IP Library Granted Patent US 11,913,095
Granted Patent B2
US 11,913,095 · App. 17/504,580 · Granted Feb 27, 2024

Fabrication of metallic parts by additive manufacturing

Inventors: Michael T. Stawovy (Cleveland Heights, OH); Scott D. Ohm (Coldwater, MI); Fahrron C. Fill (Bronson, MI)
Assignee: H.C. STARCK SOLUTIONS EUCLID, LLC
C22C27/04B22F1/103B22F9/026B22F9/04B22F9/082B22F10/00B22F10/14B33Y70/00B22F1/10B22F1/148B22F3/10B22F3/1021B22F10/25B22F10/32B22F10/66B22F2009/041B22F2201/013B22F2202/13B22F2207/13B22F2207/17B22F2301/10B22F2301/15B22F2301/20B22F2301/35B22F2999/00B33Y10/00C22C1/045
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 11,913,095
App. No.
17/504,580
Granted
Feb 27, 2024
Kind
B2
Abstract

In various embodiments, metallic alloy powders are utilized as feedstock, or to fabricate feedstock, utilized in additive manufacturing processes to form three-dimensional metallic parts. Such feedstock includes composite particles each comprising a mixture and/or alloy of a first constituent metal and one or more second constituent metals, where each of the particles comprises a plurality of grains each surrounded by a matrix, the grains comprising the first constituent metal, and the matrix comprising the one or more second constituent metals.

Claims (30)

1. A powder comprising:

a plurality of substantially spherical composite particles each comprising a mixture and/or alloy of a first constituent metal and one or more second constituent metals,

wherein:

the particles have a Hall flow rate ranging from approximately 1 s/50 g to approximately 25 s/50 g,

an outer surface of each of the particles comprises a plurality of grains, each grain being surrounded by a matrix, the grains comprising the first constituent metal, and the matrix comprising the one or more second constituent metals,

the first constituent metal is selected from the list consisting of tungsten, niobium, tantalum, rhenium, molybdenum, iron, nickel, cobalt, vanadium, palladium, zirconium, and yttrium, and

each second constituent metal is different from the first constituent metal and selected from the list consisting of tungsten, niobium, tantalum, rhenium, molybdenum, iron, nickel, cobalt, vanadium, palladium, zirconium, and yttrium.

2. The powder of claim 1 , wherein each of the particles comprises 90% or more of the first constituent metal.

3. The powder of claim 1 , wherein the first constituent metal is tungsten.

4. The powder of claim 1 , wherein the one or more second constituent metals comprise at least one of nickel, iron, or cobalt.

5. The powder of claim 1 , wherein the particles have a particle-size distribution d10 between 2 microns and 8 microns, d50 between 15 microns and 25 microns, and d90 between 50 microns and 70 microns, wherein a particle-size distribution dX of Y denotes that X % of particles have a size less than Y.

6. The powder of claim 1 , wherein a bulk density of the powder is approximately 45% or more of the theoretical density.

7. The powder of claim 1 , wherein the bulk density of the powder is approximately 65% or less of the theoretical density.

8. The powder of claim 1 , wherein a concentration, within the particles, of at least one of sodium, magnesium, phosphorus, sulfur, potassium, calcium, or antimony is less than 10 ppm.

9. A wire preform comprising:

a tube; and

disposed within the tube, a plurality of composite particles each comprising a mixture and/or alloy of a first constituent metal and one or more second constituent metals, wherein each second constituent metal is different from the first constituent metal,

wherein an outer surface of each of the particles comprises a plurality of grains, each grain being surrounded by a matrix, the grains comprising the first constituent metal, and the matrix comprising the one or more second constituent metals.

10. The wire preform of claim 9 , wherein the first constituent metal is selected from the list consisting of tungsten, niobium, tantalum, rhenium, molybdenum, iron, nickel, cobalt, vanadium, palladium, zirconium, and yttrium.

11. The wire preform of claim 10 , wherein each second constituent metal is selected from the list consisting of tungsten, niobium, tantalum, rhenium, molybdenum, iron, nickel, cobalt, vanadium, palladium, zirconium, and yttrium.

12. The wire preform of claim 9 , wherein each second constituent metal is selected from the list consisting of tungsten, niobium, tantalum, rhenium, molybdenum, iron, nickel, cobalt, vanadium, palladium, zirconium, and yttrium.

13. The wire preform of claim 9 , wherein each of the particles comprises 90% or more of the first constituent metal.

14. The wire preform of claim 9 , wherein the first constituent metal is tungsten.

15. The wire preform of claim 9 , wherein the one or more second constituent metals comprise at least one of nickel, iron, or cobalt.

16. The wire preform of claim 9 , wherein the tube comprises one or more metals having a ductility greater than a ductility of the first constituent metal.

17. The wire preform of claim 9 , wherein the tube comprises one or more metals different from the first constituent metal and different from each said second constituent metal.

18. The wire preform of claim 9 , wherein the tube comprises one or more transition metals.

19. The wire preform of claim 9 , wherein the tube comprises the first constituent metal and/or one or more of the second constituent metals.

20. The wire preform of claim 9 , wherein the tube comprises plastic, rubber, or a polymeric material.

21. The wire preform of claim 9 , wherein the tube comprises a material having a melting point less than a melting point of the first constituent metal and less than a melting point of each said second constituent metal.

Assignments (5)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 3, 2026
From: H.C. STARCK SOLUTIONS EUCLID, LLC
To: ELMET TECHNOLOGIES, LLC
Reel/Frame 073679/0340 →
SECURITY INTEREST Recorded Nov 6, 2023
From: H.C. STARCK SOLUTIONS COLDWATER, LLC; H.C. STARCK SOLUTIONS EUCLID, LLC
To: WELLS FARGO BANK, NATIONAL ASSOCIATION
Reel/Frame 065472/0843 →
CHANGE OF NAME Recorded Nov 1, 2023
From: EUCLID FACILITY HOLDINGS, LLC
To: H.C. STARCK SOLUTIONS EUCLID, LLC
Reel/Frame 065415/0762 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 31, 2023
From: H.C. STARCK INC.
To: EUCLID FACILITY HOLDINGS, LLC
Reel/Frame 065402/0594 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 18, 2023
From: STAWOVY, MICHAEL T.; OHM, SCOTT D.; FILL, FAHRRON C.
To: H.C. STARCK INC.
Reel/Frame 063684/0993 →