IP Library Granted Patent US 11,578,438
Granted Patent B2
US 11,578,438 · App. 17/318,494 · Granted Feb 14, 2023

Polyamide nanofiber nonwovens for acoustic applications

Inventors: Wai-shing Yung (Pensacola, FL); Scott E. Osborn (Pensacola, FL); Chris E. Schwier (Pensacola, FL); Vikram Gopal (The Woodlands, TX); Albert Ortega (Pensacola, FL)
Assignee: Ascend Performance Materials Operations LLC
D04H1/4334D04H1/43838D04H1/552D04H1/56D04H1/565D04H3/016D04H3/16B82Y40/00
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Quick Facts
Patent No.
US 11,578,438
App. No.
17/318,494
Granted
Feb 14, 2023
Kind
B2
Abstract

A nanofiber nonwoven product is disclosed which comprises a polyamide with a relative viscosity from 2 to 330, spun into nanofibers with an average diameter of less than 1000 nanometers (1 micron). In general, the inventive products are prepared by: (a) providing a polyamide composition, wherein the polyamide has a relative viscosity from 2 to 330; (b) melt spinning the polyamide composition into a plurality of nanofibers having an average fiber diameter of less than 1 micron, followed by (c) forming the nanofibers into the product.

Claims (22)

1. An article for an acoustic application comprising:

a scrim layer;

a nanofiber nonwoven layer comprising polyamide nanofibers deposited on the scrim layer, wherein the polyamide of the nanofibers have a relative viscosity from 4 to 330, and wherein the polyamide nanofibers have an average diameter from 100 to 950 nanometers.

2. The acoustic article of claim 1 , wherein the polyamide nanofibers have an average diameter from 125 to 700 nanometers.

3. The acoustic article of claim 1 , wherein the melt point of the nanofiber nonwoven layer is 225° C. or greater.

4. The acoustic article of claim 1 , wherein no more than 20% of the polyamide nanofibers have a diameter of greater than 700 nanometers.

5. The acoustic article of claim 1 , wherein the polyamide nanofibers comprises nylon 66 or nylon 6/66.

6. The acoustic article of claim 1 , wherein the polyamide nanofibers comprises N6, N66, N6T/66, N612, N6/66, N6I/66, N66/6I/6T, N11, N12 or combinations thereof, wherein “N” means Nylon.

7. The acoustic article of claim 1 , wherein the nanofiber nonwoven layer has an Air Permeability Value of less than 600 CFM/ft 2 .

8. The acoustic article of claim 1 , wherein the nanofiber nonwoven layer has a basis weight of 150 GSM or less.

9. The acoustic article of claim 1 , wherein the nanofiber nonwoven layer has a TDI of at least 20 ppm and an ODI of at least 1 ppm.

10. The acoustic article of claim 1 , wherein the nanofiber nonwoven layer is free of solvent.

11. The acoustic article of claim 1 , wherein the nanofiber nonwoven layer comprises less than 5000 ppm solvent.

12. The acoustic article of claim 1 , wherein the nanofiber nonwoven layer comprises an additives include oils, waxes, solvents, lubricants, stabilizers, delusterants, antioxidants, colorants, pigments, and dyes.

13. The acoustic article of claim 1 , wherein the scrim layer comprises a nylon spunbond scrim.

14. The acoustic article of claim 1 , wherein the scrim layer comprises a spunbond fabric comprising a polyester spun bond fabric or a polypropylene spunbond fabric.

15. A method of producing an acoustic article comprising:

(a) feeding a polyamide melt through a die into a high velocity gaseous stream comprising the polyamide composition;

(b) spinning the polyamide composition into a plurality of nanofibers having an average fiber diameter from 100 to 950 nanometers; and

(c) forming the polyamide nanofibers on a scrim layer, wherein the polyamide of the nanofibers have a relative viscosity from 4 to 330.

16. The method of claim 15 , wherein the polyamide composition is melt-spun by 2-phase propellant-gas spinning, including extruding the polyamide composition in liquid form with pressurized gas through a fiber-forming channel.

17. The method of claim 15 , wherein the relative viscosity of the polyamide nanofibers is reduced as compared to the polyamide composition prior to spinning and forming the product.

Assignments (6)
RELEASE OF SECURITY INTEREST Recorded Dec 23, 2025
From: WILMINGTON SAVINGS FUND SOCIETY, FSB
To: ASCEND PERFORMANCE MATERIALS OPERATIONS LLC
Reel/Frame 074050/0090 →
SECURITY INTEREST Recorded Dec 23, 2025
From: ASCEND PERFORMANCE MATERIALS OPERATIONS LLC
To: WILMINGTON SAVINGS FUND SOCIETY, FSB
Reel/Frame 074056/0183 →
SECURITY INTEREST Recorded Dec 19, 2025
From: ASCEND PERFORMANCE MATERIALS OPERATIONS LLC
To: WELLS FARGO BANK, NATIONAL ASSOCIATION
Reel/Frame 074007/0183 →
SECURITY INTEREST Recorded Apr 10, 2025
From: BANK OF AMERICA, N.A.
To: WILMINGTON SAVINGS FUND SOCIETY, FSB
Reel/Frame 070811/0705 →
SECURITY INTEREST Recorded Dec 8, 2022
From: ASCEND PERFORMANCE MATERIALS OPERATIONS LLC
To: WELLS FARGO CAPITAL FINANCE, LLC
Reel/Frame 062094/0172 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 16, 2022
From: YUNG, WAI-SHING; OSBORN, SCOTT E.; SCHWIER, CHRIS E.; GOPAL, VIKRAM; ORTEGA, ALBERT
To: ASCEND PERFORMANCE MATERIALS OPERATIONS LLC
Reel/Frame 061796/0451 →