IP Library Granted Patent US 11,384,047
Granted Patent B2
US 11,384,047 · App. 17/434,435 · Granted Jul 12, 2022

Method for preparation of decolorized acetoacetylated glycerol with activated carbon

Inventors: Leo Schmid (Ried-Brig, CH); Anja Bierstedt (Visp, CH)
Assignee: ARXADA AG
C07C67/56C07C69/72
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Quick Facts
Patent No.
US 11,384,047
App. No.
17/434,435
Granted
Jul 12, 2022
Kind
B2
Abstract

The invention discloses the use of activated carbon with a mesh size smaller than 80 for the decolorization of acetoacetylated glycerol.

Claims (5)

1. A method for decolorizing acetoacetylated glycerol using activated carbon comprising, contacting the acetoacetylated glycerol with the activated carbon, wherein the activated carbon has a mesh size of smaller than 80.

2. The method according to claim 1 , wherein the amount of activated carbon used for decolorizing the acetoacetylated glycerol is from 1 to 30 wt %, the wt % being based on the weight of acetoacetylated glycerol.

3. The method according to claim 1 , wherein the time of contacting the acetoacetylated glycerol with the activated carbon is from 10 sec to 12 h.

4. The method according to claim 1 , wherein the contacting of the acetoacetylated glycerol with the activated carbon is done at a temperature below the boiling point of acetoacetylated glycerol.

5. The method according to claim 1 , wherein the acetoacetylated glycerol has been prepared by a reaction of glycerol with diketene.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 6, 2022
From: SCHMID, LEO; BIERSTEDT, ANJA
To: ARXADA AG
Reel/Frame 059838/0824 →
CHANGE OF NAME Recorded Dec 4, 2021
From: LONZA SOLUTIONS AG
To: ARXADA AG
Reel/Frame 058414/0403 →