IP Library Granted Patent US 11,619,004
Granted Patent B2
US 11,619,004 · App. 17/292,191 · Granted Apr 4, 2023

Method for dewatering a web comprising microfibrillated cellulose and a film produced from the dewatered web

Inventors: Isto Heiskanen (Imatra, FI); Jukka Kankkunen (Imatra, FI); Riku Pihko (Jyväskylä, FI); Vesa Kunnari (Tuusula, FI)
Assignee: Stora Enso OYJ
D21F3/08D21F3/045D21F7/12D21H11/18
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Quick Facts
Patent No.
US 11,619,004
App. No.
17/292,191
Granted
Apr 4, 2023
Kind
B2
Abstract

The present invention relates to a method for dewatering a web comprising microfibrillated cellulose, wherein the method comprises the steps of: providing a suspension comprising between 50 weight-% to 100 weight-% of microfibrillated cellulose based on total dry weight, forming a fibrous web of said suspension on a support wherein said web has a dry content of 1-25% by weight, applying a dewatering felt into direct contact with the fibrous web, conducting said fibrous web, arranged between said dewatering felt and said substrate, through a pressing equipment. The invention further relates to a film produced from said method.

Claims (18)

1. A method for dewatering a web comprising microfibrillated cellulose, wherein the method comprises the steps of:

providing a suspension comprising between 50 weight-% to 100 weight-% of microfibrillated cellulose based on a total dry weight,

forming a fibrous web of said suspension on a support, wherein said fibrous web has a dry content of 1-25% by weight and wherein said support is a metal support wherein said fibrous web is formed by cast coating on the metal support so that a surface on the metal support is smooth, wherein the metal support is heated to a temperature between 30-150° C. before said fibrous web is applied to the support,

applying a dewatering felt into direct contact with said fibrous web after said fibrous web has been formed,

conducting said fibrous web, arranged between said dewatering felt and said support, through a pressing equipment to provide a dewatered web, and

drying the dewatered web to form a film which has an Oxygen Transmission Rate (OTR) value (23° C., 50% RH) below 400 cc/m 2 /24 h according to ASTM D-3985.

2. The method as claimed in claim 1 , wherein the pressing equipment comprises an extended nip.

3. The method according to claim 1 , wherein the pressing equipment is a belt press.

4. The method according to claim 3 , wherein the fibrous web is treated in the belt press for a distance of at least 20% of a diameter of a roll of the belt press.

5. The method according to claim 1 , wherein the dewatering felt is applied to the fibrous web at least 20 cm before being conducted through the pressing equipment.

6. The method according to claim 1 , wherein a pressure used in the pressing equipment is between 1-100 bar.

7. The method according to claim 1 , wherein a pressure used in the pressing equipment is gradually increased.

8. The method according to claim 1 , wherein said fibrous web has a dry content of 15-50 weight-% after dewatering in the pressing equipment.

9. The method according to claim 1 , wherein the microfibrillated cellulose of the suspension has a Schopper-Riegler (SR) value above 90.

10. The method according to claim 1 , wherein said fibrous web is conducted through the pressing equipment at a speed of at least 50 m/min.

11. The method according to claim 1 , wherein said fibrous web is heated before the dewatering felt is applied into contact.

12. A film comprising:

microfibrillated cellulose and obtained by the method of claim 1 , wherein said film has a density above 700 kg/m 3 and an Oxygen Transmission Rate (OTR) value (23° C., 50% RH) below 400 cc/m 2 /24 h according to ASTM D-3985.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 24, 2021
From: HEISKANEN, ISTO; KANKKUNEN, JUKKA; PIHKO, RIKU; KUNNARI, VESA
To: STORA ENSO OYJ
Reel/Frame 057273/0342 →
Priority Claims (1)
SE 1851394-5 · Nov 9, 2018 · national
Continuity (1)
Related Publication 20210324580A1 · Oct 21, 2021