IP Library Granted Patent US 12,577,026
Granted Patent B2
US 12,577,026 · App. 17/433,362 · Granted Mar 17, 2026

Abrasion resistant heat shrinkable multilayer film

Inventors: Prasanna U. Perera (Spartanburg, SC); Sonola Onasanya (Charlotte, NC)
Assignee: Cryovac, LLC
B65D75/004B32B27/08B32B27/306B32B27/327C08K3/36B32B2250/05B32B2250/246B32B2250/40B32B2264/102B32B2307/308B32B2307/31B32B2307/406B32B2307/584B32B2307/72B32B2307/7244B32B2307/732B32B2439/70
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Quick Facts
Patent No.
US 12,577,026
App. No.
17/433,362
Granted
Mar 17, 2026
Kind
B2
Abstract

A multilayer heat-shrinkable film having a sealant layer and skin layer each including a linear low density polyethylene copolymer and a silicon dioxide, at least two substrate layers including an ethylene copolymer; and a core layer including a very low density polyethylene copolymer.

Claims (36)

1 . A multilayer heat-shrinkable film comprising:

a. a sealant layer comprising between 30-49.99 wt % of a homogeneous polyethylene copolymer having a density from 0.91 to 0.93 g/cm 3 , between 50-69.99 wt % ethylene/octene copolymer having a density from 0.93 to 0.95 g/cm 3 , and between 0.01-0.4 wt % of a member selected from the group consisting of natural silica, synthetic silica, ceramic spheres, diatomaceous earth, kaolin, and mica;

b. at least two substrate layers comprising an ethylene/vinyl acetate copolymer;

c. a core layer comprising between 70-90 wt % ethylene/octene copolymer having a density from 0.93 to 0.95 g/cm 3 , and between 10-30 wt % of a very low density ethylene/octene copolymer having a density less than 0.915 g/cm 3 , and

d. a skin layer comprising between 30-39.99 wt % of a homogeneous ethylene/hexene copolymer having a density from 0.91 to 0.93 g/cm 3 , at least 10 wt % of a high density polyethylene homopolymer having a density of at least 0.95 g/cm 3 , and between 50-59.99 wt % ethylene/octene copolymer having a density from 0.93 to 0.95 g/cm 3 , and between 0.01-0.4 wt % of a member selected from the group consisting of natural silica, synthetic silica, ceramic spheres, diatomaceous earth, kaolin, and mica;

wherein the multilayer heat-shrinkable film has an oxygen transmission rate of between 2000 to 9000 cm 3 (STP)/(m 2 -day-1 atm) at 40° C. and 0% relative humidity measured in accordance with ASTM D3985.

2 . The multilayer heat-shrinkable film of claim 1 , wherein the multilayer heat-shrinkable film has a total thickness of between 0.0101-0.0304 mm.

3 . The multilayer heat-shrinkable film of claim 1 , wherein the sealant layer has a thickness of between 15-45% of the total thickness of the multilayer heat-shrinkable film; the skin layer has a thickness of between 15-40% of the total thickness of the multilayer heat-shrinkable film; the core layer has a thickness of between 20-45% of the total thickness of the multilayer heat-shrinkable film; and each of the at least two substrate layers have a thickness of between 5-15% of the total thickness of the multilayer heat-shrinkable film.

4 . The multilayer heat-shrinkable film of claim 1 , wherein the multilayer heat-shrinkable film is a five layer heat-shrinkable film, each of the five layers being distinct from an adjacent layer.

5 . The multilayer heat-shrinkable film of claim 1 , wherein the ethylene/hexene copolymer of the skin layer is a linear low density ethylene/hexene copolymer.

6 . The multilayer heat-shrinkable film of claim 1 , wherein the multilayer heat-shrinkable film is cross linked and biaxially oriented.

7 . The multilayer heat-shrinkable film of claim 1 , wherein the multilayer heat-shrinkable film has a haze of less than 2% measured in accordance with ASTM D1003 and has a gloss from 70% to 90% measured in accordance with ASTM D2457.

8 . A packaged product comprising:

a. a support structure exhibiting a shape;

b. a product situated within the support;

c. a multilayer heat-shrinkable film encapsulating the support thereby isolating the product from an external environment;

the multilayer heat-shrinkable film comprising:

i. a sealant layer comprising between 30-49.99 wt % of a homogeneous polyethylene copolymer having a density from 0.91 to 0.93 g/cm 3 , between 50-69.99 wt % ethylene/octene copolymer having a density from 0.93 to 0.95 g/cm 3 , and between 0.01-0.4 wt % of a member selected from the group consisting of natural silica, synthetic silica, ceramic spheres, diatomaceous earth, kaolin, and mica;

ii. at least two substrate layers comprising an ethylene/vinyl acetate copolymer;

iii. a core layer comprising between 70-90 wt % ethylene/octene copolymer having a density from 0.93 to 0.95 g/cm 3 , and between 10-30 wt % of a very low density ethylene/octene copolymer having a density less than 0.915 g/cm 3 ; and

iv. a skin layer comprising between 30-39.99 wt % of a homogeneous ethylene/hexene copolymer having a density from 0.91 to 0.93 g/cm 3 , at least 10 wt % of a high density polyethylene homopolymer having a density of at least 0.95 g/cm 3 , and between 50-59.99 wt % ethylene/octene copolymer having a density from 0.93 to 0.95 g/cm 3 , and between 0.01-0.4 wt % of a member selected from the group consisting of natural silica, synthetic silica, ceramic spheres, diatomaceous earth, kaolin, and mica;

wherein the multilayer heat-shrinkable film has an oxygen transmission rate of between 2000 to 9000 cm 3 (STP)/(m 2 -day-1 atm) at 40° C. and 0% relative humidity measured in accordance with ASTM D3985.

9 . The packaged product of claim 8 wherein the product is a food product.

10 . The packaged product of claim 8 wherein the support structure is a thermoformed tray comprising polyethylene terephthalate, crystallized polyethylene terephthalate, amorphous polyethylene terephthalate, recycled polyethylene terephthalate, glycol modified polyethylene terephthalate and blends thereof.

11 . The packaged product of claim 8 wherein the multilayer heat-shrinkable film is not perforated.

12 . The packaged product of claim 8 wherein the packaged product has a pass rate of at least 40% Shaker Table Test tested under ASTM D4169 Truck Level I.

13 . A method for packaging a product comprising the steps of:

a. providing a support structure which retains its shape while supporting a product;

b. situating a product within the support;

c. encapsulating the support with a multilayer heat-shrinkable film thereby isolating the product from an external environment;

the multilayer heat-shrinkable film comprising:

i. a sealant layer comprising between 30-49.99 wt % of a homogeneous polyethylene copolymer having a density from 0.91 to 0.93 g/cm 3 , between 50-69.99 wt % ethylene/octene copolymer having a density from 0.93 to 0.95 g/cm 3 , and between 0.01-0.4 wt % of a member selected from the group consisting of natural silica, synthetic silica, ceramic spheres, diatomaceous earth, kaolin, and mica;

ii. at least two substrate layers comprising an ethylene/vinyl acetate copolymer;

iii. a core layer comprising between 70-90 wt % ethylene/octene copolymer having a density from 0.93 to 0.95 g/cm 3 , and between 10-30 wt % of a very low density ethylene/octene copolymer having a density less than 0.915 g/cm 3 , and

iv. a skin layer comprising between 30-39.99 wt % of a homogeneous ethylene/hexene copolymer having a density from 0.91 to 0.93 g/cm 3 , at least 10 wt % of a high density polyethylene homopolymer having a density of at least 0.95 g/cm 3 , and between 50-59.99 wt % ethylene/octene copolymer having a density from 0.93 to 0.95 g/cm 3 , and between 0.01-0.4 wt % of a member selected from the group consisting of natural silica, synthetic silica, ceramic spheres, diatomaceous earth, kaolin, and mica;

wherein the multilayer heat-shrinkable film has an oxygen transmission rate of between 2000 to 9000 cm 3 (STP)/(m 2 -day-1 atm) at 40° C. and 0% relative humidity measured in accordance with ASTM D3985.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 6, 2025
From: PERERA, PRASANNA U.; ONASANYA, SONOLA
To: CRYOVAC, LLC
Reel/Frame 072809/0525 →
SECURITY INTEREST Recorded Oct 31, 2025
From: CRYOVAC, LLC
To: BANK OF AMERICA, N.A., AS AGENT
Reel/Frame 073428/0495 →