IP Library Granted Patent US 12,637,557
Granted Patent B2
US 12,637,557 · App. 18/039,703 · Granted May 26, 2026

High crystalline olefin polymer for high speed spinning

Inventor: John Kaarto (Lake Jackson, TX)
Assignee: W.R. Grace & Co.-CONN.
C08L23/142C08K5/098C08K5/14C08K5/20C08K5/3492C08K5/5317C08K5/5393D01D5/0885D04H1/4291D04H1/56C08K2201/012C08K2201/014D10B2321/022
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Quick Facts
Patent No.
US 12,637,557
App. No.
18/039,703
Granted
May 26, 2026
Kind
B2
Abstract

A polymer composition includes a low ethylene random copolymer that can be used to form a meltspun or spunbond article at high spinning velocities. The polymer composition has a low xylene soluble content, a high crystallinity, or both, while having reduced spin-break at high spinning velocities. The polymer composition also exhibits good fiber tenacity and fabric softness.

Claims (20)

1 . A polymer composition for forming a melt spun web, the polymer composition comprising: a propylene and α-olefin random copolymer; wherein: the random copolymer comprises α-olefin monomer units in an amount less than 1% by weight; the random copolymer having been peroxide cracked; the random copolymer exhibiting a rheological polydispersity index of 3 or less after peroxide cracking, a xylene solubles content of 2.7 wt. % or less prior to peroxide cracking, and a crystallinity of 55% or greater after peroxide cracking; and the polymer composition exhibits a melt flow rate of 20 dg/minute or greater (according to ASTM D1238, at 2300 C with a load of 2.16 kg).

2 . The composition of claim 1 , wherein the xylene solubles content is 2% or less.

3 . The composition of claim 1 , wherein the xylene solubles content is 1.8% or less.

4 . The composition of claim 1 , wherein the crystallinity is 60% or greater.

5 . The composition of claim 1 , wherein the crystallinity is 65% or greater.

6 . The composition of claim 1 wherein the α-olefin is ethylene.

7 . The composition of claim 1 , wherein the melt flow rate is 25 dg/min to 100 dg/min.

8 . The composition of claim 7 , wherein the melt flow rate is 35 dg/min to 65 dg/min.

9 . The composition of claim 1 , wherein the polydispersity index is 2.7 or less.

10 . The composition of claim 1 , wherein the polydispersity index is 2.5 or less.

11 . The composition of claim 1 , wherein the polymer composition includes an antacid and a stabilizer.

12 . The composition of claim 11 , wherein the polymer composition further comprises a lubricant, a processing aid, or a combination of any two or more thereof.

13 . The composition of claim 12 , wherein the lubricant comprises ethylene bis-stearamide, the processing aid comprises a fluoropolymer, the stabilizer comprises a phosphite, and the antacid comprises calcium stearate.

14 . The composition of claim 11 , wherein the stabilizer is present in a concentration of about 100 ppm up to about 2500 ppm.

15 . The composition of claim 1 , wherein the composition comprises a primary antioxidant, optionally a secondary antioxidant, and an antacid.

16 . The composition of claim 1 , wherein the composition comprises a primary antioxidant and an optional secondary antioxidant, wherein the primary antioxidant or the optional secondary antioxidant comprises a phenolic antioxidant; a lubricant comprising ethylene bis-stearamide; a processing aid comprising a fluoropolymer; a stabilizer comprises comprising a phosphite; and an antacid comprises comprising calcium stearate.

17 . A spunbond nonwoven web comprising, a plurality of fibers comprising the polymer composition of claim 1 , wherein the plurality of fibers are bonded together to form the web.

18 . The spunbond nonwoven web of claim 17 , comprising fibers having a linear mass density (denier, grams/9000 meters) of less than 2 denier per filament.

19 . A process for making a spunbond nonwoven web, the process comprising feeding the polymer composition of claim 1 into an extruder, the polymer composition being heated into a molten state and extruded through a die to form filaments, quenching the filaments, depositing the filaments on a moving belt, and bonding the filaments together to form a nonwoven web.

20 . The process of claim 19 , further comprising drawing the filaments at a high speed to a linear mass density (grams/9000 meters) of less than 2 denier per filament.

Assignments (7)
RELEASE OF SECURITY INTEREST SUPPLEMENT NO. 2, RECORDED AT REEL/FRAME 072519/0265 Recorded Feb 2, 2026
From: WILMINGTON TRUST, NATIONAL ASSOCIATION
To: W. R. GRACE & CO.-CONN.
Reel/Frame 074612/0591 →
NOTES SECURITY INTEREST Recorded Jan 29, 2026
From: W. R. GRACE & CO.-CONN.; ADVANCED REFINING TECHNOLOGIES LLC
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS NOTES COLLATERAL AGENT
Reel/Frame 074532/0229 →
SECURITY INTEREST Recorded Aug 19, 2025
From: W. R. GRACE & CO.-CONN.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION
Reel/Frame 072519/0240 →
SECURITY AGREEMENT (NOTES) Recorded Aug 19, 2025
From: W. R. GRACE & CO.-CONN.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS NOTES COLLATERAL AGENT
Reel/Frame 072520/0653 →
SECURITY INTEREST Recorded Aug 19, 2025
From: W. R. GRACE & CO.-CONN.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION
Reel/Frame 072519/0265 →
SECURITY AGREEMENT (SUPPLEMENTAL NO. 2) Recorded Aug 19, 2025
From: W. R. GRACE & CO.-CONN.
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 072497/0481 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 1, 2023
From: KAARTO, JOHN
To: W.R. GRACE & CO.-CONN.
Reel/Frame 063831/0067 →
Continuity (2)
Provisional Application 63122680 · Dec 8, 2020
Related Publication 20240018346A1 · Jan 18, 2024
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