Fabrication of metallic parts by additive manufacturing
In various embodiments, wire composed at least partially of arc-melted refractory metal material is utilized to fabricate three-dimensional parts by additive manufacturing.
1. A method of fabricating a three-dimensional part comprising a metallic material, the method comprising:
(a) providing a wire comprising arc-melted metallic material, wherein the wire is produced by a process comprising (i) in a processing ambient comprising a vacuum or one or more inert gases, arc-melting a feed electrode comprising the metallic material to thereby form a billet, and (ii) mechanically deforming the billet into wire having a diameter less than a diameter of the billet;
(b) translating a tip of the wire relative to a platform;
(c) while the tip of the wire is being translated, melting the tip of the wire with an energy source to form a molten bead, whereby the bead cools to form at least a portion of a layer of a three-dimensional part; and
(d) repeating steps (b) and (c) one or more times to produce the three-dimensional part,
wherein the three-dimensional part comprises the metallic material.
2. The method of claim 1 , wherein the metallic material comprises at least one of niobium, tantalum, rhenium, tungsten, or molybdenum.
3. The method of claim 1 , wherein a concentration within the wire of at least one of sodium, calcium, antimony, magnesium, phosphorous, or potassium is less than 5 ppm by weight.
4. The method of claim 1 , wherein a concentration of oxygen within the wire is less than 20 ppm by weight.
5. The method of claim 1 , wherein a density of the three-dimensional part is greater than 97% of a theoretical density of the metallic material.
6. The method of claim 1 , wherein in step (c) the energy source comprises an electron beam and/or a laser beam.
7. A method of fabricating a three-dimensional part comprising a metallic material, the method comprising:
(a) providing a wire comprising arc-melted metallic material;
(b) translating a tip of the wire relative to a platform;
(c) while the tip of the wire is being translated, melting the tip of the wire with an energy source to form a molten bead, whereby the bead cools to form at least a portion of a layer of a three-dimensional part; and
(d) repeating steps (b) and (c) one or more times to produce the three-dimensional part,
wherein the three-dimensional part comprises the metallic material, and the wire is produced by a process comprising:
compacting powder to form a feed electrode, the powder comprising the metallic material;
arc-melting the feed electrode in a processing ambient comprising a vacuum or one or more inert gases, thereby forming a billet; and
mechanically deforming the billet into wire having a diameter less than a diameter of the billet.
8. The method of claim 7 , wherein the metallic material comprises at least one of niobium, tantalum, rhenium, tungsten, or molybdenum.
9. The method of claim 7 , wherein a concentration within the wire of at least one of sodium, calcium, antimony, magnesium, phosphorous, or potassium is less than 5 ppm by weight.
10. The method of claim 7 , wherein a concentration of oxygen within the wire is less than 20 ppm by weight.
11. The method of claim 7 , wherein a density of the three-dimensional part is greater than 97% of a theoretical density of the metallic material.
12. The method of claim 7 , wherein in step (c) the energy source comprises an electron beam and/or a laser beam.
13. The method of claim 7 , wherein mechanically deforming the billet comprises at least one of drawing, rolling, swaging, extruding, or pilgering.
14. The method of claim 7 , wherein the wire-production process comprises sintering the compacted powder at a temperature greater than 900° C.
15. The method of claim 7 , wherein the wire-production process comprises providing the powder by a process comprising at least one of plasma densification or plasma atomization.
16. The method of claim 7 , wherein the wire-production process comprises:
hydrogenating metal to form a metal hydride;
mechanically grinding the metal hydride into a plurality of particles; and
dehydrogenating the metal hydride particles.
17. The method of claim 1 , wherein mechanically deforming the billet comprises at least one of drawing, rolling, swaging, extruding, or pilgering.