IP Library Patent Application 17334480
Patent Application
App. No. 17/334,480

CARBON FOAM, SYSTEMS AND METHODS FOR FORMING THE SAME

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Quick Facts
Patent No.
US None
App. No.
17/334,480
Abstract

Embodiments disclosed herein relate to low-cost methods of producing a carbon foam through a partial solvent extraction process and sintering process carried out at atmospheric pressure. Given that the carbon foam is produced at atmospheric pressure, the methods disclosed herein may include a continuous process.

Claims (51)

1 . A method to form a carbon foam, the method comprising:

providing a carbon source within a container, wherein the carbon source includes a volatile portion;

reducing the volatile portion of the carbon source by a partial solvent extraction including at least one solvent to form a carbon foam precursor; and

heating the carbon foam precursor at atmospheric pressure to form the carbon foam.

2 . The method of claim 1 , wherein the carbon foam precursor is heated in a non-oxidizing atmosphere.

3 . The method of claim 1 , wherein:

reducing the volatile portion of the at least one carbon source by a partial solvent extraction forms an extracted portion of the of the carbon source; and

the extracted portion is further processed to produce at least one other carbon material.

4 . The method of claim 3 , wherein the at least one other carbon material comprises at least one of a pitch, a graphene, a carbon fiber, or a combination thereof.

5 . The method of claim 3 , wherein the extracted portion of the carbon forms a protective layer on an exterior surface of the carbon foam.

6 . The method of claim 1 , further comprising:

adding a pitch the container;

wherein the pitch or other form of volatile hydrocarbons forms a protective layer on an exterior surface of the carbon foam.

7 . The method of claim 1 , wherein the carbon source comprises at least one of a coal, a coal-derived pitch, a coal tar, a graphite, a petroleum, a petroleum product, a petroleum-derived pitch, a naphthalene-derived pitch, a green carbon foam, a green coke, or a combination thereof.

8 . The method of claim 1 , wherein the at least one solvent comprises at least a polar solvent, a non-polar solvent, an organic solvent, an inorganic solvent, a supercritical solvent, a sub-critical solvent, or a combination thereof.

9 . The method of claim 1 , wherein the method comprises a continuous process.

10 . The method of claim 1 , wherein heating the carbon foam precursor at atmospheric pressure comprises heating the carbon foam precursor at one or more heating rates to produce a green carbon foam.

11 . The method of claim 1 , wherein the carbon source is placed in a vented mold to permit the escape of volatile material such that the carbon foam includes predetermined shapes.

12 . The method of claim 1 , further comprising calcinating the carbon foam;

wherein calcinating the carbon foam comprises heating the carbon foam in a non-oxidizing atmosphere to a temperature from about 800° C. to about 1400° C.

13 . The method of claim 1 , further comprising graphitizing the carbon foam;

wherein graphitizing the carbon foam comprises heating the carbon foam in a non-oxidizing atmosphere to a temperature from about 2000° C. to about 2600° C.

14 . A carbon foam, comprising:

a solid porous carbon;

a carbon fiber or carbon fiber tow incorporated within the porous carbon; and

a protective coating disposed on an outer surface of the carbon foam.

15 . The carbon foam of claim 15 , wherein the protective coating is formed by applying a volatile rich component to an interior surface of a container holding a precursor to the carbon foam, manipulating the volatile content of the precursor to the carbon foam during the solvent extraction processor, or a combination thereof.

16 . The carbon foam of claim 15 , wherein:

the carbon foam is produced from two or more precursors to the carbon foam; and

a portion of the carbon foam produced from a first precursor exhibits characteristics different from a portion of the carbon foam produced from a second precursor.

17 . The carbon foam of claim 17 , wherein the characteristics include at least one of hear transfer rate, strength, weight, or electrical conductivity.

18 . The carbon foam of claim 15 , wherein the protective coating comprises a graphene, a graphene oxide, a form of non-porous carbon, or a combination thereof.

19 . The carbon foam of claim 15 , wherein the coefficient of thermal expansion of the porous carbon is approximately the same as the coefficient of thermal expansion of the carbon fiber or the carbon fiber tow.

20 . A method to form a composite carbon foam, the method comprising:

producing a first carbon foam precursor through a partial solvent extraction;

grinding the first carbon foam precursor into a powder, wherein the powder includes an average particle size of about 50 nm or greater;

adding one or more carbon fibers or carbon fiber tows to the first carbon foam precursor; and

heating the first carbon foam precursor and the one or more carbon fibers or carbon fiber tows at atmospheric pressure to form a composite carbon foam.

21 . The method of claim 20 , wherein adding one or more carbon fibers or carbon fiber tows to the first carbon foam precursor comprises:

drawing the one or more carbon fibers across a surface of the carbon foam precursor; and

adding an additional carbon foam precursor to incorporate the carbon fiber or carbon fiber tows within the composite carbon foam.

22 . The method of claim 21 , wherein:

the additional carbon foam precursor includes a second carbon foam precursor; and

the second carbon foam precursor is different than the first carbon foam precursor.

23 . The method of claim 21 , wherein:

adding one or more carbon fibers or carbon fiber tows includes applying a tension to the one or more carbon fibers or carbon fiber tows; and

wherein the tension is configured to compensate for thermal expansion of the porous carbon and the carbon fiber.

24 . The method of claim 20 , further comprising calcinating the composite carbon foam, wherein calcinating the composite carbon foam comprises heating the composite carbon foam to a temperature from about 800° C. to about 1400° C.

25 . The method of claim 20 , further comprising graphitizing the composite carbon foam;

wherein graphitizing the composite carbon foam comprises heating the composite carbon foam to a temperature from about 2000° C. to about 2600° C.

26 . The method of claim 20 , wherein the first carbon foam precursor is heated in a non-oxidizing atmosphere.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 21, 2021
From: YURCHICK, CHRISTOPHER L.
To: CARBON HOLDINGS INTELLECTUAL PROPERTIES, LLC
Reel/Frame 057871/0339 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 14, 2021
From: ATKINS, CHARLES AGEE
To: CARBON HOLDINGS INTELLECTUAL PROPERTIES, LLC
Reel/Frame 057797/0641 →