IP Library Granted Patent US 12,123,074
Granted Patent B2
US 12,123,074 · App. 18/315,623 · Granted Oct 22, 2024

Method for dissolving lithium compound, method for manufacturing lithium carbonate, and method for recovering lithium from lithium ion secondary cell scrap

Inventors: Hirotaka Ariyoshi (Hitachi, JP); Isao Tomita (Hitachi, JP); Hiroshi Abe (Hitachi, JP)
Assignee: JX METALS CIRCULAR SOLUTIONS CO., LTD.
C22B26/12B09B3/80C01D15/08C22B1/02C22B3/06C22B3/44H01M10/0525H01M10/54C01P2002/72C01P2006/40
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Quick Facts
Patent No.
US 12,123,074
App. No.
18/315,623
Granted
Oct 22, 2024
Kind
B2
Abstract

A method for dissolving a lithium compound according to the present invention includes bringing a lithium compound into contact with water or an acidic solution, and feeding, separately from the lithium compound, a carbonate ion to the water or the acidic solution to produce carbonic acid, and allowing the carbonic acid to react with the lithium compound to produce lithium hydrogen carbonate.

Claims (9)

1. A method for dissolving a lithium compound, the method, comprising bringing a lithium compound into contact with water or an acidic solution, and feeding, separately from the lithium compound, a carbonate ion to the water or the acidic solution to obtain a lithium dissolved solution,

wherein the lithium compound comprises cobalt, aluminum, and at least one of lithium hydroxide, lithium oxide, and lithium carbonate, and

wherein a pH of the lithium dissolved solution is from 7 to 10.

2. The method for dissolving the lithium compound according to claim 1 , wherein the carbonate ion is fed so as to maintain a saturated state of carbonic acid in the water or the acidic solution.

3. The method for dissolving the lithium compound according to claim 1 , wherein the feeding of the carbonate ion is carried out by blowing a carbon dioxide gas into the water or the acidic solution.

4. The method for dissolving the lithium compound according to claim 1 further comprising separating lithium from the lithium dissolved solution, and precipitating a lithium ion in the lithium dissolved solution as lithium carbonate.

5. The method for dissolving the lithium compound according to claim 4 , wherein when the lithium ion is precipitated, the lithium dissolved solution is heated to separate carbonic acid as a carbon dioxide gas from the lithium dissolved solution.

6. The method for dissolving the lithium compound according to claim 5 , wherein when the lithium ion is precipitated, the lithium dissolved solution is heated at a temperature of from 50° C. to 90° C.

7. The method for dissolving the lithium compound according to claim 1 , wherein when the lithium compound is brought into contact with the water or the acidic solution, the water or the acidic solution has a temperature of from 5° C. to 25° C.

Assignments (3)
CHANGE OF NAME Recorded Sep 17, 2024
From: JX ADVANCED METALS CORPORATION
To: JX METALS CIRCULAR SOLUTIONS CO., LTD.
Reel/Frame 068609/0690 →
CHANGE OF NAME Recorded Jul 29, 2024
From: JX METALS CORPORATION
To: JX ADVANCED METALS CORPORATION
Reel/Frame 068179/0696 →
CHANGE OF NAME Recorded Jun 27, 2024
From: JX NIPPON MINING & METALS CORPORATION
To: JX METALS CORPORATION
Reel/Frame 068050/0527 →