IP Library Granted Patent US 12,005,047
Granted Patent B2
US 12,005,047 · App. 18/361,837 · Granted Jun 11, 2024

Riluzole prodrugs and their use

Inventors: Jay Edward Wrobel (Lawrenceville, NJ); Allen B. Reitz (Lansdale, PA); Jeffery Claude Pelletier (Lafayette Hill, PA); Garry Robert Smith (Royersford, PA); Haiyan Bian (Princeton, NJ)
Assignee: Biohaven Therapeutics Ltd.
A61K31/428A61K9/006A61K9/1617A61K9/2004A61K31/454A61K31/496A61K31/506A61K31/5377A61K31/541A61K38/05A61K38/06A61K39/4636A61K45/06A61P25/00A61P25/28A61P35/00C07D277/82C07D417/12C07K5/06026C07K5/0806C07K5/0808C07K5/0812A61K2300/00
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Quick Facts
Patent No.
US 12,005,047
App. No.
18/361,837
Granted
Jun 11, 2024
Kind
B2
Abstract

Pharmaceutical compositions of the invention include substituted riluzole prodrugs useful for the treatment of cancers including melanoma, breast cancer, brain cancer, and prostate cancer through the release of riluzole. Prodrugs of riluzole have enhanced stability to hepatic metabolism and are delivered into systemic circulation by oral administration, and then cleaved to release riluzole in the plasma via either an enzymatic or general biophysical release process.

Claims (19)

1. A method for treating spinocerebellar ataxia, comprising administering to a subject in need of such treatment an effective amount of at least one compound having formula:

wherein R 23 is selected from the group consisting of H, CH 3 , CH 2 CH 3 , CH 2 CH 2 CH 3 , CH 2 CCH, CH(CH 3 ) 2 , CH 2 CH(CH 3 ) 2 , CH(CH 3 )CH 2 CH 3 , CH 2 OH, CH 2 OCH 2 Ph, CH 2 CH 2 OCH 2 Ph, CH(OH)CH 3 , CH 2 Ph, CH 2 (cyclohexyl), CH 2 (4-OH-Ph), (CH 2 ) 4 NH 2 , (CH 2 ) 3 NHC(NH 2 )NH, CH 2 (3-indole), CH 2 (5-imidazole), CH 2 CO 2 H, CH 2 CH 2 CO 2 H, CH 2 CONH 2 , and CH 2 CH 2 CONH 2 ; or an enantiomer, diastereomer, hydrate, solvate, pharmaceutically acceptable salt, or complex thereof.

2. The method according to claim 1 , wherein R 23 is H.

3. The method according to claim 1 , wherein the compound is selected from the group consisting of

(S)-2-amino-N-(2-(methyl(2-oxo-2-((6-(trifluoromethoxy)benzo[d]thiazol-2-yl)amino)ethyl)amino)-2-oxoethyl)propanamide;

(R)-2-amino-N-(2-(methyl(2-oxo-2-((6-(trifluoromethoxy)benzo[d]thiazol-2-yl)amino)ethyl)amino)-2-oxoethyl)propanamide;

(S)-2-amino-3-methyl-N-(2-(methyl(2-oxo-2-((6-(trifluoromethoxy)benzo[d]thiazol-2-yl)amino)ethyl)amino)-2-oxoethyl)butanamide;

(R)-2-amino-3-methyl-N-(2-(methyl(2-oxo-2-((6-(trifluoromethoxy)benzo[d]thiazol-2-yl)amino)ethyl)amino)-2-oxoethyl)butanamide;

(S)-2-amino-N-(2-(methyl(2-oxo-2-((6-(trifluoromethoxy)benzo[d]thiazol-2-yl)amino)ethyl)amino)-2-oxoethyl)-3-phenylpropanamide;

(R)-2-amino-N-(2-(methyl(2-oxo-2-((6-(trifluoromethoxy)benzo[d]thiazol-2-yl)amino)ethyl)amino)-2-oxoethyl)-3-phenylpropanamide;

(S)-2-amino-4-methyl-N-(2-(methyl(2-oxo-2-((6-(trifluoromethoxy)benzo[d]thiazol-2-yl)amino)ethyl)amino)-2-oxoethyl)pentanamide;

(R)-2-amino-4-methyl-N-(2-(methyl(2-oxo-2-((6-(trifluoromethoxy)benzo[d]thiazol-2-yl)amino)ethyl)amino)-2-oxoethyl)pentanamide;

(S)-2-amino-3-hydroxy-N-(2-(methyl(2-oxo-2-((6-(trifluoromethoxy)benzo[d]thiazol-2-yl)amino)ethyl)amino)-2-oxoethyl)propanamide;

(R)-2-amino-3-hydroxy-N-(2-(methyl(2-oxo-2-((6-(trifluoromethoxy)benzo[d]thiazol-2-yl)amino)ethyl)amino)-2-oxoethyl)propanamide;

2-(2-aminoacetamido)-N-methyl-N-(2-oxo-2-((6-(trifluoromethoxy)benzo[d]thiazol-2-yl)amino)ethyl)acetamide;

or a pharmaceutically acceptable salt thereof.

4. A compound according to claim 3 , which is 2-(2-aminoacetamido)-N-methyl-N-(2-oxo-2-((6-(trifluoromethoxy)benzo[d]thiazol-2-yl)amino)ethyl)acetamide or a pharmaceutically acceptable salt thereof.

5. The method according to claim 1 , wherein the at least one compound is administered in a composition further comprising at least one excipient.

6. The method according to claim 1 , wherein the spinocerebellar ataxia is hereditary spinocerebellar ataxia.

Assignments (1)
SECURITY INTEREST Recorded May 1, 2025
From: BIOHAVEN THERAPEUTICS LTD
To: BEETLEJUICE SA LLC, AS PURCHASER AGENT
Reel/Frame 071147/0260 →
Continuity (5)
Continuation 17164654 · Feb 1, 2021
Continuation 16449948 · Jun 24, 2019
Continuation 15549154
Provisional Application 62127684 · Mar 3, 2015
Related Publication 20230381149A1 · Nov 30, 2023
Cited By (1)
US 12,472,165