IP Library Granted Patent US 12,697,602
Granted Patent B2
US 12,697,602 · App. 18/230,848 · Granted Aug 4, 2026

Antibiological sorbent and method of manufacture thereof

Inventor: Jaspreet S. Dhau (San Francisco, CA)
Assignee: Molekule Group, Inc.
B01J20/324B01J20/0259B01J20/0262B01J20/041B01J20/20B01J20/28083B01J20/28085B01J2220/42B82Y30/00
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Quick Facts
Patent No.
US 12,697,602
App. No.
18/230,848
Filed
Aug 7, 2023
Granted
Aug 4, 2026
Kind
B2
Art Unit
1736
USPC
502/417
Abstract

An antibiological sorbent can include sorbent material (e.g., porous carbon, activated carbon, inorganic carbon, organic carbon, etc.), antibiological material, optionally a functionalizing material, and/or any other suitable material. The antibiological material (and/or the functionalizing material) can coat, intercalate within (e.g., within a porous network of), form structures on, be disposed on, bind to, and/or otherwise be interfaced to the sorbent material. A method for manufacturing the antibiological sorbent can include: mixing sorbent material with a precursor; optionally, functionalizing (e.g., activating) the sorbent material; forming antibiological material from the precursor; optionally, post-processing (e.g., washing) the resulting material; and/or any suitable steps.

Claims (14)

1 . A method comprising:

a. forming a slurry comprising porous carbon particles, a solvent, and an antibiological precursor;

b. reducing the antibiological precursor to form a reduced antibiological precursor by adding a reducing agent to the slurry, wherein the only byproducts from oxidation of the reducing agent are water or gas-phase at standard temperature and pressure;

c. after the antibiological precursor has been reduced, adding an oxidizing agent to the slurry to form coated carbon particles comprising antibiological nanoparticles dispersed on a surface of the porous carbon particles, wherein the oxidizing agent oxidizes the reduced antibiological precursor to form the antibiological nanoparticles;

wherein the antibiological precursor comprises selenium powder and the antibiological nanoparticles comprise selenium nanoparticles, wherein the reducing agent reduces the selenium powder into selenium anions, wherein the oxidizing agent oxidizes the selenium anions into the selenium nanoparticles.

2 . The method of claim 1 , wherein a sorption capacity of the coated carbon particles is substantially the same as the sorption capacity of the porous carbon particles.

3 . The method of claim 1 , further comprising sparging the slurry with carbon dioxide gas prior to adding the reducing agent.

4 . The method of claim 1 , further comprising functionalizing the porous carbon particles with a material that increases a VOC sorption capacity of the porous carbon particles.

5 . The method of claim 4 , wherein functionalizing the porous carbon particles does not substantially change an antibiological property of the coated carbon particles.

6 . The method of claim 1 , wherein the antibiological precursor further comprises copper nitrate and the antibiological nanoparticles further comprise copper oxide nanoparticles, wherein the reducing agent reduces the copper nitrate into copper nanoparticles, wherein the oxidizing agent oxidizes the copper nanoparticles into the copper oxide nanoparticles.

7 . The method of claim 6 , wherein the copper oxide nanoparticles comprise a mixture of copper (I) oxide and copper (II) oxide.

8 . The method of claim 1 , wherein the reducing agent comprises hydrazine hydrate.

9 . The method of claim 1 , wherein the antibiological nanoparticles comprise porous and nonporous nanoparticles.

10 . The method of claim 1 , wherein the porous carbon particles comprise activated carbon.

Assignments (6)
CHANGE OF NAME Recorded Nov 6, 2024
From: MOLEKULE GROUP, INC.
To: MKUL, INC.
Reel/Frame 069318/0895 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 6, 2024
From: MKUL, INC.
To: MOLEKULE GROUP, INC.
Reel/Frame 069319/0930 →
DEBTORS' JOINT PLAN OF REORGANIZATION UNDER CHAPTER 11 OF THEBANKRUPTCY CODE Recorded Nov 6, 2024
From: MOLEKULE, INC.
To: MOLEKULE GROUP, INC.
Reel/Frame 069322/0709 →
SECURITY INTEREST Recorded Nov 1, 2024
From: MOLEKULE GROUP, INC.
To: FIRST-CITIZENS BANK & TRUST COMPANY
Reel/Frame 069109/0262 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNMENT DOCUMENT HAD TYPO IN THE ASSIGNEE NAME PREVIOUSLY RECORDED ON REEL 64635 FRAME 141. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Oct 22, 2024
From: DHAU, JASPREET S.; SINGH, AVTAR
To: MOLEKULE, INC.
Reel/Frame 069230/0844 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 18, 2023
From: DHAU, JASPREET S.; SINGH, AVTAR
To: MOLEKULE, INC.
Reel/Frame 064635/0141 →
Continuity (2)
Provisional Application 63395405 · Aug 5, 2022
Related Publication 20240042418A1 · Feb 8, 2024
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