IP Library Granted Patent US 12,195,337
Granted Patent B2
US 12,195,337 · App. 17/699,144 · Granted Jan 14, 2025

Long and narrow diameter carbon nanotubes and catalysts for producing same

Inventors: Ricardo A. Prada Silvy (Norman, OK); Sathish Kumar Lageshetty (Edmond, OK)
Assignee: Chasm Advanced Materials, Inc.
C01B32/162B01J21/08B01J23/882B01J35/23C01P2004/13
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Quick Facts
Patent No.
US 12,195,337
App. No.
17/699,144
Granted
Jan 14, 2025
Kind
B2
Abstract

A bundle of carbon nanotubes (CNT), comprising a plurality of CNT with lengths of at least about 7 microns, wherein the bundle has a diameter of less than about 12 nm.

Claims (15)

1. A single wall carbon nanotubes (SWCNT) bundle, comprising:

a catalyst construction, comprising:

a metal oxide support;

nanoclusters of active metal nanoparticles, wherein the active metal nanoparticles comprise at least one of cobalt, molybdenum, and nickel; and

a group of SWCNT made up of a plurality of separate, closely-spaced SWCNT grown on the active metal nanoparticles,

wherein most of the SWCNT have diameters of less than one nanometer, wherein a length of the bundle is at least 7 microns, and wherein the bundle has a diameter of less than 12 nm.

2. The SWCNT bundle of claim 1 , wherein at least some of the SWCNT are straight.

3. The SWCNT bundle of claim 1 , wherein at least about 90% of the SWCNT have a diameter of less than 1 nm.

4. The SWCNT bundle of claim 1 , wherein the catalyst construction comprises about the same weight percent of cobalt and molybdenum.

5. The SWCNT bundle of claim 1 , wherein the catalyst construction comprises a molybdenum to cobalt weight ratio of less than 1.

6. The SWCNT bundle of claim 1 , wherein the catalyst construction comprises about 0.1 weight percent cobalt and a molybdenum to cobalt weight ratio of about 0.5.

7. The SWCNT bundle of claim 1 , wherein at least some of the nanoclusters have a size in the range of from about 0.6 nm to about 1.0 nm.

8. The SWCNT bundle of claim 1 with a length to diameter (L/D) aspect ratio of at least about 1,000.

9. The SWCNT bundle of claim 1 , wherein the SWCNT purity is at least about 95%.

10. The SWCNT bundle of claim 1 , wherein the active metal makes up less than 0.2 wt % of the catalyst construction.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 25, 2023
From: CHASM ADVANCED MATERIALS, INC.
To: CHASM SPV LLC
Reel/Frame 063440/0425 →
SECURITY INTEREST Recorded Apr 25, 2023
From: CHASM SPV LLC
To: AON IP ADVANTAGE FUND LP, AS AGENT
Reel/Frame 063440/0545 →
Continuity (2)
Provisional Application 63163389 · Mar 19, 2021
Related Publication 20220298017A1 · Sep 22, 2022
References Cited (3)
US 20090286675A1 · Wei · 2009 [cited by examiner]
Ebbesen et al., Nature, (1992), v358, p. 220-222. [cited by examiner]
Lijima et al., Nature, (1993), v363, p. 603-605. [cited by examiner]