IP Library Granted Patent US 12,558,310
Granted Patent B2
US 12,558,310 · App. 17/758,811 · Granted Feb 24, 2026

Dosage form with sustained release melatonin pellets

Inventors: Syed M. Shah (Boca Raton, FL); Daniel Hassan (Boca Raton, FL)
Assignee: Societe des Produits Nestle S.A.
A61K9/0053A61K9/0056A61K9/0095A61K9/2054A61K9/48A61K9/5047A61K9/5078A61K31/4045
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Quick Facts
Patent No.
US 12,558,310
App. No.
17/758,811
Granted
Feb 24, 2026
Kind
B2
Abstract

A composition comprises a therapeutically effective oral pharmaceutical dosage form. The dosage form includes an aqueous carrier material having an acidic pH and a plurality of individual pellets having a first dose of melatonin therein. The individual pellets comprises (i) a solid core; (ii) an active coating over the solid core, the active coating including melatonin and a hydrophilic binder; and (iii) an enteric coating over the active coating. A dissolution pH of the enteric coating is higher than the acidic pH of the aqueous carrier material.

Claims (33)

1 . A composition comprising a therapeutically effective oral pharmaceutical dosage form comprising:

(a) an aqueous carrier material having an acidic pH; and

(b) a plurality of individual pellets having a first dose of melatonin therein, the individual pellets comprising (i) a solid core; (ii) an active coating over the solid core, the active coating including melatonin and a hydrophilic binder; and (iii) an enteric coating over the active coating, a dissolution pH of the enteric coating being higher than the acidic pH of the aqueous carrier material,

the individual pellets further comprising a separation coating over the active coating, a subcoat between over the separation coating, and enteric coating over the subcoat,

wherein the subcoat includes a hydrogel-forming polymer and an acid, the acid imparting a pH of 0.1 to 4.4 to the hydrogel-forming polymer, and

the separation coating separates the acid from the melatonin, wherein the dosage form is a beverage or gummy.

2 . The composition of claim 1 , wherein the melatonin is a powder having a median melatonin particle size of 5 μm to 40 μm.

3 . The composition of claim 1 , wherein the aqueous carrier material includes a second dose of melatonin therein and dosage form releases the second dose of melatonin into the subject's oral cavity and stomach.

4 . The composition of claim 1 , wherein the dosage form is a beverage.

5 . The composition of claim 1 , wherein the dosage form is a gummy and the aqueous carrier material is a gummy gelling agent.

6 . The composition of claim 1 , wherein the aqueous carrier material is hydroxypropyl methylcellulose, the solid core is a microcrystalline cellulose bead having a diameter of 0.1 to 2 mm, the hydrophilic binder includes hydroxypropyl methylcellulose, the melatonin is a powder having a median melatonin particle size of 5 μm to 40 μm lodged in the hydrophilic binder, the separation coating includes hydroxypropyl methylcellulose, the hydrogel-forming polymer includes hydroxypropyl methylcellulose, the acid includes citric acid, and the separation coating includes hydroxypropyl methylcellulose.

7 . A method comprising administering a therapeutically effective amount of an oral pharmaceutical dosage form to a patient in need thereof, the dosage form comprising:

(a) an aqueous carrier material having an acidic pH; and

(b) a plurality of individual pellets having a first dose of melatonin therein, the individual pellets comprising (i) a solid core; (ii) an active coating over the solid core, the active coating including melatonin and a hydrophilic binder; and (iii) an enteric coating over the active coating, a dissolution pH of the enteric coating being higher than the acidic pH of the aqueous carrier material,

the individual pellets further comprising a separation coating over the active coating, a subcoat between over the separation coating, and enteric coating over the subcoat,

wherein the subcoat includes a hydrogel-forming polymer and an acid, the acid imparting a pH of 0.1 to 4.4 to the hydrogel-forming polymer, and

the separation coating separates the acid from the melatonin, wherein the dosage form is a beverage or gummy.

8 . The method of claim 7 , wherein the melatonin is a powder having a median melatonin particle size of 5 μm to 40 μm.

9 . The method of claim 7 , wherein the aqueous carrier material includes a second dose of melatonin therein and dosage form releases the second dose of melatonin into the subject's oral cavity and stomach.

10 . The method of claim 7 , wherein the dosage form is a beverage and.

11 . The method of claim 7 , wherein the dosage form is a gummy and the aqueous carrier material is a gummy gelling agent.

12 . The method of claim 7 , wherein the aqueous carrier material is hydroxypropyl methylcellulose, the solid core is a microcrystalline cellulose bead having a diameter of 0.1 to 2 mm, the hydrophilic binder includes hydroxypropyl methylcellulose, the melatonin is a powder having a median melatonin particle size of 5 μm to 40 μm lodged in the hydrophilic binder, the separation coating includes hydroxypropyl methylcellulose, the hydrogel-forming polymer includes hydroxypropyl methylcellulose, the acid includes citric acid, and the separation coating includes hydroxypropyl methylcellulose.

13 . The method of claim 7 , wherein the dosage form is therapeutically effective for assisting the patient to sleep.

14 . A method comprising:

combining an aqueous carrier material with a plurality of individual pellets to form a therapeutically effective oral pharmaceutical dosage form;

the aqueous carrier material having an acidic pH; and

the a plurality of individual pellets having a first dose of melatonin therein, the individual pellets comprising (i) a solid core; (ii) an active coating over the solid core, the active coating including melatonin and a hydrophilic binder; and (iii) an enteric coating over the active coating, a dissolution pH of the enteric coating being higher than the acidic pH of the aqueous carrier material,

the individual pellets further comprising a separation coating over the active coating, a subcoat between over the separation coating, and enteric coating over the subcoat,

wherein the subcoat includes a hydrogel-forming polymer and an acid, the acid imparting a pH of 0.1 to 4.4 to the hydrogel-forming polymer, and

the separation coating separates the acid from the melatonin, wherein the dosage form is a beverage or gummy.

15 . The method of claim 14 , wherein the melatonin is a powder having a median melatonin particle size of 5 μm to 40 μm.

16 . The method of claim 14 , wherein the aqueous carrier material includes a second dose of melatonin therein and dosage form releases the second dose of melatonin into the subject's oral cavity and stomach.

17 . The method of claim 14 , wherein the dosage form is a gummy and the aqueous carrier material is a gummy gelling agent.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 21, 2025
From: SHAH, SYED M.; HASSAN, DANIEL
To: PHYSICIAN'S SEAL, LLC
Reel/Frame 072619/0235 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 21, 2025
From: ZX PHARMA LLC; CARET PHARMA LLC; PHYSICIAN'S SEAL LLC; IM HEALTHSCIENCE LLC
To: SOCIETE DES PRODUITS NESTLE S.A.
Reel/Frame 072622/0912 →
Continuity (2)
Provisional Application 62962574 · Jan 17, 2020
Related Publication 20230045118A1 · Feb 9, 2023
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