IP Library Granted Patent US 12,070,732
Granted Patent B2
US 12,070,732 · App. 17/309,776 · Granted Aug 27, 2024

Highly effective functional additive products

Inventors: Scott Kevin Palm (Reno, NV); Fangfu Zhang (Reno, NV)
Assignee: U.S. Silica Company
B01J20/14B01J20/3021B01J20/3078
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Quick Facts
Patent No.
US 12,070,732
App. No.
17/309,776
Granted
Aug 27, 2024
Kind
B2
Abstract

This invention concerns highly effective functional additive products that comprise diatomite. More particularly, it concerns such functional additive products possessing particle size distributions which make them more effective as functional additives in filled systems. Higher effectiveness is demonstrated through lower Standard Sheen and/or reduced unit consumption relative to diatomite functional additives already in the public domain. Such products may also possess high brightness, low tint and/or an absence of detectable crystalline silica.

Claims (28)

1. A product comprising diatomite, wherein the product is powdered and has

(a) Standard Sheen of 0.4 to 0.5 and Hegman of 1.0 to 2.0, or (b) Standard Sheen of 0.6 to 0.7 and Hegman of 2.5 to 3.5.

2. The product of claim 1 , wherein the Standard Sheen is 0.4 to 0.5 and the Hegman is 1.0 to 2.0, wherein the product further has a Ratio (R) of 0.35 to 0.52.

3. The product of claim 1 , wherein the Standard Sheen is 0.6 to 0.7 and the Hegman is 2.5 to 3.5, wherein the product further has a Ratio (R) of 0.34 to 0.45.

4. The product of claim 1 , wherein the product further has a Y value of 79 to 91, and an L* value of 91 to 97.

5. The product of claim 1 , wherein the product further has an a* value of −0.1 to 1.2.

6. The product of claim 1 , wherein the product further has a b* value of 1.0 to 5.0.

7. The product of claim 1 , wherein the product further has a Standard Contrast Ratio of 0.90 to 0.92.

8. The product of claim 1 , wherein the product is free of a total crystalline silica content as measured according to an LH Method.

9. The product of claim 2 , wherein the product is free of a total crystalline silica content as measured according to an LH Method.

10. The product of claim 3 , wherein the product is free of a total crystalline silica content as measured according to an LH Method.

11. The product of claim 1 , wherein the product is free of a cristobalite content as measured according to an LH method.

12. The product of claim 2 , wherein the product is free of a cristobalite content as measured according to an LH method.

13. The product of claim 3 , wherein the product is free of a cristobalite content as measured according to an LH method.

14. A method of using the product of claim 1 comprising adding the product of claim 1 into a paint, a coating, a personal care product, a plastic film, a paper, a fiberboard, an elastomer, an adhesive, a caulk or a sealant.

15. The product of claim 1 , in which the diatomite comprises flux calcined diatomite,

wherein the Standard Sheen is 0.4 to 0.5 and the Hegman is 1.0 to 2.0,

wherein the product further has a D50 of 27 to 36 and a D95 of 58 to 68.

16. The product of claim 1 , in which the diatomite comprises flux calcined diatomite,

wherein the Standard Sheen is 0.6 to 0.7 and the Hegman is 2.5 to 3.5,

wherein the product further has a D50 of 19 to 24 and a D95 of 40 to 46.

17. The product of claim 1 , in which the diatomite comprises flux calcined diatomite,

wherein the Standard Sheen is 0.4 to 0.5 and the Hegman is 1.0 to 2.0, and

wherein the product further has a Flatting Efficiency of 96% to 99%.

18. The product of claim 1 , in which the diatomite comprises flux calcined diatomite,

wherein the Standard Sheen is 0.6 to 0.7 and the Hegman is 2.5 to 3.5,

wherein the product further has a Flatting Efficiency of 93% to 99%.

19. The product of claim 11 , in which the product is free of a quartz content as measured according to an LH method.

Assignments (2)
NOTICE OF GRANT OF SECURITY INTEREST IN INTELLECTUAL PROPERTY (FIRST LIEN) Recorded Jul 31, 2024
From: EP MINERALS, LLC
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 068312/0958 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 7, 2021
From: PALM, SCOTT KEVIN; ZHANG, FANGFU
To: EP MINERALS, LLC
Reel/Frame 056772/0481 →
Continuity (1)
Related Publication 20220048009A1 · Feb 17, 2022