IP Library Granted Patent US 11,952,271
Granted Patent B2
US 11,952,271 · App. 17/393,961 · Granted Apr 9, 2024

Photo triggered covalent organic frameworks and methods of using

Inventors: Derek Richard Vardon (Lakewood, CO); Wade A. Braunecker (Boulder, CO); Justin Carter Johnson (Denver, CO); Thomas Gennett (Denver, CO); Rachel Elizabeth Mow (Boulder, CO); Kurt Michael Van Allsburg (Denver, CO); Gabriella Lahti (Denver, CO)
Assignees: Alliance for Sustainable Energy, LLC; Colorado School of Mines
C01B3/0015C07F1/08B82Y40/00
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Quick Facts
Patent No.
US 11,952,271
App. No.
17/393,961
Granted
Apr 9, 2024
Kind
B2
Abstract

Described herein are compositions and methods for the storage and release of hydrogen gas using covalent organic frameworks (COFs). Advantageously, the compositions and methods described herein may be used for the facile and rapid release of hydrogen gas at near ambient temperatures. The described COFs allow for photoactivation, where the release of gas is initiated or the rate of release is increased with the COF is exposed to electromagnetic radiation, for example, UV light.

Claims (14)

1. A composition comprising:

a covalent organic framework (COF) comprising a plurality of Cu(I) moieties,

wherein the COF desorbs hydrogen gas when exposed to light; and

wherein the COF is defined by the structure:

2. The composition of claim 1 , wherein the COF further comprises a capping group.

3. The composition of claim 2 , wherein the capping group comprises an aldehyde functionalized tetrakis(3,5-bis(trifluoromethyl)phenyl) borate) ionic liquid compound.

4. The composition of claim 1 , wherein the COF defines a pore.

5. The composition of claim 1 , wherein the light is in the UV spectrum selected from the range of 10 nm to 400 nm.

6. The composition of claim 1 , further comprising a fluid, wherein: the COF and the fluid form a colloidal solution where the COF is stably suspended in the fluid.

7. The composition of claim 6 , wherein the COF is present in the form of nanoparticles.

8. The composition of claim 6 , wherein the fluid comprises at least one of an ionic liquid or a liquid polymer.

9. The composition of claim 8 , wherein the liquid polymer comprises a siloxane.

10. The composition of claim 1 , wherein the COF also desorbs ethylene when exposed to light.

11. The composition of claim 1 , wherein the COF also desorbs carbon monoxide when exposed to light.

Assignments (3)
CHANGE OF NAME Recorded Dec 16, 2025
From: ALLIANCE FOR SUSTAINABLE ENERGY, LLC
To: ALLIANCE FOR ENERGY INNOVATION, LLC
Reel/Frame 073993/0276 →
CONFIRMATORY LICENSE Recorded Mar 25, 2022
From: NATIONAL RENEWABLE ENERGY LABORATORY
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 059401/0554 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 5, 2021
From: BRAUNECKER, WADE A.; JOHNSON, JUSTIN C.; LAHTI, GABRIELLA; VAN ALLSBURG, KURT MICHAEL; VARDON, DEREK RICHARD
To: ALLIANCE FOR SUSTAINABLE ENERGY, LLC
Reel/Frame 057090/0929 →
Continuity (2)
Provisional Application 63060870 · Aug 4, 2020
Related Publication 20220041437A1 · Feb 10, 2022