IP Library Granted Patent US 12,492,512
Granted Patent B2
US 12,492,512 · App. 17/979,087 · Granted Dec 9, 2025

Functional paper for electronics printing and methods of making

Inventors: Lokendra Pal (Raleigh, NC); Manoj Kumar Dixit (Matthews, NC); Sachin Agate (Raleigh, NC); Brian Watson Ranson (Greensboro, SC)
Assignees: North Carolina State University; Domtar Paper Company LLC
D21H21/16D21H17/29D21H17/37D21H17/66D21H23/24H05K1/0386H05K1/097H05K2201/10037H05K2201/10098H05K2201/10106H05K2201/10128H05K2201/10151
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Quick Facts
Patent No.
US 12,492,512
App. No.
17/979,087
Granted
Dec 9, 2025
Kind
B2
Abstract

Provided herein is an uncoated functional paper formed from a slurry comprising about 10 wt % to 90 wt % cellulosic fibers and about 1% to 25% sizing solution per total weight of the fibers. The sizing solution can be applied during papermaking and/or applied in a size press or coater. The paper can be calendered at a temperature greater than 50° C. Methods of making are also provided. Also provided are flexible electronics including a functional paper substrate printed with a conductive ink.

Claims (12)

1 . A method of making a functional paper comprising:

forming a paper from a slurry, the slurry comprising about 10 wt % to 90 wt % cellulosic fibers and about 1% to 25% sizing solution per total weight of the fibers;

calendering the paper at a temperature greater than 50° C. and a pressure between 100 psi and 1500 psi;

printing on the paper with a conductive ink wherein the calendering can be performed before printing, after printing, or both;

applying an internal sizing agent at a wet end of a paper machine; and

applying a surface sizing solution at a dry end of the paper machine using a size press,

wherein the surface sizing solution is selected from an aqueous solution comprising 10% solids by weight, wherein the solids comprise about 90 wt % ethylated starch and 10 wt % NaCl or wherein the solids comprise about 85 wt % ethylated starch, 10 wt % NaCl and 5 wt % acrylic copolymer.

2 . The method of claim 1 , further comprising applying the surface sizing solution to the paper using a rod coater to form sized and treated sheets.

3 . The method of claim 2 , wherein the surface treatment comprises a film-forming material in an aqueous medium, wherein the film-forming material is selected from ethylated starch, alginate, carboxymethyl cellulose (CMC), SBR latex (SBR), polyvinyl alcohol, and combinations thereof.

4 . The method of claim 2 , wherein the surface treatment further comprises one or more additives, wherein the additives are selected from a salt, a surface sizing agent, or a combination thereof.

5 . The method of claim 4 , wherein the surface sizing agent comprises acrylic copolymer or a copolymer of styrene and maleic anhydride.

6 . The method of claim 4 , wherein the salt is selected from a monovalent salt, a divalent salt, a multivalent salt, and a combination thereof, and wherein the surface treatment comprises about 10 wt % salt.

Assignments (3)
SECURITY INTEREST Recorded Jan 30, 2025
From: RESOLUTE FP US INC.; EAM CORPORATION; DOMTAR PAPER COMPANY, LLC
To: BANK MANDIRI (EUROPE) LIMITED, AS THE COLLATERAL AGENT
Reel/Frame 070059/0666 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 7, 2024
From: PAL, LOKENDRA; AGATE, SACHIN
To: NORTH CAROLINA STATE UNIVERSITY
Reel/Frame 069186/0359 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 7, 2024
From: DIXIT, MANOJ KUMAR; RANSON, BRIAN WATSON
To: DOMTAR PAPER COMPANY LLC
Reel/Frame 069186/0651 →
Continuity (2)
Provisional Application 63275092 · Nov 3, 2021
Related Publication 20230136850A1 · May 4, 2023
References Cited (6)
US 20080035292A1 · Singh · 2008 [cited by examiner]
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Smook Front Matter (Year: 2016). [cited by examiner]
Gary A Smook, Handbook for Pulp & Paper Technologists, 2016, published by Tappi, p. 293-309 (Year: 2016). [cited by examiner]