IP Library Granted Patent US 12,410,382
Granted Patent B2
US 12,410,382 · App. 18/159,019 · Granted Sep 9, 2025

Dental material compositions for cleansing and removal of anionic contaminants from substrates and their methods of use

Inventor: Alexander D. Johnson (Racine, WI)
Assignee: INTER-MED, INC.
C11D3/046A61C17/02A61C19/002C11D3/124C11D3/40
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Quick Facts
Patent No.
US 12,410,382
App. No.
18/159,019
Granted
Sep 9, 2025
Kind
B2
Abstract

Compositions and methods useful for removing anionic contaminates and debris including phosphates from dental restorative substrates are disclosed.

Claims (30)

1. A composition for removing anionic contaminants from dental restorative surfaces, comprising:

at least one metal trihalide salt;

at least one thickening agent;

at least colorant; and water

wherein the pH of the composition is between 2 and 4.

2. The composition of claim 1 , wherein the composition retains its chemical stability for more than 60 days without the formation of a visible precipitate.

3. The composition of claim 1 , wherein the at least one metal trihalide salt contains a metal element exhibiting an electronegativity value between 1.0 and 1.3.

4. The composition of claim 1 , wherein the at least one metal trihalide salt dissolves in water forming at least one metal cations, wherein the at least one metal cations has a high affinity for phosphate.

5. The composition of claim 1 , wherein the metal of the at least one metal trihalide salt has an atomic size between 125 pm and 215 pm.

6. The composition of claim 1 , wherein the at least one metal trihalide salt comprises a lanthanum salt.

7. The composition of claim 1 , wherein the at least one metal trihalide salt comprises lanthanum chloride hydrate.

8. The composition of claim 1 , wherein the at least one metal trihalide salt comprises lanthanum chloride hydrate at a concentration between 20% and 40%.

9. The composition of claim 1 , wherein the at least one thickening agent comprises polyvinyl alcohol.

10. The composition of claim 1 , wherein the at least one thickening agent comprises fumed silica.

11. The composition of claim 1 , further comprising a surfactant or blend of surfactants.

12. The composition of claim 1 , further comprising a humectant or humectants.

13. The composition of claim 1 , wherein the composition has a viscosity between 0.2 and 0.8 Pa·s.

14. The composition of claim 1 , wherein the colorant is added in sufficient quantity to provide visual contrast when applied to a dental restorative surface.

15. The composition of claim 1 , wherein the composition consists of: lanthanum chloride hydrate at a concentration of 28% (wt/wt), polyvinyl alcohol at a concentration of 3.2% (wt/wt), a blend of FD&C yellow #5-6 and red #40 at a concentration of 0.5% (wt/wt), and deionized water.

16. A method of cleaning a dental restorative surface, comprising:

applying a cleaning solution of claim 1 to a dental restoration surface;

allowing the cleaning solution to dwell on the dental restoration surface for a period of time; and

rinsing away the cleaning solution from the dental restoration surface,

wherein the pH of the cleaning solution is between 2 and 4.

17. The method of claim 16 , wherein, the cleaning solution does not require shaking prior to application to the dental restoration surface, wherein, the cleaning solution chemically removes substantially all phosphate contaminates from the dental restoration surface; and, wherein, the cleaning solution is chemically stable for at least 60 days without the formation of a visible precipitate.

18. The method of claim 16 , wherein the dwell time is between 10 and 30 seconds.

19. A dental restoration kit, comprising:

a cleaning composition of claim 1 ; and,

application tips or application brushes.

20. The kit of claim 19 further comprising a dental primer and a dental cement or a dental composite.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 15, 2025
From: JOHNSON, ALEXANDER D.
To: INTER-MED, INC.
Reel/Frame 072032/0982 →
SECURITY INTEREST Recorded Apr 3, 2024
From: INTER-MED, INC.
To: BMO BANK N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 066993/0755 →
Continuity (2)
Provisional Application 63267074 · Jan 24, 2022
Related Publication 20230235248A1 · Jul 27, 2023
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