IP Library Granted Patent US 11,682,530
Granted Patent B2
US 11,682,530 · App. 17/517,830 · Granted Jun 20, 2023

Materials for stabilizing semiconductors and methods of making the same

Inventors: Kai Zhu (Littleton, CO); Fei Zhang (Tianjin, CN); Tao Xu (Naperville, IL)
Assignees: Alliance for Sustainable Energy, LLC; Board of Trustees of Northern Illinois University
H01G9/2009H01G9/0036H10K30/30H10K30/40H10K71/12H10K85/40H10K85/30
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Quick Facts
Patent No.
US 11,682,530
App. No.
17/517,830
Granted
Jun 20, 2023
Kind
B2
Abstract

The present disclosure relates to a device that includes a first layer having an active material and a stabilizing material, where the active material includes a semiconductor, the stabilizing material includes at least one of an oligomer, an elastomer, a polymer, and/or a resin, and the stabilizing material provides to the device an improved performance metric compared to a device constructed of the first layer but constructed of only the active material (i.e., in the absence of the stabilizing material).

Claims (30)

1. A device comprising:

a first layer comprising a perovskite and a stabilizing material; and

a second layer comprising a charge transport material and the stabilizing material, wherein:

the second layer is in physical contact with the first layer,

the stabilizing material comprises at least one of an oligomer, an elastomer, a polymer, or a resin, and

the stabilizing material is present in the first layer at a concentration between 0.0001 wt % and 1.0 wt %.

2. The device of claim 1 , wherein the polymer comprises at least one of silicon, carbon, oxygen, or hydrogen.

3. The device of claim 2 , wherein the polymer comprises at least one of a siloxane, a polyethylene, a polyvinylidene difluoride, or a polyepoxide.

4. The device of claim 3 , wherein the siloxane further comprises at least one of an alkyl group, a hydrogen atom, a halogen atom, an aromatic group, a siloxy group, an acrylate, an epoxy group, or a carbonate group.

5. The device of claim 4 , wherein the alkyl group comprises at least one of a methyl group, an ethyl group, a propyl group, or a butyl group.

6. The device of claim 4 , wherein the aromatic group comprises at least one of an aryl group, a phenyl group, or a benzyl group.

7. The device of claim 3 , wherein the siloxane comprises a polydimethylsiloxane.

8. The device of claim 1 , further comprising:

a third layer, wherein:

the first layer is positioned between the third layer and the second layer, and

at least a portion of the third layer comprises the stabilizing material.

9. The device of claim 8 , further comprising:

a fourth layer, wherein:

the second layer is positioned between the first layer and the fourth layer, and

at least a portion of the fourth layer comprises the stabilizing material.

10. The device of claim 7 , wherein the siloxane further comprises poly(methylhydro-siloxane).

11. The device of claim 1 , wherein the second layer comprises a hole transport material.

12. The device of claim 8 , wherein the third layer comprises an electron transport material.

13. The device of claim 9 , wherein the fourth layer consists essentially of the stabilizing material.

14. The device of claim 1 , further comprising:

a starting power conversion efficiency (PCE) and a final PCE, wherein:

the starting PCE is measured before the device is exposed to a test,

the final PCE is measured after the device is exposed to the test,

the test comprises maintaining the device at a temperature of 55° C., in the absence of light, at a relative humidity between 10% and 20%, for at least 1200 hours, and

the final PCE is at least 80% of the starting PCE.

Assignments (4)
CHANGE OF NAME Recorded Dec 16, 2025
From: ALLIANCE FOR SUSTAINABLE ENERGY, LLC
To: ALLIANCE FOR ENERGY INNOVATION, LLC
Reel/Frame 073993/0276 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 16, 2022
From: XU, TAO
To: BOARD OF TRUSTEES OF NORTHERN ILLINOIS UNIVERSITY
Reel/Frame 060225/0445 →
CONFIRMATORY LICENSE Recorded Mar 30, 2022
From: NATIONAL RENEWABLE ENERGY LABORATORY
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 059448/0279 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 3, 2021
From: ZHU, KAI; ZHANG, FEI
To: ALLIANCE FOR SUSTAINABLE ENERGY, LLC
Reel/Frame 058005/0292 →