IP Library Granted Patent US 11,661,380
Granted Patent B2
US 11,661,380 · App. 17/395,992 · Granted May 30, 2023

Multi-environmental barrier coating, processes for coating articles, and their coated articles

Inventors: Richard Wesley Jackson (Mystic, CT); James T. Beals (West Hartford, CT); Xia Tang (West Hartford, CT); Xuan Liu (Glastonbury, CT); David A. Litton (West Hartford, CT); Brian T. Hazel (Avon, CT)
Assignee: Raytheon Technologies Corporation
C04B41/4527C04B41/5071C04B41/52
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Quick Facts
Patent No.
US 11,661,380
App. No.
17/395,992
Granted
May 30, 2023
Kind
B2
Abstract

A coated article including an article having a surface; an oxidation resistant bond coat layer deposited on the surface, the oxidation resistant bond coat layer comprising a metal silicide phase, a crystalline ceramic phase and an amorphous ceramic phase, wherein the metal silicide phase has an aspect ratio greater than 1:1 but less than 50:1.

Claims (11)

1. A coated article, comprising:

an article having a surface; and

an oxidation resistant bond coat layer deposited on the surface, the oxidation resistant bond coat layer comprising a metal silicide phase, a crystalline ceramic phase and an amorphous ceramic phase, wherein the metal silicide phase has an aspect ratio greater than 1:1 but less than 50:1.

2. The coated article as recited in claim 1 , wherein the metal silicide phase and the crystalline ceramic phase each have an aspect ratio greater than 3:1.

3. The coated article as recited in claim 1 , wherein the metal silicide phase and the crystalline ceramic phase each have an aspect ratio greater than 5:1.

4. The coated article as recited in claim 1 , wherein a volume fraction of the metal silicide phase ranges between 20-80 vol. %, a volume fraction of the crystalline ceramic phase is 25-75 vol. %, and a volume fraction of the amorphous ceramic phase ranges between 1-30 vol. %.

5. The coated article as recited in claim 1 , wherein a volume fraction of the metal silicide phase is 60 vol. % MoSi 2 , a volume fraction of the crystalline ceramic phase is 25 vol. % HfSiO 4 , and a volume fraction of the amorphous ceramic phase is 15 vol. % boro-silicate glass where the glass has the composition (Si 0.75 B 0.15 Al 0.05 Na 0.05 )O 2 with porosity less than 10%.

6. The coated article as recited in claim 1 , wherein a volume fraction of the metal silicide phase is 60 vol. % MoSi 2 , a volume fraction of the crystalline ceramic phase is 25 vol. % HfSiO 4 , and 5% HfB 2 ; and a volume fraction of the amorphous ceramic phase is 10 vol. % boro-silicate glass where the glass has the composition (Si 0.75 B 0.15 Al 0.05 Na 0.05 )O 2 with porosity less than 10%.

7. The coated article as recited in claim 1 , further comprising an environmental protective top coat layer disposed upon the oxidation resistant bond coat layer, whereby the oxidation resistant bond coat layer is operable to repair a crack in the environmental protective top coat layer during operation of the coated article.

8. The coated article as recited in claim 1 , wherein the metal silicide phase has an aspect ratio greater than 3:1.

9. The coated article as recited in claim 1 , wherein the metal silicide phase has an aspect ratio greater than 5:1.

Assignments (2)
CHANGE OF NAME Recorded Jul 27, 2023
From: RAYTHEON TECHNOLOGIES CORPORATION
To: RTX CORPORATION
Reel/Frame 064714/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 19, 2022
From: JACKSON, RICHARD WESLEY; BEALS, JAMES T.; TANG, XIA; LIU, XUAN; LITTON, DAVID A.; HAZEL, BRIAN T.
To: RAYTHEON TECHNOLOGIES CORPORATION
Reel/Frame 060550/0259 →
Continuity (1)
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