IP Library Granted Patent US 12,099,039
Granted Patent B2
US 12,099,039 · App. 17/581,262 · Granted Sep 24, 2024

Method for evaluating embrittlement of amorphous alloy ribbon and test device for evaluating embrittlement of amorphous alloy ribbon

Inventors: Nakao Moritsugu (Tokyo, JP); Hiroshi Takashima (Tokyo, JP)
Assignee: PROTERIAL, LTD.
G01N3/28C22C45/02G01N3/02G01N33/20
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Quick Facts
Patent No.
US 12,099,039
App. No.
17/581,262
Granted
Sep 24, 2024
Kind
B2
Abstract

A new method for evaluating embrittlement of an amorphous alloy ribbon is provided. The method includes: pressing a pressurization member from one side to a plurality of positions of an amorphous alloy ribbon; scattering, in the amorphous alloy ribbon, pressurization portions where the pressurization member is pressed to form indentation; and evaluating embrittlement by the number or distribution of pressurization portions where cracks have occurred.

Claims (25)

1. A method for evaluating embrittlement of an amorphous alloy ribbon, the method comprising:

pressing a pressurization member from one side to a plurality of positions of an amorphous alloy ribbon, wherein an elastic member is placed on a side of the amorphous alloy ribbon opposite to a surface on which the pressurization member is pressed, so as not to hinder a deformation by the pressurization member;

scattering, in the amorphous alloy ribbon, pressurization portions where the pressurization member is pressed to form indentation; and

evaluating embrittlement by the number or distribution of pressurization portions where cracks have occurred.

2. The method for evaluating embrittlement of an amorphous alloy ribbon according to claim 1 , wherein the amorphous alloy ribbon is magnetically adsorbed and fixed, and the pressurization member is pressed.

3. The method for evaluating embrittlement of an amorphous alloy ribbon according to claim 1 , wherein a crack is discriminated by discontinuity of waviness of a surface shape of the pressurization portion.

4. The method for evaluating embrittlement of an amorphous alloy ribbon according to claim 1 , wherein a crack is discriminated from a light transmission state of the pressurization portion.

5. The method for evaluating embrittlement of an amorphous alloy ribbon according to claim 1 , wherein a crack is discriminated by a decrease change in pressurization force of the pressurization member.

6. The method for evaluating embrittlement of an amorphous alloy ribbon according to claim 1 , wherein the amorphous alloy ribbon is manufactured by continuous casting and the amorphous alloy ribbon at least has a length equal to or greater than a circumference length of a casting roll in the continuous casting.

7. The method for evaluating embrittlement of an amorphous alloy ribbon according to claim 1 , wherein the pressurization member comes into contact with the amorphous alloy ribbon and the pressurization member is lowered until a force applied to the pressurization portion becomes a preset value, and when an occurrence of a crack is detected, descending of the pressurization member is stopped and the pressurization member is raised to a predetermined position and the pressurization member is moved to a position of a next pressurization portion.

8. The method for evaluating embrittlement of an amorphous alloy ribbon according to claim 1 , wherein a crack is determined by imaging the pressurization portion using a camera, binarizing a captured image, and applying a threshold value to binarized data.

9. The method for evaluating embrittlement of an amorphous alloy ribbon according to claim 1 , wherein the elastic member comprises a resin having a Shore A hardness of 30 or more and 100 or less and a thickness of 0.5 mm or more and 3.0 mm or less.

10. A test device for evaluating embrittlement of an amorphous alloy ribbon, the test device including:

a measurement table including a plane on which an amorphous alloy ribbon is placed,

an elastic member placed on a side of the amorphous alloy ribbon opposite to a surface on which a pressurization member is pressed, so as not to hinder a deformation by the pressurization member, and

a pressurization device for pressing the pressurization member from one side to a plurality of positions of the amorphous alloy ribbon and scattering, in the amorphous alloy ribbon, pressurization portions where the pressurization member is pressed to form indentation.

11. The test device for evaluating embrittlement of an amorphous alloy ribbon according to claim 10 , the test device wherein the pressurization device can form a crack in at least one of a plurality of the pressurization portions.

12. The test device for evaluating embrittlement of an amorphous alloy ribbon according to claim 10 , wherein the pressurization device is positioned above a plane of the measurement table and can move in a substantially perpendicular direction with respect to a plane of the measurement table.

13. The test device for evaluating embrittlement of an amorphous alloy ribbon according to claim 12 , wherein the pressurization device is further movable on a plane parallel to the plane of the measurement table.

14. The test device for evaluating embrittlement of an amorphous alloy ribbon according to claim 10 , wherein the pressurization member is a rod-shaped member, and the pressurization member is moved in a substantially perpendicular direction with respect to a plane of the measurement table to pressurize the amorphous alloy ribbon with a tip end side of the pressurization member.

15. The test device for evaluating embrittlement of an amorphous alloy ribbon according to claim 14 , wherein the tip end side of the pressurization member is curved or pyramid.

16. The test device for evaluating embrittlement of an amorphous alloy ribbon according to claim 15 , wherein an end portion of the pressurization member has a predetermined vertex-angle within a range of 60° to 130°.

17. The test device for evaluating embrittlement of an amorphous alloy ribbon according to claim 10 , the test device comprising a magnetic adsorbent device for fixing the amorphous alloy ribbon to the measurement table.

18. The test device for evaluating embrittlement of an amorphous alloy ribbon according to claim 10 , wherein the pressurization device includes a load sensor.

19. The test device for evaluating embrittlement of an amorphous alloy ribbon according to claim 18 , the test device that is configured to be able to detect a crack in the amorphous alloy ribbon from pressurization force information obtained based on an electric signal from the load sensor.

Assignments (2)
CHANGE OF NAME Recorded Mar 6, 2023
From: HITACHI METALS, LTD.
To: PROTERIAL, LTD.
Reel/Frame 062958/0525 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 21, 2022
From: MORITSUGU, NAKAO; TAKASHIMA, HIROSHI
To: HITACHI METALS, LTD.
Reel/Frame 058726/0559 →
Priority Claims (3)
JP 2021-009942 · Jan 26, 2021 · national
JP 2021-009943 · Jan 26, 2021 · national
JP 2021-154980 · Sep 24, 2021 · national
Continuity (1)
Related Publication 20220236158A1 · Jul 28, 2022