IP Library Granted Patent US 12,637,712
Granted Patent B2
US 12,637,712 · App. 18/305,745 · Granted May 26, 2026

Fragmentation of DNA

Inventors: Lynne Apone (Waltham, MA); Brittany S. Sexton (Amesbury, MA); Margaret Heider (Ipswich, MA); Louise Js Williams (Reading, MA); Eileen T. Dimalanta (Wakefield, MA)
Assignee: New England Biolabs, Inc.
C12Q1/6869C12N15/1065C12Q1/6855C12Q1/686C40B20/04C40B40/06C40B50/06
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Quick Facts
Patent No.
US 12,637,712
App. No.
18/305,745
Granted
May 26, 2026
Kind
B2
Abstract

Provided herein is a polymerase-free enzyme mix (FRAG) for fragmenting double-stranded DNA. In some embodiments the enzyme mix may comprise a double-stranded DNA nickase and at least one of a DNA ligase capable of sealing a nick within a DNA, and a single-strand specific DNA nuclease. Methods for fragmenting double-stranded DNA are also provided.

Claims (16)

1 . A reaction mix comprising:

(a) a nickase that nicks double-stranded DNA;

(b) a single-strand DNA nuclease;

(c) a DNA ligase; and

(d) fragments of double-stranded genomic DNA, wherein the fragments have a median length in the range of 100 bp to 40 kbp.

2 . The reaction mix according to claim 1 , wherein: the double-stranded random DNA nickase is at a concentration of 0.001 ng/μl-0.25 ng/μl, the single-strand nuclease is at a concentration of 0.0025 μg/μl-1.4 μg/μl, and the ligase is at a concentration of 0.03 ng/μl-8 ng/μl.

3 . The reaction mix according to 1 , further comprising: one or more of a polynucleotide kinase (PNK), a nicking agent, and a DNA repair enzyme.

4 . The reaction mix according to claim 1 , wherein the DNA ligase is an NAD + DNA ligase.

5 . The reaction mix according to claim 1 , wherein the DNA ligase is selected from the group consisting of Taq DNA ligase, E. coli DNA ligase and an archaeal DNA Ligase.

6 . The reaction mix according to claim 1 , wherein the single-strand nuclease is zinc dependent.

7 . The reaction mix according to claim 1 , wherein the single-strand nuclease is selected from the group consisting of mung bean nuclease, recJ, a nuclease T, and a member of the S1 or P1 nuclease family of nucleases.

8 . The reaction mix according to claim 1 , wherein the single-strand nuclease is a P1 nuclease.

9 . The reaction mix according to claim 1 , wherein the nickase is selected from the group consisting of a DNase or mutants thereof, Vvn nuclease, and micrococcal nuclease.

10 . The reaction mix according to claim 9 , wherein the nickase is DNase I.

11 . The reaction mix according to claim 1 , wherein the fragments have a median length in the range of 100 bp to 10 kb.

12 . The reaction mix according to claim 1 , wherein the fragments have a median length in the range of 10 kb to 40 kb.

Assignments (2)
NOTICE OF GRANT OF SECURITY INTEREST IN PATENTS Recorded Sep 27, 2023
From: NEW ENGLAND BIOLABS, INC.
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 065044/0729 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 25, 2023
From: APONE, LYNNE; SEXTON, BRITTANY S.; HEIDER, MARGARET; WILLIAMS, LOUISE JS; DIMALANTA, EILEEN T.
To: NEW ENGLAND BIOLABS, INC.
Reel/Frame 063426/0405 →
Continuity (3)
Division 17658485 · Apr 8, 2022
Provisional Application 63193667 · May 27, 2021
Related Publication 20230257808A1 · Aug 17, 2023
References Cited (31)
US 6191267B1 · Kong et al. · 2001 [cited by applicant]
US 7081358B2 · Heiter et al. · 2006 [cited by applicant]
US 7435572B2 · Bitinaite · 2008 [cited by applicant]
US 7666645B2 · Wang · 2010 [cited by applicant]
US 7700283B2 · Evans et al. · 2010 [cited by applicant]
US 7943303B2 · Xu et al. · 2011 [cited by applicant]
US 8158388B2 · Evans et al. · 2012 [cited by applicant]
US 8163529B2 · Xu et al. · 2012 [cited by applicant]
US 9963687B2 · Hsieh et al. · 2018 [cited by applicant]
US 10633644B1 · Chen et al. · 2020 [cited by applicant]
US 11001836B2 · Andersen et al. · 2021 [cited by applicant]
US 20080145913A1 · Padgett et al. · 2008 [cited by applicant]
US 20090005252A1 · Drmanac · 2009 [cited by examiner]
US 20100002887A1 · Roeck et al. · 2010 [cited by applicant]
US 20100173364A1 · Evans, Jr. · 2010 [cited by examiner]
US 20110281776A1 · Eshoo · 2011 [cited by examiner]
US 20140343265A1 · Chen et al. · 2014 [cited by applicant]
US 20150111256A1 · Church · 2015 [cited by examiner]
US 20200255824A1 · Lai et al. · 2020 [cited by applicant]
US 20210054363A1 · Koetsier et al. · 2021 [cited by applicant]
CA 2263847A1 · 1998 [cited by applicant]
WO 2001092501A1 · 2001 [cited by applicant]
WO 2011102802A1 · 2011 [cited by applicant]
WO 2021034750A1 · 2021 [cited by applicant]
Kapa Biosystems, KAPA Frag Kit, Jun. 2016. (Year: 2016). [cited by examiner]
Schmidt, Digestion of insect chromatin with micrococcal nuclease, DNase I and DNase I combined with single-strand specific nuclease S1, Nucleic Acids Research, 4(7): 2169-2180, 1977. (Year: 1977). [cited by examiner]
Vogt, Purification and Further Properties of Single-Strand-Specific Nuclease from Aspergillus oryzae, Eur. J. Biochem. 33, 192-200, 1973. (Year: 1973). [cited by examiner]
Gregory, Characterization and mitigation of fragmentation enzyme-induced dual stranded artifacts, NAR Genomic and Bioinformatics, 2(4): 1-7, 2020. (Year: 2020). [cited by examiner]
Desai, et al. (2003) FEMS Microbiology Reviews, 26, 457-91. [cited by applicant]
Swinton, et al. (1985) FEBS, 2548, 184, 2, 294-298. [cited by applicant]
Ariga, et al. (1979) FEBS Letters, 107, 2, 355-358. [cited by applicant]