IP Library Granted Patent US 12,612,652
Granted Patent B2
US 12,612,652 · App. 18/369,464 · Granted Apr 28, 2026

High purity starch stream methods and systems

Inventors: Steven Redford (Brandon, SD); Todd Peterson (Brandon, SD)
Assignee: POET Research, Inc.
C12P7/06B02C9/04B02C13/22B02C23/14C12P7/10
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Quick Facts
Patent No.
US 12,612,652
App. No.
18/369,464
Granted
Apr 28, 2026
Kind
B2
Abstract

Methods and systems for isolating a high purity starch stream are provided. The methods provide an initial treatment step in advance of traditional grinding or fractionation operations (such as dry milling or wet milling operations) that facilitate separation of starch from other components of starch-based grains, for example facilitate separation of soft endosperm from other components of corn kernels including hard endosperm. The systems include a first treatment system for separating a high purity starch stream from other components of the grain stream, wherein the system can be configured as a bolt on for traditional milling operations such as wet milling and dry milling operations.

Claims (31)

1 . A process, comprising:

pretreating corn grain to produce a pretreated corn grain that facilitates separation of at least a portion of soft endosperm from the corn grain;

separating a first stream comprising soft endosperm from the pretreated corn grain resulting in a second stream suitable for use as feedstock in a fermentation process, wherein the second stream comprises fiber, germ, and starch;

exposing at least a portion of the second stream to fermentation conditions to produce ethanol; and

providing the first stream to a non-ethanol process, wherein the non-ethanol process comprises producing one or more non-ethanol bio-products.

2 . The process of claim 1 , further comprising processing starch in the first stream into sugar.

3 . The process of claim 2 , wherein processing starch in the first stream comprises:

enzymatically hydrolyzing starch into one or more dextrins; and

enzymatically hydrolyzing one or more dextrins into one or more sugars.

4 . The process of claim 1 , further comprising saccharifying the starch in the first stream into sugar.

5 . The process of claim 4 , further comprising, after saccharifying starch in the first stream, producing one or more non-ethanol bio-products.

6 . The process of claim 1 , further comprising:

saccharifying starch in the second stream into sugar; and

fermenting sugar in the second stream into ethanol.

7 . The process of claim 6 , wherein saccharifying is performed before fermenting.

8 . The process of claim 6 , wherein saccharifying and fermenting are performed simultaneously.

9 . The process of claim 6 , further comprising processing the second stream through a grinding operation prior to saccharifying starch into sugar.

10 . The process of claim 6 , further comprising:

distilling ethanol to form whole stillage;

separating thin stillage from whole stillage; and

evaporating water from thin stillage to form syrup.

11 . The process of claim 1 , wherein producing one or more non-ethanol bio-products comprises refining the first stream to increase purity of starch in the first stream, and wherein the one or more non-ethanol bio-products comprise starch.

12 . The process of claim 1 , wherein producing one or more non-ethanol bio-products comprises providing the first stream to a fermentation process to produce a non-ethanol bio-chemical, wherein the one or more non-ethanol bio-products comprise the bio-chemical.

13 . The process of claim 1 , wherein the one or more non-ethanol bio-products comprise starch.

14 . The process of claim 1 , wherein the one or more non-ethanol bio-products comprise one or more non-ethanol bio-chemicals produced via fermentation.

15 . The process of claim 1 , wherein the one or more non-ethanol bio-products comprise sugar.

16 . The process of claim 1 , wherein the first stream comprises at least 88% starch on a dry basis.

17 . The process of claim 1 , wherein the first stream comprises at least 90% starch on a dry basis.

18 . The process of claim 1 , wherein the first stream comprises at least 94% starch on a dry basis.

19 . The process of claim 1 , wherein pretreating corn grain comprises milling corn grain.

20 . The process of claim 1 , wherein pretreating corn grain comprises milling corn grain with a pin mill.

Assignments (3)
SECURITY INTEREST Recorded Aug 19, 2025
From: POET RESEARCH, INC.
To: COBANK, ACB
Reel/Frame 072062/0409 →
SECURITY INTEREST Recorded Aug 15, 2025
From: POET RESEARCH, INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 072489/0295 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 20, 2023
From: REDFORD, STEVEN G.; PETERSON, TODD
To: POET RESEARCH, INC.
Reel/Frame 064963/0624 →
Continuity (4)
Division 17009456 · Sep 1, 2020
Division 14983320 · Dec 29, 2015
Provisional Application 62098654 · Dec 31, 2014
Related Publication 20240002889A1 · Jan 4, 2024
References Cited (51)
US 3979375A · Rao et al. · 1976 [cited by applicant]
US 4287304A · Muller et al. · 1981 [cited by applicant]
US 7138257B2 · Galli et al. · 2006 [cited by applicant]
US 7303899B2 · Baldwin et al. · 2007 [cited by applicant]
US 7452425B1 · Langhauser · 2008 [cited by applicant]
US 9689003B2 · Lee · 2017 [cited by applicant]
US 9777303B2 · Jakel et al. · 2017 [cited by applicant]
US 10233466B2 · Redford · 2019 [cited by applicant]
US 10480038B2 · Jakel et al. · 2019 [cited by applicant]
US 10793879B2 · Redford et al. · 2020 [cited by applicant]
US 11060116B2 · Redford · 2021 [cited by applicant]
US 12084706B2 · Redford · 2024 [cited by applicant]
US 20040023349A1 · Bisgaard-Frantzen et al. · 2004 [cited by applicant]
US 20040187863A1 · Langhauser · 2004 [cited by applicant]
US 20060251762A1 · Jansen et al. · 2006 [cited by applicant]
US 20070259410A1 · Donaldson et al. · 2007 [cited by applicant]
US 20080299256A1 · Batie et al. · 2008 [cited by applicant]
US 20100059609A1 · Teeter, Jr. et al. · 2010 [cited by applicant]
US 20120244590A1 · Lee · 2012 [cited by applicant]
US 20130337517A1 · Razavi-Shirazi et al. · 2013 [cited by applicant]
US 20140106419A1 · Bazzana et al. · 2014 [cited by applicant]
US 20160186215A1 · Redford · 2016 [cited by applicant]
US 20160222135A1 · Lee · 2016 [cited by examiner]
US 20180016602A1 · Franko et al. · 2018 [cited by applicant]
US 20190153481A1 · Redford · 2019 [cited by applicant]
US 20190284593A1 · Jakel et al. · 2019 [cited by applicant]
US 20190284649A1 · Jakel et al. · 2019 [cited by applicant]
US 20190309377A1 · Jakel et al. · 2019 [cited by applicant]
US 20200399663A1 · Redford et al. · 2020 [cited by applicant]
US 20210163996A1 · Redford · 2021 [cited by applicant]
US 20210324423A1 · Redford · 2021 [cited by applicant]
WO 2006119386A2 · 2006 [cited by applicant]
WO 2009015333A1 · 2009 [cited by applicant]
WO 2013180863A1 · 2013 [cited by applicant]
WO 2014100685A1 · 2014 [cited by applicant]
Satyanarayana et al. “Development of an ideal starch saccharification process using amylolytic enzymes from thermophiles” Biochemical Society Transactions (2004) vol. 32, part 2, 276-278 (Year: 2004). [cited by examiner]
Tomask et al. “Enzymatic Conversions of Starch” Advances in Carbohydrate Chemistry and Biochemistry, vol. 68, pp. 59-436 (Year: 2012). [cited by examiner]
Gáspár et al. “Corn fiber as a raw material for hemicellulose and ethanol production” Process Biochemistry 42 (2007) 1135-1139 (Year: 2007). [cited by examiner]
International Search Report and Written Opinion from International Application No. PCT/US2015/067944, mailed Apr. 15, 2016 (12 pages). [cited by applicant]
Kwiatkowski et al. “Modeling the process and costs of fuel ethanol production by the corn dry-grind process” Industrial Crops and Products, vol. 23, pp. 288-296, 2006, (9 pages). [cited by applicant]
Jakel, “Product Diversification: Proven Path Forward”, Presented at American Coalition for Ethanol Annual Conference, Omaha, NE, Aug. 2017, https://ethanol.org/news/news/2017/08, (71 pages). [cited by applicant]
Robert, “Industrial Glucose: Bridging the Biochemical GAP”, Presented at ABLC2019, Renewable Chemicals Summit, Washington, DC, Apr. 4, 2019, (20 pages). [cited by applicant]
International Search Report and Written Opinion from International Application No. PCT/US2015/067951, mailed Apr. 20, 2016 (11 pages). [cited by applicant]
Jessen, “The Quest for Maximu Yield: Wet Mill to Dry Mill”, Ethanol Producer Magazine, Aug. 15, 2011, pp. 1-2, (2 pages). [cited by applicant]
Mueller et al., “2012 Corn Ethanol: Emerging Plant Energy and Environmental Technologies”, University of Illinois at Chicago, Energy Resources Center, College of Engineering, Apr. 29, 2013, pp. 1-31, (31 pages). [cited by applicant]
Wang et al., “Effect of Endosperm Hardness on an Ethanol Process Using a Granular Starch Hydrolyzing Enzyme”, Transactions of the the Asabe, vol. 53, No. 1, Jan. 1, 2010, pp. 307-312, (6 pages). [cited by applicant]
Ezeji et al., “Production of acetone-butanol-ethanol (ABE) in a continuous flow bioreactor using degermed corn and Clostridium beijerinckii”, Process Biochemistry, vol. 42, pp. 34-39, 2007, (6 pages). [cited by applicant]
Taylor et al., “Dry-Grind Process for Fuel Ethanol by Continuous Fermentation and Stripping”, Biotechnol. Prag. vol. 16, pp. 541-547, 2000, (7 pages). [cited by applicant]
Dien et al., “The U.S. corn ethanol industry: An overview of current technology and future prospects”, Int. Sugar Jnl., vol. 104, No. 1241, 2002, (8 pages). [cited by applicant]
Kim et al., “Composition of corn dry-grind ethanol by-products: DOGS, wet cake, and thin stillage”, Bioresource Technology, vol. 99, pp. 5165-5176, 2008, (12 pages). [cited by applicant]
Sigma Aldrich Chemicals-Technical Library “Particle Size Conversion Table” accessed at https://www.sigmaaldrich.com/chemistry/stockroom-reagents/learning-center/tech n ical-1 i brary /particle-Size-conversion. html avai… [cited by applicant]