IP Library Granted Patent US 12,043,733
Granted Patent B2
US 12,043,733 · App. 17/567,599 · Granted Jul 23, 2024

Compositions and articles comprising complexes of 1-methylcyclopropene and α-cyclodextrin

Inventors: Andrzej Wolan (Torun, PL); Mariusz Bosiak (Torun, PL); Marcin Pakulski (Przysiek, PL); Lucyna Czajkowska (Kwidzyn, PL); Katarzyna Anna Guranowska (Grebocin, PL); Roksana Katarzyna Radlowska (Bydgoszcz, PL)
Assignee: Fresh Inset S.A.
C08L5/16A01N25/22C08L39/06C09J7/21C09J7/401C09J9/005C09J11/06C09J2203/334C09J2400/283C09J2405/005
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Quick Facts
Patent No.
US 12,043,733
App. No.
17/567,599
Granted
Jul 23, 2024
Kind
B2
Abstract

Compositions comprising complexes of 1-methylcyclopropene and α-cyclodextrin, and articles including the composition, are provided. Methods for using the compositions and articles in delaying the maturation of fruits, vegetables, and plants are also provided.

Claims (26)

1. A substrate comprising a surface comprising a composition,

wherein the composition comprises:

(i) a complex of 1-methylcyclopropene and α-cyclodextrin; and

(ii) a polymer binder selected from the group consisting of polyvinylpyrrolidone and copolymers thereof, polyvinyl alcohol and copolymers thereof, polyvinyl acetate copolymers, and combinations thereof;

wherein the ratio of polymer binder to complex on a weight to weight basis ranges from about 1:2 to about 4:1;

wherein the polymer binder has a molecular weight ranging from about 5,000 to about 15,000; and

wherein the composition is capable of releasing the 1-methylcyclopropene in the form of a gas when exposed to moisture.

2. The substrate of claim 1 , wherein the substrate comprises a second surface comprising an adhesive.

3. The substrate of claim 1 , wherein the ratio of polymer binder to complex on a weight to weight basis is from about 1:2 to about 3:1.

4. The substrate of claim 1 , wherein the ratio of polymer binder to complex on a weight to weight basis is from about 1:2 to about 2:1.

5. The substrate of claim 1 , wherein the ratio of polymer binder to complex on a weight to weight basis is about 1:1.

6. The substrate of claim 1 , wherein the polymer binder has a molecular weight of about 10,000.

7. The substrate of claim 1 , wherein the composition further comprises a hygroscopic agent.

8. The substrate of claim 7 , wherein the hygroscopic agent is selected from the group consisting of glycerol, glucose, and combinations thereof.

9. The substrate of claim 1 , wherein the composition further comprises a humidity-indicating dye.

10. The substrate of claim 1 , wherein the substrate comprises a paper substrate.

11. The substrate of claim 1 , wherein the substrate comprises a synthetic substrate.

12. The substrate of claim 1 , wherein the 1-methylcyclopropene is present in the composition in an amount of from about 0.825 wt % to about 2.2 wt %.

13. The substrate of claim 1 , wherein the composition has a release profile characterized in that when exposed at room temperature in a sealed vessel to conditions of 85% relative humidity, the composition releases substantially no 1-methylcyclopropene after a time period of at least 1 hour after exposure and thereafter continuously releases 1-methylcyclopropene for at least 5 hours after exposure.

14. The substrate of claim 1 , wherein the composition has a release profile characterized in that when exposed at room temperature in a sealed vessel to conditions of 85% relative humidity, the composition releases substantially no 1-methylcyclopropene after 2 hours.

15. The substrate of claim 1 , wherein the composition has a release profile characterized in that when exposed at room temperature in a sealed vessel to conditions of 85% relative humidity, the composition releases substantially no 1-methylcyclopropene after 3 hours.

16. The substrate of claim 1 , wherein the composition has a release profile characterized in that when exposed at room temperature in a sealed vessel to conditions of 85% relative humidity, the composition releases substantially no 1-methylcyclopropene after a time period of at least 1 hour after exposure and thereafter continuously releases 1-methylcyclopropene for at least 24 hours after exposure.

17. The substrate of claim 1 , wherein the composition has a release profile characterized in that when exposed at room temperature in a sealed vessel to conditions of 85% relative humidity, the composition releases substantially no 1-methylcyclopropene after a time period of at least 3 hours after exposure and thereafter continuously releases 1-methylcyclopropene for at least 24 hours after exposure.

18. The substrate of claim 1 , wherein the composition has a release profile characterized in that when exposed in a sealed vessel to conditions of 80% relative humidity, the composition immediately releases 1-methylcyclopropene and thereafter continuously releases 1-methylcyclopropene for at least 96 hours after exposure.

19. The substrate of claim 1 , wherein the wherein the 1-methylcyclopropene is present in the composition in an amount of from about 0.66 wt % to about 2.2 wt %.

20. The substrate of claim 1 , wherein the substrate comprises a cardboard substrate.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 2, 2023
From: WOLAN, ANDRZEJ; BOSIAK, MARIUSZ; PAKULSKI, MARCIN; CZAJKOWSKA, LUCYNA; GURANOWSKA, KATARZYNA ANNA; RADLOWSKA, ROKSANA KATARZYNA
To: FRESH INSET S.A.
Reel/Frame 063514/0035 →
Priority Claims (3)
PL 425413 · Apr 27, 2018 · national
PL 425414 · Apr 27, 2018 · national
PL 425415 · Apr 27, 2018 · national
Continuity (4)
Continuation 16870333 · May 8, 2020
Continuation 16456128 · Jun 28, 2019
Continuation PCTEP2019060816 · Apr 26, 2019
Related Publication 20220372251A1 · Nov 24, 2022
Cited By (1)
US 12,653,182