IP Library Granted Patent US 11,613,111
Granted Patent B2
US 11,613,111 · App. 17/306,915 · Granted Mar 28, 2023

Functional tie-layer formulations in biaxially oriented films containing HDPE

Inventors: Eric T. Gohr (Sharpsburg, GA); Robert M. Sheppard (Peachtree City, GA)
Assignee: Jindal Films Americas LLC
B32B27/32B29C48/0018B29C48/08B29C48/21B29C55/143B32B7/12B32B27/08B32B27/16B32B27/18B32B27/20B32B27/327B65D65/40B29K2023/065B29K2023/0633B29K2023/12B29K2105/0008B32B2250/03B32B2250/05B32B2250/24B32B2250/242B32B2255/10B32B2255/20B32B2255/205B32B2255/26B32B2270/00B32B2307/30B32B2307/516B32B2307/518B32B2307/72B32B2307/7244B32B2307/7246B32B2307/732B32B2439/40B32B2439/46B32B2439/70B32B2553/00
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Quick Facts
Patent No.
US 11,613,111
App. No.
17/306,915
Granted
Mar 28, 2023
Kind
B2
Abstract

Disclosed are compositions and methods for multilayer films, which, in one embodiment may comprise a core layer comprising at least 50 wt. % of high-density polyethylene. Further, the multilayer film may include a first skin layer consisting essentially of one or more ethylene-propylene copolymers. Further still, the multilayer film may include a second skin layer consisting essentially of one or more ethylene-propylene-butylene terpolymers. And yet further, the multilayer film may be oriented in at least one direction, and at least two layers of the multilayer film are coextruded.

Claims (33)

1. A coextruded, biaxially oriented, multilayer film comprising:

a core layer comprising: (i) at least 50 wt. % of high-density polyethylene, (ii) linear, low-density polyethylene, and (iii) hydrocarbon resin;

a first tie layer and a second tie layer, wherein each comprises: (i) high-density polyethylene, (ii) linear, low: density polyethylene, and (iii) olefin-block copolymer in an amount ≤40 wt. % but ≥15 wt. %;

a first skin layer located adjacent to the first tie layer, wherein the first skin layer consists essentially of one or more ethylene-propylene copolymers; and

a second skin layer located adjacent to the second tie layer, wherein the second skin layer consists essentially of one or more ethylene-propylene-butylene terpolymers,

wherein the first tie layer and/or the second tie layer comprise at least 60 wt. % of the high-density polyethylene,

wherein the coextruded, biaxially oriented multilayer film has a haze of ≤7% using ASTM D1003.

2. The coextruded, biaxially oriented, multilayer film of claim 1 , further comprising one or more additives.

3. The coextruded, biaxially oriented, multilayer film of claim 1 , wherein the linear, low-density polyethylene in the first tie layer and/or the second tie layer comprises a concentration within a range from 5 wt. % through 35 wt. %.

4. The coextruded, biaxially oriented, multilayer film of claim 1 , wherein the first tie layer and/or the second tie layer comprise at least 80 wt. % high-density polyethylene.

5. The coextruded, biaxially oriented, multilayer film of claim 1 , wherein the first skin layer comprises at least 98 wt. % ethylene-polypropylene copolymers.

6. The coextruded, biaxially oriented, multilayer film of claim 1 , wherein the first skin layer and/or the second skin layer comprises at least 98 wt. % ethylene-polypropylene-butylene terpolymers.

7. The coextruded, biaxially oriented, multilayer film of claim 1 , wherein the first skin layer consists of the one or more ethylene-propylene copolymers and antiblock, optionally in a masterbatch solution.

8. The coextruded, biaxially oriented, multilayer film of claim 1 , wherein the second skin layer consists of the one or more ethylene-propylene-butylene terpolymers and antiblock, optionally in a masterbatch solution.

9. The coextruded, biaxially oriented, multilayer film of claim 1 , wherein the core layer consists of the at least 50 wt. % of high-density polyethylene, 40 wt. % or less of the linear, low-density polyethylene and the hydrocarbon resin.

10. The coextruded, biaxially oriented, multilayer film of claim 1 , wherein the core layer consists of the at least 50 wt. % of high-density polyethylene, 40 wt. % or less of the linear, low-density polyethylene, the hydrocarbon resin, and optionally, additives.

11. The coextruded, biaxially oriented, multilayer film of claim 1 , wherein haze is 5% or less using ASTM D1003.

12. The coextruded, biaxially oriented, multilayer film of claim 1 , wherein haze is 4% or less using ASTM D1003.

13. The coextruded, biaxially oriented, multilayer film of claim 1 , wherein the first skin layer consist of at least 95 wt % of the one or more ethylene-propylene copolymers and 5 wt. % or less of additives.

14. The coextruded, biaxially oriented, multilayer film of claim 1 , wherein the core further comprises 5 wt. % or less of additives.

15. The coextruded, biaxially oriented, multilayer film of claim 1 , wherein the linear, low-density polyethylene in the core layer, the first tie layer and/or the second tie layer is metallocene-catalyzed.

16. The coextruded, biaxially oriented, multilayer film of claim 1 , further comprising one or more polymeric films and/or paper products laminated to the coextruded, biaxially oriented, multilayer film.

17. The coextruded, biaxially oriented, multilayer film of claim 1 , further comprising one or more metallized layers, printable layers, adhesive layers, primer layers and/or coated layers in proximity to one or both outer surfaces of the coextruded, biaxially oriented, multilayer film.

18. A method comprising providing the coextruded, biaxially oriented, multilayer film of claim 1 , and forming a package or pouch therefrom.

19. The coextruded, biaxially oriented, multilayer film of claim 1 , further comprising surface treatment to one or both outer surfaces of the coextruded, biaxially oriented, multilayer film.

20. A coextruded, biaxially oriented, multilayer film comprising:

a core layer comprising: (i) at least 50 wt. % of high-density polyethylene, (ii) low-density polyethylene, and (iii) hydrocarbon resin;

a first tie layer and a second tie layer, wherein each comprises: (i) high-density polyethylene, (ii) low-density polyethylene, and (iii) olefin-block copolymer in an amount ≤40 wt. % but ≥15 wt. %;

a first skin layer located adjacent to the first tie layer, wherein the first skin layer consists essentially of one or more ethylene-propylene copolymers; and

a second skin layer located adjacent to the second tie layer, wherein the second skin layer consists essentially of one or more ethylene-propylene-butylene terpolymers,

wherein the first tie layer and/or the second tie layer comprise at least 60 wt. % of the high-density polyethylene,

wherein the low-density polyethylene in the core layer, the first tie layer, and/or the second tie layer: (i) comprises non-linear low-density polyethylene and/or non-metallocene-catalyzed, linear, low-density polyethylene; and/or (ii) further comprises non-linear low-density polyethylene and/or non-metallocene-catalyzed, linear, low-density polyethylene,

wherein the coextruded, biaxially oriented multilayer film has a haze of ≤7% using ASTM D1003.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 5, 2021
From: JINDAL FILMS AMERICAS LLC
To: JINDAL INNOVATION CENTER SRL
Reel/Frame 057699/0318 →