IP Library Granted Patent US 12,458,906
Granted Patent B2
US 12,458,906 · App. 17/726,860 · Granted Nov 4, 2025

Methods of modifying a naturally occurring cannabis raw plant material, a purified cannabis product from a naturally occurring cannabis raw plant material, and a modified cannabis product from a naturally occurring cannabis raw plant material

Inventor: Vincent C. Lombardi (Reno, NV)
Assignee: HIGH SIERRA TECHNOLOGIES, INC.
B01D11/0492A61K36/185A61P1/08B01D11/0288C07B63/00C07C37/80C11B1/10A61K2236/37B01D11/0296B01D2257/70C07C39/19C07C65/03C07D311/78
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Quick Facts
Patent No.
US 12,458,906
App. No.
17/726,860
Granted
Nov 4, 2025
Kind
B2
Abstract

A method of modifying a naturally occurring Cannabis raw plant material, a purified Cannabis product from a naturally occurring Cannabis raw plant material, and a modified Cannabis product from a naturally occurring Cannabis raw plant material. The method includes selectively extracting at least some volatile organic compounds from a naturally occurring Cannabis raw plant material. At least some of a naturally occurring potential cannabinoid content in the Cannabis raw plant material is retained after removal of the at least some of the volatile organic compounds as well as substantially all of the physical structure of the Cannabis raw plant material.

Claims (41)

1 . A method of modifying a naturally occurring Cannabis raw plant material, the method comprising:

selectively extracting at least some volatile organic compounds from a naturally occurring Cannabis raw plant material,

wherein at least some of a naturally occurring potential cannabinoid content in the Cannabis raw plant material is retained after removal of the at least some of the volatile organic compounds.

2 . The method of modifying a naturally occurring Cannabis raw plant material according to claim 1 , wherein the at least some volatile organic compounds are selectively extracted by controlling a pressure in a variable-pressure steam extraction apparatus.

3 . The method of modifying a naturally occurring Cannabis raw plant material according to claim 2 , wherein reducing the pressure decreases the boiling point of the at least some volatile organic compounds in the variable-pressure steam extraction apparatus.

4 . The method of modifying a naturally occurring Cannabis raw plant material according to claim 2 , wherein increasing the pressure increases the boiling point of the at least some volatile organic compounds in the variable-pressure steam extraction apparatus.

5 . The method of modifying a naturally occurring Cannabis raw plant material according to claim 2 , wherein the pressure in the variable-pressure steam extraction apparatus is set to be in a range of 0.0001 to 100 bar.

6 . The method of modifying a naturally occurring Cannabis raw plant material according to claim 2 , wherein the pressure in the variable-pressure steam extraction apparatus is set to be in a range of 0.001 to 15 bar.

7 . The method of modifying a naturally occurring Cannabis raw plant material according to claim 2 , wherein the pressure in the variable-pressure steam extraction apparatus is set to be in a range of 0.001 to 0.99 bar.

8 . The method of modifying a naturally occurring Cannabis raw plant material according to claim 2 , wherein the variable-pressure steam extraction apparatus is a superheating steam extraction apparatus.

9 . The method of modifying a naturally occurring Cannabis raw plant material according to claim 1 , further comprising recovering and drying the Cannabis raw plant material after removal of the at least some volatile organic compounds to form a purified Cannabis product.

10 . The method of modifying a naturally occurring Cannabis raw plant material according to claim 9 , further comprising adding at least one volatile organic compound to the purified Cannabis product to form a modified Cannabis product.

11 . The method of modifying a naturally occurring Cannabis raw plant material according to claim 1 , wherein the at least some volatile organic compounds are selectively extracted by hydrodistillation.

12 . The method of modifying a naturally occurring Cannabis raw plant material according to claim 1 , wherein the at least some volatile organic compounds are selectively extracted by genetically modifying the naturally occurring Cannabis raw plant material.

13 . The method of modifying a naturally occurring Cannabis raw plant material according to claim 1 , wherein the at least some volatile organic compounds are selectively extracted by selectively breeding the naturally occurring Cannabis raw plant material.

14 . The method of modifying a naturally occurring Cannabis raw plant material according to claim 1 , wherein the at least some volatile organic compounds include an unsaturated hydrocarbon.

15 . The method of modifying a naturally occurring Cannabis raw plant material according to claim 1 , wherein the at least some volatile organic compounds include a saturated hydrocarbon.

16 . The method of modifying a naturally occurring Cannabis raw plant material according to claim 1 , wherein the at least some volatile organic compounds includes at least one thiol compound.

17 . The method of modifying a naturally occurring Cannabis raw plant material according to claim 16 , wherein the at least one thiol compound is at least one compound selected from the group consisting of 3-methyl-2-butene-1-thiol, 4-mercapto-4-methylpentan-2-one, 3-mercaptohexan-1-ol and 3-mercaptohexyl acetate.

18 . The method of modifying a naturally occurring Cannabis raw plant material according to claim 17 , wherein the at least one thiol compound is 3-methyl-2-butene-1-thiol.

19 . The method of modifying a naturally occurring Cannabis raw plant material according to claim 1 , wherein at least some of a naturally occurring physical structure in the Cannabis raw plant material is retained after removal of the at least some of the volatile organic compounds.

20 . The method of modifying a naturally occurring Cannabis raw plant material according to claim 1 , wherein the at least some of the naturally occurring potential cannabinoid content in the Cannabis raw plant material is retained such that the purified Cannabis product can be at least one of (i) consumed, (ii) ingested, and (iii) combusted and inhaled, in a manner similar to the naturally occurring Cannabis raw plant material under similar conditions.

21 . A purified Cannabis product from a naturally occurring Cannabis raw plant material, the purified Cannabis product comprising:

cannabinoids; and

a reduced amount of volatile organic compounds relative to the Cannabis raw plant material,

wherein at least one thiol compound has been removed from the Cannabis raw plant material to form the purified Cannabis product, and

at least some of a naturally occurring potential cannabinoid content in the Cannabis raw plant material is retained in the purified Cannabis product after removal of the at least one thiol compound.

22 . A modified Cannabis product from a naturally occurring Cannabis raw plant material, the modified Cannabis product comprising:

cannabinoids; and

at least one volatile organic compound,

wherein at least some volatile organic compounds have been removed from the Cannabis raw plant material to form a purified Cannabis product,

at least one volatile organic compound has been added to the purified Cannabis product to form the modified Cannabis product, and

at least some of a naturally occurring cannabinoid content of the Cannabis raw plant material is retained in the purified Cannabis product after removal of the at least one thiol compound.

23 . A method of extracting at least some volatile organic compounds from a naturally occurring Cannabis raw plant material, the method comprising:

adjusting a pressure of a variable-pressure steam extraction apparatus based on a boiling point of at least one volatile organic compound in the naturally occurring Cannabis raw plant material; and

selectively extracting the at least some volatile organic compounds from the naturally occurring Cannabis raw plant material in the variable-pressure steam extraction apparatus by operating the variable-pressure steam extraction apparatus at the pressure.

24 . The method of extracting at least one volatile organic compound according to claim 23 , wherein reducing the pressure decreases the boiling point of the at least some volatile organic compounds in the variable-pressure steam extraction apparatus.

25 . The method of extracting at least one volatile organic compound according to claim 23 , wherein increasing the pressure increases the boiling point of the at least some volatile organic compounds in the variable-pressure steam extraction apparatus.

26 . The method of extracting at least one volatile organic compound according to claim 23 , wherein the pressure in the variable-pressure steam extraction apparatus is adjusted to be in a range of 0.0001 to 100 bar.

27 . The method of extracting at least one volatile organic compound according to claim 23 , wherein the pressure in the variable-pressure steam extraction apparatus is adjusted to be in a range of 0.001 to 15 bar.

28 . The method of extracting at least one volatile organic compound according to claim 23 , wherein the pressure in the variable-pressure steam extraction apparatus is adjusted to be in a range of 0.001 to 0.99 bar.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 9, 2022
From: LOMBARDI, VINCENT C.
To: HIGH SIERRA TECHNOLOGIES, INC.
Reel/Frame 060152/0236 →
Continuity (6)
Continuation In Part 17098539 · Nov 16, 2020
Continuation 16912031 · Jun 25, 2020
Continuation 16255157 · Jan 23, 2019
Provisional Application 62633478 · Feb 21, 2018
Provisional Application 62620726 · Jan 23, 2018
Related Publication 20220266168A1 · Aug 25, 2022
References Cited (58)
US 6403126B1 · Webster et al. · 2002 [cited by applicant]
US 9044390B1 · Speier · 2015 [cited by applicant]
US 9532593B2 · Turner · 2017 [cited by applicant]
US 9649349B1 · Tucker et al. · 2017 [cited by applicant]
US 9744200B1 · Tucker et al. · 2017 [cited by applicant]
US 9980996B2 · Speier · 2018 [cited by examiner]
US 10821147B2 · Cooper et al. · 2020 [cited by applicant]
US 20050266108A1 · Flockhart et al. · 2005 [cited by applicant]
US 20090035396A1 · De Meijer · 2009 [cited by applicant]
US 20100197962A1 · Makovec et al. · 2010 [cited by applicant]
US 20140107192A1 · Maione et al. · 2014 [cited by applicant]
US 20140298511A1 · Lewis et al. · 2014 [cited by applicant]
US 20150105455A1 · Bjorncrantz · 2015 [cited by applicant]
US 20150297653A1 · Speier · 2015 [cited by applicant]
US 20160250270A1 · Wendschuh et al. · 2016 [cited by applicant]
US 20160300289A1 · Rose · 2016 [cited by applicant]
US 20170060907A1 · Raber et al. · 2017 [cited by applicant]
US 20170189463A1 · Franklin et al. · 2017 [cited by applicant]
US 20170202170A1 · Lewis et al. · 2017 [cited by applicant]
US 20170266153A1 · Levy et al. · 2017 [cited by applicant]
US 20170273349A1 · Moore · 2017 [cited by applicant]
US 20180296616A1 · Rivas · 2018 [cited by applicant]
US 20190192993A1 · Levy et al. · 2019 [cited by applicant]
EP 1385595B1 · 2012 [cited by applicant]
WO 2016138505A1 · 2016 [cited by applicant]
WO 2017053731A1 · 2017 [cited by applicant]
WO 2017100369A1 · 2017 [cited by applicant]
WO 2017214529A1 · 2017 [cited by applicant]
WO 2018044953A1 · 2018 [cited by applicant]
WO 2018160827A1 · 2018 [cited by applicant]
Feb. 14, 2023 Office Action issued in European Patent Application No. 19 743 904.5. [cited by applicant]
Jul. 13, 2022 Office Action issued in Canadian Patent Application No. 3,031,123. [cited by applicant]
May 28, 2019 International Search Report issued in International Patent Application No. PCT/US19/14778. [cited by applicant]
May 28, 2019 Written Opinion of the International Searching Authority issued in International Patent Application No. PCT/US19/14778. [cited by applicant]
Dekker, Victoria. “Customize Your Cannabis Experience With Terpenes —Wherever You Are”, Civilized, (2017), https://www.civilized.life/articles/cannabis-terpenes-experience/. [cited by applicant]
Sievers, A. F. et al., “Methods of Extracting Volatile Oils From Plant Material and the Production of Such Oils in the United States”, Technical Bulletin, No. 16, (1928), pp. 1-28. [cited by applicant]
Babiker, Tayseer. “Charactization of Constituents of Catullus Colocynths Fixed Oil and Its Biological Activity”, Sudan University of Science and Technology, (2017), pp. 1-49. [cited by applicant]
McPartland, John et al., “Cannabis and Cannabis Extracts: Greater Than the Sum of Their Parts?”, Journal of Cannabis Therapeutics, vol. 1, (2008), pp. 103-132. [cited by applicant]
Mar. 25, 2020 International Preliminary Report on Patentability issued in International Patent Application No. PCT/US2019/014778. [cited by applicant]
Jan. 18, 2021 Office Action issued in Canadian Patent Application No. 3,031,123. [cited by applicant]
GoldLeaf Scientific, “Cannabis Terpene Extraction and Discussion”, YouTube (available at: https://www.youtube.com/watch?v=nB9LvsxCL4Q&t=243s), Apr. 27, 2018. [cited by applicant]
Nov. 3, 2021 Office Action issued in Canadian Patent Application No. 3,031,123. [cited by applicant]
Nov. 26, 2021 Protest issued in Canadian Patent Application No. 3,031,123. [cited by applicant]
Stangel, Matt, “We Tested the New Terpene Concentrates That Make Your Weed Tastier”, https://www.wweek.com/cannabis/2017/03/29/we-tested-the-new-terpene-concentrates-that-make-your-weed-tastier/, Mar. 29, 2017 (accessed… [cited by applicant]
Herb, “Say Hello to Odorless Marijuana and Tasteless Cannabutter. Will This Mean Big Problems for Enforcement?”, https://herb.co/news/culture/say-hello-to-odorless-marijuana-and-tasteless-cannabutter/, May 30, 2015 (acc… [cited by applicant]
Adams, Mike, “MediJean Develops Odorless Weed”, https://dopechef.com/2014/04/medijean-develops-odorless-weed/, Apr. 3, 2014 (accessed Nov. 15, 2021). [cited by applicant]
Briggs, David, “How to make (nearly) odorless/tasteless cannabis”, https://www.papakief.com/2010/11/how-to-make-nearly-odorlesstasteless.html, Nov. 16, 2010 (accessed Nov. 15, 2021). [cited by applicant]
“Outdoor Marijuana Breeding”, https://growlode.com/cannabis/blog/2017/04/05/breeding/, Apr. 5, 2017 (accessed Nov. 15, 2021). [cited by applicant]
YouTube Video, “Essential oil extraction from fresh Blue Dream Flowers”, https://www.youtube.com/watch?v=XseRGjpYDrM, Golden Beaver Farms, Jan. 29, 2017. [cited by applicant]
YouTube Video, “Cannabis Chef Invents Way to Neutralize the Smell and Taste of Marijuana [INSIGHTS]”, https://www.youtube.com/watch?v=qwu2NcugkG4″, Jeff the 420 Chef, Mar. 31, 2015. [cited by applicant]
YouTube Video, “Steam Distillation of Live Marijuana”, https://www.youtube.com/watch?v=NFkk4kYGg1Y, Golden Beaver Farms, Feb. 13, 2017. [cited by applicant]
YouTube Video, “Nitrogen Assisted Steam Distillation of Cannabis”, https://www.youtube.com/watch?v=vIRbvqhVv2Y, Golden Beaver Farms, Apr. 29, 2017. [cited by applicant]
YouTube Video, “Cannabis Essential Oil Steam Extraction”, https://www.youtube.com/watch?v=ds0cl6nSODE, Eden Labs, Mar. 26, 2014. [cited by applicant]
YouTube Video, “Steam distilled cannabis essential oil NOT THC-Terpenes! only”, https://www.youtube.com/watch?v=U-16M5cHyOo, Coreymillia 710, Nov. 28, 2012. [cited by applicant]
Dec. 22, 2021 Extended European Search Report issued in European Patent Application No. 19743904.5. [cited by applicant]
Starks, Michael, “Marijuana Chemistry Genetics, Processing & Potency,” Sep. 1, 1993, 206 pages, https://catnews.org. [cited by applicant]
Mar. 31, 2023 Office Action issued in Canadian Patent Application No. 3,031,123. [cited by applicant]
Sep. 8, 2023 Notice of Allowance issued in Canadian Patent Application No. 3,031,123. [cited by applicant]