IP Library Granted Patent US 12,410,351
Granted Patent B2
US 12,410,351 · App. 18/030,625 · Granted Sep 9, 2025

Refrigerant compositions for refrigerant compressor systems

Inventors: Stephen Spletzer (Lincoln University, PA); Barbara Haviland Minor (The Villages, FL)
Assignee: THE CHEMOURS COMPANY FC, LLC
C09K5/045C09K2205/122C09K2205/126C09K2205/40
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Quick Facts
Patent No.
US 12,410,351
App. No.
18/030,625
Granted
Sep 9, 2025
Kind
B2
Abstract

Disclosed is a composition comprising difluoromethane (R-32), 2,3,3,3-tetrafluoropropene (R-1234yf), and isobutane (R-600a). A refrigeration system, including a hermetic compressor and a refrigerant composition. The refrigerant composition includes difluoromethane (R-32), 2,3,3,3-tetrafluoropropene (R-1234yf), and isobutane (R-600a).

Claims (27)

1. A composition comprising a refrigerant consisting essentially of 15 to 22 weight percent difluoromethane, 70 to 84 weight percent 2,3,3,3-tetrafluoropropene, and 1.0 to 10 weight percent isobutane.

2. The composition of claim 1 , wherein the refrigerant consists essentially of 15 to 19 weight percent difluoromethane, 76 to 84 weight percent 2,3,3,3-tetrafluoropropene, and 1.0 to 6.0 weight percent isobutane.

3. The composition of claim 1 , wherein the refrigerant consists essentially of 20 to 22 weight percent difluoromethane, 73 to 76 weight percent 2,3,3,3-tetrafluoropropene, and 4.0 to 5.0 weight percent isobutane.

4. The composition of claim 1 , further comprising a non-refrigerant compound in an amount of 0.01 to 49 weight percent based on the weight of the refrigerant composition.

5. The composition of claim 4 , wherein the non-refrigerant compound includes a lubricant selected from the group consisting of mineral oil, alkylbenzene, polyol esters, polyalkylene glycols, polyvinyl ethers, polycarbonates, perfluoropolyethers, silicones, silicate esters, phosphate esters, paraffins, naphthenes, polyalpha-olefins, and combinations thereof.

6. A refrigeration system, comprising:

a hermetic compressor;

and the composition of claim 1 .

7. The refrigeration system of claim 6 , wherein said hermetic compressor is a rotary, scroll, or reciprocating compressor.

8. The refrigeration system of claim 6 , further comprising a non-refrigerant compound in an amount of 0.01 to 49 weight percent based on the weight of the refrigerant composition.

9. The refrigeration system of claim 8 , wherein the non-refrigerant compound includes a lubricant selected from the group consisting of mineral oil, alkylbenzene, polyol esters, polyalkylene glycols, polyvinyl ethers, polycarbonates, perfluoropolyethers, silicones, silicate esters, phosphate esters, paraffins, naphthenes, polyalpha-olefins, and combinations thereof.

10. The refrigeration system of claim 6 :

wherein the compressor discharge temperature is below the compressor discharge temperature of R-457A or R-454C.

11. A method of operating a hermetic compressor as part of a refrigeration system, comprising the steps of:

receiving by the hermetic compressor the composition of claim 1 ;

compressing by the hermetic compressor the composition;

wherein the discharge temperature of the hermetic compressor is between 80.0° C. and 100.0° C.

12. The method of claim 11 , wherein the hermetic compressor is a low back pressure hermetic reciprocating compressor and the low back pressure hermetic reciprocating compressor receives the composition of claim 1 from an evaporator having an average evaporator temperature between −40° C. and −5° C.

13. The method of claim 11 , wherein the discharge temperature of the compressor is between 81.0° C. and 99.0° C.

14. The method of claim 11 , wherein:

the hermetic compressor is a low back pressure hermetic reciprocating compressor; and

the method further comprises a step of receiving by the low back pressure hermetic reciprocating compressor the refrigerant composition from an evaporator;

wherein the average evaporator temperature is below −5° C.

15. A method of replacing a first refrigerant composition comprising R-404A, R-457A, R-290, or R-454C with a second refrigerant composition comprising 70 to 84 weight percent 2,3,3,3-tetrafluoropropene, 15 to 22 weight percent difluoromethane, and 1.0 to 10 weight percent isobutane, wherein the replacing is performed in a refrigeration system including a hermetic compressor.

16. The method of claim 15 , wherein the second refrigerant composition further comprises a non-refrigerant compound in an amount of 0.01 to 50 weight percent based on the weight of the refrigerant composition.

17. The method of claim 16 , wherein the non-refrigerant compound includes a lubricant selected from the group consisting of mineral oil, alkylbenzene, polyol esters, polyalkylene glycols, polyvinyl ethers, polycarbonates, perfluoropolyethers, silicones, silicate esters, phosphate esters, paraffins, naphthenes, polyalpha-olefins, and combinations thereof.

18. The method of claim 15 , wherein the compressor discharge temperature is below the compressor discharge temperature of R- 457 A.

Assignments (2)
SECURITY INTEREST Recorded May 7, 2024
From: THE CHEMOURS COMPANY FC, LLC
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 067341/0844 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 7, 2023
From: SPLETZER, STEPHEN; MINOR, BARBARA HAVILAND
To: THE CHEMOURS COMPANY FC, LLC
Reel/Frame 063252/0963 →
Continuity (3)
Provisional Application 63138928 · Jan 19, 2021
Provisional Application 63089186 · Oct 8, 2020
Related Publication 20230374361A1 · Nov 23, 2023
References Cited (8)
US 10414962B2 · Saito et al. · 2019 [cited by applicant]
US 20080230738A1 · Minor et al. · 2008 [cited by applicant]
US 20190062613A1 · Saito · 2019 [cited by examiner]
US 20220363967A1 · Tækker Svendsen · 2022 [cited by examiner]
GB 2435747A · 2007 [cited by examiner]
ASHRAE Standard 34-2019, Designation and Safety Classification of Refrigerants, ANSI/ASHRAE, 2019, pp. 1-52, Atlanta, GA. [cited by applicant]
PCT International Search Report and Written Opinion for Application No. PCT/US2021/053969 mailed Jan. 28, 2022. [cited by applicant]
Standard Test Method for Concentration Limits of Flammability of Chemicals (Vapors and Gases), ASTM, 2015, E681-09, pp. 1 to 12, West Conshohocken, PA. [cited by applicant]