IP Library Granted Patent US 11,746,413
Granted Patent B2
US 11,746,413 · App. 17/829,007 · Granted Sep 5, 2023

Chemical delivery system and method of operating the chemical delivery system

Inventors: David James Eldridge (Liberty Hill, TX); David Peters (Kingsland, TX); Robert Wright, Jr. (Newtown, CT); Bryan C. Hendrix (Danbury, CT); Scott L. Battle (Cedar Park, TX); John Gregg (Marble Falls, TX)
Assignee: ENTEGRIS, INC.
C23C16/4487C23C16/45512C23C16/45523C23C16/45525C23C16/45561C23C16/52
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Quick Facts
Patent No.
US 11,746,413
App. No.
17/829,007
Granted
Sep 5, 2023
Kind
B2
Abstract

A chemical delivery system includes a bulk container, a run/refill chamber, a first conduit and a second conduit. The bulk container stores a precursor. The run/refill chamber includes a plurality of spaced tubes having a plurality of surfaces for receiving the precursor in vapor form and storing the precursor in solid form. The first conduit connects the bulk container to the run/refill chamber for transporting the precursor from the bulk container to the run/refill chamber in vapor form. The second conduit connects the run/refill chamber to a deposition chamber for transporting the precursor from the run/refill chamber to the deposition chamber in vapor form.

Claims (26)

1. A method of operating a chemical delivery system comprising at least one bulk container, at least one run/refill chamber, and at least one deposition chamber, the method comprising: storing a precursor in at least one of the bulk containers; transporting the precursor in vapor form from the bulk container to a first run/refill chamber; receiving the precursor in vapor form in the first run/refill chamber; condensing and storing the precursor in solid form in the first run/refill chamber; causing sublimation of the solid precursor within the first run/refill chamber; and transporting the sublimed precursor in vapor form from the first run/refill chamber to a first deposition chamber, wherein at least one of the run/refill chambers includes a plurality of spaced tubes having a plurality of surfaces configured to receive the precursor in vapor form and store the precursor in solid form.

2. The method of claim 1 further comprising:

transporting the precursor in vapor form from the bulk container to a second run/refill chamber;

receiving the precursor in vapor form in the second run/refill chamber; and condensing and storing the precursor in solid form in the second run/refill chamber.

3. The method of claim 2 , wherein the precursor is received in vapor form in the second run/refill chamber while the solid precursor is sublimed within the first run/refill chamber.

4. The method of claim 2 , further comprising:

causing sublimation of the solid precursor within the second run/refill chamber; and

transporting the sublimed precursor in vapor form from the second run/refill chamber to the first deposition chamber.

5. The method of claim 4 , wherein the solid precursor is sublimed within the second run/refill chamber while the precursor is received in vapor form in the first run/refill chamber.

6. The method of claim 2 , further comprising:

causing sublimation of the solid precursor within the second run/refill chamber; and transporting the sublimed precursor in vapor form from the second run/refill chamber to a second deposition chamber.

7. The method of claim 2 , wherein transporting the precursor in vapor form from the bulk container to the first run/refill chamber alternates with transporting the precursor in vapor form from the bulk container to the second run/refill chamber.

8. The method of claim 1 , wherein the precursor stored in the bulk container is in a solid form in the bulk container.

9. The method of claim 1 , wherein transporting the precursor in vapor form comprises heating the bulk container to sublimate the precursor and transporting the vapor through a heated conduit.

10. The method of claim 1 , wherein storing the precursor in solid form includes storing the precursor in a fabrication area, and storing the precursor in the bulk container includes storing the precursor outside the fabrication area.

11. The method of claim 1 , wherein

transporting the precursor in vapor form from the bulk container to the first run/refill chamber comprises heating the bulk container and transporting the vapor in a first heated conduit;

condensing and storing the precursor in solid form in the first run/refill chamber comprises cooling the first run/refill chamber; and

transporting the sublimed precursor in vapor form from the first run/refill chamber to a first deposition chamber comprises heating the first run/refill chamber and transporting the vapor in a second heated conduit.

12. A method of operating a chemical delivery system comprising at least one bulk container, multiple run/refill chambers, and at least one deposition chamber, the method comprising: storing a precursor in at least one of the bulk containers; transporting the precursor in vapor form from the bulk container(s) to a first run/refill chamber; receiving the precursor in vapor form in the first run/refill chamber; condensing and storing the precursor in solid form in the first run/refill chamber; causing sublimation of the solid precursor within the first run/refill chamber while transporting the precursor in vapor form from the bulk container(s) to a second run/refill chamber; and transporting the sublimed precursor in vapor form from the first run/refill chamber to a first deposition chamber, wherein at least one of the run/refill chambers includes a plurality of spaced tubes having a plurality of surfaces configured to receive the precursor in vapor form and store the precursor in solid form.

13. The method of claim 12 , further comprising causing sublimation of the solid precursor within the second run/refill chamber while transporting the precursor in vapor form from the bulk container(s) to the first run/refill chamber.

14. The method of claim 12 , wherein condensing and storing the precursor in solid form in the first run/refill chamber comprises cooling the first run/refill chamber.

15. The method of claim 14 , wherein causing sublimation of the solid precursor within the first run/refill chamber while transporting the precursor in vapor form from the bulk container(s) to a second run/refill chamber comprises heating the first run/refill chamber.

16. The method of claim 12 , wherein the multiple run/refill chambers provide an uninterrupted flow of precursor in vapor form to at least one deposition chamber.

17. The method of claim 12 , wherein the at least one bulk container provides precursor in vapor form to the multiple run/refill chambers sequentially.

18. The method of claim 12 , wherein the run/refill chambers are located in a fabrication area, and the bulk container(s) is located outside the fabrication area.

Assignments (2)
SECURITY INTEREST Recorded Jun 2, 2023
From: ENTEGRIS, INC.; CMC MATERIALS LLC
To: MORGAN STANLEY SENIOR FUNDING, INC., AS COLLATERAL AGENT
Reel/Frame 063857/0199 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 30, 2022
From: ELDRIDGE, DAVID JAMES; PETERS, DAVID; WRIGHT, ROBERT, JR.; HENDRIX, BRYAN C.; BATTLE, SCOTT L.; GREGG, JOHN
To: ENTEGRIS, INC.
Reel/Frame 061925/0216 →