic part of claim 12 , wherein C is present at 0.1 wt. % to 0.30 wt. %, and Cr is present at 10.5 wt. % to 12.0 wt. %.

Assignments (6)
NOTICE OF GRANT OF SECURITY INTEREST IN PATENTS Recorded May 16, 2024
From: MAC LEAN-FOGG COMPANY
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 067455/0802 →
SECURITY INTEREST Recorded May 7, 2024
From: MAC LEAN-FOGG COMPANY
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 067337/0156 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 9, 2021
From: TUFFILE, CHARLES D.; LEMKE, HARALD
To: THE NANOSTEEL COMPANY, INC.
Reel/Frame 056487/0555 →
SECURITY INTEREST Recorded Jun 9, 2021
From: THE NANOSTEEL COMPANY, INC.
To: HORIZON TECHNOLOGY FINANCE CORPORATION
Reel/Frame 056489/0248 →
NUNC PRO TUNC ASSIGNMENT Recorded Jun 3, 2021
From: FORMETRIX, INC.
To: MACLEAN-FOGG COMPANY
Reel/Frame 056429/0061 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 21, 2021
From: HORIZON TECHNOLOGY FINANCE CORPORATION; HORIZON FUNDING TRUST 2019-1; HORIZON CREDIT II LLC
To: FORMETRIX, INC.
Reel/Frame 056316/0941 →
Continuity (4)
Continuation 16393194 · Apr 24, 2019
Continuation In Part 15800210 · Nov 1, 2017
Provisional Application 62415667 · Nov 1, 2016
Related Publication 20210301362A1 · Sep 30, 2021