IP Library Patent Application 17420158
Patent Application
App. No. 17/420,158

QUATERNARY AZEOTROPE AND AZEOTROPE-LIKE COMPOSITIONS FOR SOLVENT AND CLEANING APPLICATIONS

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Patent No.
US None
App. No.
17/420,158
Abstract

The present application provides quaternary azeotrope or azeotrope-like compositions comprising trans-dichloroethylene and three or more additional components. Methods of using the compositions provided herein in cleaning, defluxing, deposition, and carrier fluid applications are also provided.

Claims (74)

1 . An azeotrope or azeotrope-like composition, comprising:

i) trans-1,2-dichloroethylene;

ii) a second component selected from a hydrofluoroolefin, a hydrofluoroether, a hydrochlorofluoroolefin, and an alkyl perfluoroalkene ether;

iii) a third component which is a hydrofluorocarbon; and

iv) a fourth component selected from a C 1-6 alcohol, a C 3-6 ketone, a C 5-8 alkane, a C 3-6 cycloalkane, and a C 1-6 alkyl acetate.

2 . The composition of claim 1 , wherein the second component is a hydrofluoroolefin.

3 . The composition of claim 2 , wherein the hydrofluoroolefin is (Z)-1,1,1,4,4,4-hexafluoro-2-butene.

4 . The composition of claim 1 , wherein the second component is a hydrofluoroether.

5 . The composition of claim 4 , wherein the hydrofluoroether is selected from HFE-7000, HFE-7100, HFE-7200, HFE-7300, HFE-347pc-f, and 1,1,1,2,2,3,4,5,5,5-decafluoro-3-methoxy-4-(trifluoromethyl)pentane.

6 . The composition of claim 4 , wherein the hydrofluoroether is 1,1,1,2,2,3,4,5,5,5-decafluoro-3-methoxy-4-(trifluoromethyl)pentane.

7 . The composition of claim 1 , wherein the second component is a hydrochlorofluoroolefin.

8 . The composition of claim 7 , wherein the hydrochlorofluoroolefin is selected from HCFO-1233zd(Z), HCFO-1233zd(E), and HCFO-1233yd(Z).

9 . The composition of claim 1 , wherein the second component is an alkyl perfluoroalkene ether.

10 . The composition of claim 9 , wherein the alkyl perfluoroalkene ether is methyl perfluoroheptene ether.

11 . The composition of claim 10 , wherein methyl perfluoroheptene ether comprises a mixture of about 50 weight percent 5-methoxy perfluoro-3-heptene, about 20 weight percent 3-methoxy perfluoro-3-heptene, about 20 weight percent 4-methoxy perfluoro-2-heptene, and about 8 weight percent 4-methoxy perfluoro-3-heptene.

12 . The composition of claim 11 , wherein the composition comprises about 1 to about 5 weight percent methyl perfluoroheptene ether.

13 . The composition of claim 11 , wherein the composition comprises about 3 to about 5 weight percent methyl perfluoroheptene ether.

14 . The composition of claim 1 , wherein the third component is selected from 1,1,2,2,3,3,4-heptafluorocyclopentane, 1,1,1,3,3-pentafluorobutane, and 1, 1,1,3,3-pentafluoropropane.

15 . The composition of claim 1 , wherein the third component is 1,1,2,2,3,3,4-heptafluorocyclopentane.

16 . The composition of claim 15 , wherein the composition comprises about 10 to about 15 weight percent 1,1,2,2,3,3,4-heptafluorocyclopentane.

17 . The composition of claim 15 , wherein the composition comprises about 11 to about 13 weight percent 1,1,2,2,3,3,4-heptafluorocyclopentane.

18 . The composition of claim 1 , wherein the fourth component is a C 1-6 alcohol.

19 . The composition of claim 18 , wherein the C 1-6 alcohol is selected from methanol, ethanol, and isopropanol.

20 . The composition of claim 18 , wherein the C 1-6 alcohol is ethanol.

21 . The composition of claim 20 , wherein the composition comprises about 1 to about 5 weight percent ethanol.

22 . The composition of claim 20 , wherein the composition comprises about 2 to about 4 weight percent ethanol.

23 . The composition of claim 1 , wherein the fourth component is a C 3-6 ketone.

24 . The composition of claim 23 , wherein the C 3-6 ketone is acetone.

25 . The composition of claim 1 , wherein the fourth component is a C 6-8 alkane.

26 . The composition of claim 25 , wherein the C 6-8 alkane is n-hexane.

27 . The composition of claim 1 , wherein the fourth component is a C 3-6 cycloalkane.

28 . The composition of claim 27 , wherein the C 3-6 cycloalkane is cyclopentane.

29 . The composition of claim 1 , wherein the fourth component is a C 1-6 alkyl acetate.

30 . The composition of claim 29 , wherein the C 1-6 alkyl acetate is ethyl acetate.

31 . The composition of claim 1 , wherein the composition comprises about 75 to about 85 weight percent trans-1,2-dichloroethylene.

32 . The composition of claim 1 , wherein the composition comprises about 79 to about 81 weight percent trans-1,2-dichloroethylene.

33 . The composition of claim 1 , wherein the composition comprises:

i) about 75 to about 85 weight percent trans-1,2-dichloroethylene;

ii) about 1 to about 5 weight percent methyl perfluoroheptene ether;

iii) about 10 to about 15 weight percent 1,1,2,2,3,3,4-heptafluorocyclopentane; and

iv) about 1 to about 5 weight percent ethanol.

34 . The composition of claim 1 , wherein the composition comprises:

i) about 79 to about 81 weight percent trans-1,2-dichloroethylene;

ii) about 3 to about 5 weight percent methyl perfluoroheptene ether;

iii) about 11 to about 13 weight percent 1,1,2,2,3,3,4-heptafluorocyclopentane; and

iv) about 2 to about 4 weight percent ethanol.

35 . The composition of claim 1 , wherein the composition comprises:

i) about 81 weight percent trans-1,2-dichloroethylene;

ii) about 4 weight percent methyl perfluoroheptene ether;

iii) about 12 weight percent 1,1,2,2,3,3,4-heptafluorocyclopentane; and

iv) about 3 weight percent ethanol.

36 . The composition of claim 35 , wherein the composition has a boiling point of about 44° C. to about 46° C. at a pressure of about 101 kPa.

37 . The composition of claim 1 , wherein the composition consists essentially of trans-1,2-dichloroethylene, methyl perfluoroheptene ether, 1,1,2,2,3,3,4-heptafluorocyclopentane, and ethanol.

38 . The composition of claim 1 , wherein the composition consists of trans-1,2-dichloroethylene, methyl perfluoroheptene ether, 1,1,2,2,3,3,4-heptafluorocyclopentane, and ethanol.

39 . The composition of claim 1 , wherein the composition is an azeotrope composition.

40 . The composition of claim 1 , wherein the composition is an azeotrope-like composition.

41 . The composition of claim 1 , wherein the composition comprises:

i) about 75 to about 85 weight percent trans-1,2-dichloroethylene;

ii) about 1 to about 5 weight percent methyl perfluoroheptene ether;

iii) about 10 to about 15 weight percent 1,1,2,2,3,3,4-heptafluorocyclopentane; and

iv) about 1 to about 5 weight percent isopropanol.

42 . The composition of claim 1 , wherein the composition comprises:

i) about 70 to about 80 weight percent trans-1,2-dichloroethylene;

ii) about 5 to about 15 weight percent 1,1,1,2,2,3,4,5,5,5-decafluoro-3-methoxy-4-(trifluoromethyl)pentane;

iii) about 5 to about 10 weight percent 1,1,2,2,3,3,4-heptafluorocyclopentane; and

iv) about 1 to about 5 weight percent n-hexane.

43 . A process for dissolving a solute, comprising contacting and mixing said solute with a sufficient quantity of the composition of claim 1 .

44 . A process of cleaning a surface, comprising contacting the composition of claim 1 with said surface.

45 . A process for removing at least a portion of water from the surface of a wetted substrate, comprising contacting the substrate with the composition of claim 1 , and then removing the substrate from contact with the composition.

46 . The process of claim 45 , wherein composition further comprises at least one surfactant suitable for dewatering or drying the substrate.

47 . A process of depositing a fluorolubricant on a surface, comprising:

a) combining a fluorolubricant and a solvent to form a lubricant-solvent combination, wherein the solvent comprises a composition of claim 1 ;

b) contacting the lubricant-solvent combination with the surface; and

c) evaporating the solvent from the surface to form a fluorolubricant coating on the surface.

Assignments (2)
SECURITY INTEREST Recorded Mar 2, 2022
From: THE CHEMOURS COMPANY FC, LLC
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 059552/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 1, 2021
From: WU, RAYMOND; FRASER, MICHAEL R.; MUSYIMI, HARRISON K; SIMONI, LUKE DAVID
To: THE CHEMOURS COMPANY FC, LLC
Reel/Frame 056730/0347 →