IP Library Granted Patent US 12,370,169
Granted Patent B2
US 12,370,169 · App. 17/821,146 · Granted Jul 29, 2025

Small molecule Bcl-2 functional converters as cancer therapeutics

Inventors: Siva K. Kolluri (Corvallis, OR); Prasad R. Kopparapu (Houston, TX); Martin Pearce (Independence, OR)
Assignee: Oregon State University
A61K31/341A61K31/167A61K38/16A61K45/06
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Quick Facts
Patent No.
US 12,370,169
App. No.
17/821,146
Granted
Jul 29, 2025
Kind
B2
Abstract

Methods for inducing growth inhibition or apoptosis of Bcl-2-expressing cells and treatments of Bcl-2 expressing cancers are provided. Additionally, assays for agents that can induce apoptosis of Bcl-2 expressing cells are disclosed.

Claims (31)

1. A method of treating Bcl-2-expressing cancer, comprising targeting the Bcl-2 protein in a cancer cell of a subject by administering to the subject a therapeutically effective amount of a compound of formula (III):

or a tautomer, hydrate, or salt thereof,

wherein:

Ar 1 is optionally substituted C6-C10 aryl or optionally substituted C5-C10 heteroaryl;

R 1 and R 2 are independently H, halogen, optionally substituted C1-C8 alkyl, optionally substituted C1-C8 alkenyl, optionally substituted C1-C8 alkynyl, O (C1-C8 alkyl), or C (O) NHR, wherein R is optionally substituted C1-C8 alkyl, optionally substituted C6-C10 aryl, or optionally substituted C5-C10 heteroaryl; or together with the carbon atoms to which each is attached, R 1 and R 2 form an optionally substituted 6-membered cycle;

Y is COOH, CONH 2 , optionally substituted C6-C10 aryl, optionally substituted C5-C10 heteroaryl, or C (O) X; and

X is optionally substituted C6-C10 aryl, or optionally substituted C3-C10 heteroaryl.

2. The method of claim 1 , wherein the compound is selected from the group consisting of:

2-[(2-methoxy-5-nitrobenzyl)thio]-3-phenyl-5,6,7,8-tetrahydro[1]benzothieno[2,3-d]pyrimidin-4 (3H)-one;

2-{[2-(4-chlorophenyl)-2-oxoethyl]thio}-5,6-dimethyl-3-phenylthieno[2,3-d]pyrimidin-4 (3H)-one;

5,6-dimethyl-2-{[2-(4-nitrophenyl)-2-oxoethyl]thio}-3-phenylthieno[2,3-d]pyrimidin-4 (3H)-one;

2-{[2-oxo-2-(2-thienyl)ethyl]thio}-3-phenyl-5,6,7,8-tetrahydro[1]benzothieno[2,3-d]pyrimidin-4 (3H)-one;

2-[(4-nitrobenzyl)thio]-3-phenyl-5,6,7,8-tetrahydro[1]benzothieno[2,3-d]pyrimidin-4 (3H)-one;

2-(benzylthio)-3-phenyl-5,6,7,8-tetrahydro[1]benzothieno[2,3-d]pyrimidin-4 (3H)-one;

2-[(4-methoxybenzyl)thio]-3-phenyl-5,6,7,8-tetrahydro[1]benzothieno[2,3-d]pyrimidin-4 (3H)-one;

{[3-(4-ethoxyphenyl)-4-oxo-3,4,5,6,7,8-hexahydro[1]-benzothieno[2,3-d]pyrimidin-2-yl]thio}acetic acid;

2-{[3-(4-ethoxyphenyl)-4-oxo-3,4,5,6,7,8-hexahydro[1]benzothieno[2,3-d]pyrimidin-2-yl]thio}acetamide;

4-({[3-(4-methoxyphenyl)-4-oxo-3,4,5,6,7,8-hexahydro[1]benzothieno[2,3-d]pyrimidin-2-yl]thio}methyl)benzoic acid; and

7-tert-butyl-2-[(4-methoxybenzyl)thio]-3-phenyl-5,6,7,8-tetrahydro[1]benzothieno[2,3-d]pyrimidin-4 (3H)-one;

or a tautomer, hydrate, or salt thereof.

3. A method of treating Bcl-2-expressing cancer-in a subject, comprising administering to the subject in need of cancer treatment, a therapeutically effective amount of 2-[(2-methoxy-5-nitrobenzyl)thio]-3-phenyl-5,6,7,8-tetrahydro[1]benzothieno[2,3-d]pyrimidin-4 (3 H)-one, 2-{[2-(4-chlorophenyl)-2-oxoethyl]thio}-5,6-dimethyl-3-phenylthieno[2,3-d]pyrimidin-4 (3H)-one;

5,6-dimethyl-2-{[(2-methyl-1,3-thiazol-4-yl)methyl]thio}-3-phenylthieno[2,3-d]pyrimidin-4 (3H)-one;

5,6-dimethyl-2-{[2-(4-nitrophenyl)-2-oxoethyl]thio}-3-phenylthieno[2,3-d]pyrimidin-4 (3H)-one;

2-{[2-(4-fluorophenoxy)ethyl]thio}-5,6-dimethyl-3-phenylthieno[2,3-d]pyrimidin-4 (3H)-one;

2-{[2-oxo-2-(2-thienyl)ethyl]thio}-3-phenyl-5,6,7,8-tetrahydro[1]benzothieno[2,3-d]pyrimidin-4 (3H)-one;

2-[(4-nitrobenzyl)thio]-3-phenyl-5,6,7,8-tetrahydro[1]benzothieno[2,3-d]pyrimidin-4 (3H)-one;

2-(benzylthio)-3-phenyl-5,6,7,8-tetrahydro[1]benzothieno[2,3-d]pyrimidin-4 (3H)-one;

2-[(4-methoxybenzyl)thio]-3-phenyl-5,6,7,8-tetrahydro[1]benzothieno[2,3-d]pyrimidin-4 (3H)-one;

{[3-(4-ethoxyphenyl)-4-oxo-3,4,5,6,7,8-hexahydro[1]-benzothieno[2,3-d]pyrimidin-2-yl]thio} acetic acid;

2-{[3-(4-ethoxyphenyl)-4-oxo-3,4,5,6,7,8-hexahydro[1]benzothieno[2,3-d]pyrimidin-2-yl]thio} acetamide;

4-({[3-(4-methoxyphenyl)-4-oxo-3,4,5,6,7,8-hexahydro[1]benzothieno[2,3-d]pyrimidin-2-yl]thio} methyl)benzoicacid; 7-tert-butyl-2-[(4-methoxybenzyl)thio]-3-phenyl-5,6,7,8-tetrahydro[1]benzothieno[2,3-d]pyrimidin-4 (3H)-one; or a tautomer, hydrate, or salt thereof.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 3, 2023
From: KOLLURI, SIVA K.; KOPPARAPU, PRASAD R.; PEARCE, MARTIN
To: OREGON STATE UNIVERSITY
Reel/Frame 062258/0575 →
Continuity (3)
Continuation 16465971
Provisional Application 62428864 · Dec 1, 2016
Related Publication 20230129487A1 · Apr 27, 2023
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