IP Library Granted Patent US 11,988,599
Granted Patent B2
US 11,988,599 · App. 17/550,267 · Granted May 21, 2024

Miniature FT-MIR using a MEMS interferometer with a metasurface emitter and detector

Inventor: Dwight W. Swett (Cypress, TX)
Assignee: Saudi Arabian Oil Company
G01N21/35G01N21/3577G01N33/2823G01N2021/3595G01N2201/0221G01N2201/061
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Quick Facts
Patent No.
US 11,988,599
App. No.
17/550,267
Granted
May 21, 2024
Kind
B2
Abstract

A miniature Fourier transform mid-infrared (FT-MIR) spectrometer is provided. The FT-MIR includes a metasurface IR source to emit radiation when heated, a microelectromechanical (MEMS) interferometer, and a metasurface microbolometer to measure an interferogram from the MEMS interferometer, wherein the miniature FT-MIR spectrometer is less than about 20 mm in outer diameter.

Claims (28)

1. A mid-infrared (MIR) spectrometer, comprising:

a metasurface IR source to emit radiation when heated, wherein the metasurface IR source comprises an electrically conductive geometric pattern based on a geometric inversion of the Rhodonea conformal mapping contours; and

a metasurface microbolometer to detect the radiation from the metasurface IR source.

2. The MIR spectrometer of claim 1 , wherein the metasurface IR source comprises an electrically conductive geometric pattern based on a geometric inversion of the Tangent Circles conformal mapping contours.

3. The MIR spectrometer of claim 1 , wherein the metasurface IR source is tuned to emit radiation from about 500 wavenumbers (cm −1 ) to about 2000 cm −1 .

4. The MIR spectrometer of claim 1 , wherein the metasurface IR source comprises a heating filament to heat the metasurface IR source to about 900 K.

5. The MIR spectrometer of claim 1 , wherein the metasurface microbolometer comprises:

a metasurface tuned to adsorb radiation in a range of frequencies in the mid infrared;

a thermometric layer in contact with the metasurface, wherein the thermometric layer changes in resistivity with temperature changes;

a dielectric substrate supporting the thermometric layer and the metasurface; and

a readout integrated circuit to measure a response from the thermometric layer comprising a voltage drop across the contacts of the bridge with a constant bias current.

6. The MIR spectrometer of claim 5 , wherein the metasurface is tuned to adsorb radiation from about 500 wavenumbers (cm −1 ) to about 2000 cm −1 .

7. The MIR spectrometer of claim 5 , wherein the metasurface comprises gold.

8. The MIR spectrometer of claim 5 , wherein the metasurface absorbs light through surface plasmon resonances.

9. The MIR spectrometer of claim 5 , wherein the metasurface is about 120 nm in thickness.

10. The MIR spectrometer of claim 5 , wherein the metasurface is less than 30 nm in thickness.

11. The MIR spectrometer of claim 5 , wherein the metasurface has a diameter of about 150 μm.

12. The MIR spectrometer of claim 5 , wherein the metasurface has a 35% fill factor.

13. The MIR spectrometer of claim 5 , wherein the metasurface has a detectivity (D*) of about 1×10 10 cm*sqrt(Hz)/W at 333 K at a bias current of 75 μA.

14. The MIR spectrometer of claim 5 , wherein the metasurface has a noise equivalent difference temperature (NEDT) of about 1 mK at a bias current of 75 μA.

15. The MIR spectrometer of claim 5 , wherein the thermometric layer comprises undoped vanadium oxide (VO 2 ).

16. The MIR spectrometer of claim 5 , wherein the thermometric layer is about 500 nm in thickness.

17. The MIR spectrometer of claim 5 , wherein the dielectric substrate comprises silicon nitride (Si 3 N 4 ).

18. The MIR spectrometer of claim 5 , wherein the dielectric substrate is about 200 nm in thickness.

19. The MIR spectrometer of claim 5 , wherein the dielectric substrate is about 100 nm in thickness.

20. The MIR spectrometer of claim 5 , wherein the dielectric substrate is separated from the readout integrated circuit by an airgap.

21. The MIR spectrometer of claim 5 , wherein the metasurface microbolometer has a broadband absorption of more than 90% in a wavenumber range of about 1500 to about 600 cm −1 .

22. The MIR spectrometer of claim 1 , wherein the metasurface microbolometer has an absorption bandwidth of 156% of full width half maximum (FWHM) centered on a wavenumber of 1070 cm −1 .

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 1, 2022
From: ARAMCO SERVICES COMPANY
To: SAUDI ARAMCO UPSTREAM TECHNOLOGY COMPANY
Reel/Frame 060066/0887 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 1, 2022
From: SAUDI ARAMCO UPSTREAM TECHNOLOGY COMPANY
To: SAUDI ARABIAN OIL COMPANY
Reel/Frame 060067/0052 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 21, 2021
From: SWETT, DWIGHT W.
To: ARAMCO SERVICES COMPANY
Reel/Frame 058446/0157 →
Continuity (2)
Continuation 17453290 · Nov 2, 2021
Related Publication 20230139316A1 · May 4, 2023
Cited By (1)
US 12,196,936