IP Library Granted Patent US 12,313,529
Granted Patent B2
US 12,313,529 · App. 17/792,115 · Granted May 27, 2025

Fluid analyzer with self-check, leak detection, and adjustable gain

Inventors: H. T. Stinson (San Diego, CA); Rudy Bermudez (San Diego, CA); Mark Bermal (San Diego, CA); Jeremy Rowlette (Escondido, CA); David Francis Arnone (Mountain View, CA); Edeline Fotheringham (San Diego, CA); Ronald Arp (Ramona, CA)
Assignee: Daylight Solutions, Inc.
G01N21/276G01N21/39G01N29/30G01N30/74G01N2030/027
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Quick Facts
Patent No.
US 12,313,529
App. No.
17/792,115
Granted
May 27, 2025
Kind
B2
Abstract

A fluid analyzer ( 214 ) that analyzes a sample ( 12 ) includes an analyzer frame ( 236 ); a test cell assembly ( 242 ) that receives the sample ( 12 ); a laser assembly ( 238 ) that generates a laser beam ( 239 A) a signal detector assembly ( 232 ) and a self-check assembly ( 230 ). The self-check assembly ( 230 ) includes (i) a check frame ( 230 A); (ii) a check substance ( 230 E) with known spectral characteristics; and (iii) a check frame mover ( 230 B) that selectively moves the check frame ( 230 A) between a self-check position ( 231 B) and a test position ( 231 A) relative to the analyzer frame ( 236 ). In the self-check position ( 231 B), the laser beam ( 239 A) is directed through the check substance ( 230 E) to evaluate the performance of the fluid analyzer ( 214 ). In the test position ( 231 A), the laser beam ( 239 A) is directed through the sample ( 12 ) in the test cell assembly ( 242 ) to evaluate the sample ( 12 ).

Claims (25)

1. A fluid analyzer that analyzes a sample, the fluid analyzer comprising:

a test cell assembly that receives the sample;

a laser assembly that generates a tunable laser beam that is directed through the test cell assembly, the laser assembly being tunable over a tunable range; and

a signal detector assembly that collects a test signal light transmitted through the test cell assembly, wherein a signal gain setting of the signal detector assembly is adjusted as the laser assembly is tuned over at least a portion of the tunable range.

2. The fluid analyzer of claim 1 further comprising a reference detector assembly; and a splitter element that splits a portion of the laser beam and directs the portion of laser beam at the reference detector assembly; wherein a reference gain setting of the reference detector assembly is adjusted as the laser is tuned over at least a portion of the tunable range.

3. The fluid analyzer of claim 2 wherein the reference gain setting of the reference detector assembly is adjusted as the laser is tuned over at least a portion of the tunable range as a function of the absorbance of the sample; and the signal gain setting of the signal detector assembly is adjusted as the laser is tuned over at least a portion of the tunable range as a function of the absorbance of the sample.

4. The fluid analyzer of claim 2 wherein the reference gain setting of the reference detector assembly is optimized for the magnitude of the light that is expected to be received by the reference detector assembly as the laser beam is tuned.

5. The fluid analyzer of claim 1 wherein the signal gain setting of the signal detector assembly is adjusted as the laser is tuned over at least a portion of the tunable range as a function of the absorbance of the sample.

6. The fluid analyzer of claim 1 wherein the signal gain setting of the signal detector assembly is optimized for the magnitude of the light that is expected to be received by the signal detector assembly as the laser beam is tuned.

7. The fluid analyzer of claim 1 further comprising a leak detection assembly that detects a leak in the test cell assembly.

8. The fluid analyzer of claim 7 wherein the leak detection assembly includes a reservoir that receives sample leaking from the test cell assembly and a leak sensor that detects when there is sufficient sample in the reservoir.

9. A method for analyzing a sample comprising:

providing a test cell assembly that receives the sample;

generating a tunable laser beam that is directed through the test cell assembly with a laser assembly that is tunable over a tunable range;

collecting a test signal light transmitted through the test cell assembly with a signal detector assembly; and

adjusting a signal gain setting of the signal detector assembly while the laser assembly is tuned over at least a portion of the tunable range and the test signal light is collected with the signal detector assembly.

10. The method of claim 9 further comprising providing a reference detector assembly; splitting a portion of the laser beam and directing the portion of laser beam at the reference detector assembly with a splitter element; and adjusting a reference gain setting of the reference detector assembly as the laser is tuned over at least a portion of the tunable range.

11. The method of claim 10 wherein adjusting a reference gain setting includes adjusting the reference gain setting as the laser is tuned over a portion of the tunable range as a function of the absorbance of the sample; and wherein the step of adjusting a signal gain setting includes adjusting the signal gain setting as the laser is tuned over at least a portion of the tunable range as a function of the absorbance of the sample.

12. The method of claim 10 wherein adjusting a reference gain setting of the reference detector assembly including adjusting to optimized for the magnitude of the light that is expected to be received by the reference detector assembly as the laser beam is tuned.

13. The method claim 9 wherein adjusting a signal gain setting includes adjusting the signal gain setting as the laser is tuned over at least a portion of the tunable range as a function of the absorbance of the sample.

14. The method of claim 9 wherein adjusting a signal gain setting includes optimizing the signal gain setting for the magnitude of the light that is expected to be received by the signal detector assembly as the laser beam is tuned.

15. The method of claim 9 further comprising detecting a leak in the test cell assembly with a leak detection assembly.

16. The method of claim 15 wherein detecting a leak includes receiving any sample leaking from the test cell assembly with a reservoir positioned below the test cell assembly, and detecting when there is sufficient sample in the reservoir with a leak sensor.

17. The method of claim 9 further comprising (i) providing a check frame; (ii) coupling a check substance to the check frame; and (iii) selectively moving the check frame between a self-check position and a test position relative to the analyzer frame with a check frame mover; wherein in the self-check position, the laser beam is directed through the check substance to create a check signal light that is collected by the signal detector assembly to evaluate the performance of the fluid analyzer; and wherein in the test position, the laser beam is directed through the sample in the test cell assembly to create a test signal light that is collected by the signal detector assembly to evaluate the sample.

18. The fluid analyzer of claim 1 comprising a self-check assembly that includes (i) a check frame; (ii) a check substance coupled to the check frame; and (iii) a check frame mover that selectively moves the check frame between a self-check position and a test position relative to the analyzer frame; wherein in the self-check position, the laser beam is directed through the check substance to create a check signal light that is collected by the signal detector assembly to evaluate the performance of the fluid analyzer; and wherein in the test position, the laser beam is directed through the sample in the test cell assembly to create a test signal light that is collected by the signal detector assembly to evaluate the sample.

Assignments (1)
LICENSE Recorded Feb 3, 2026
From: DAYLIGHT SOLUTIONS, INC.
To: QUANTINUUM, LLC
Reel/Frame 074623/0515 →