IP Library Granted Patent US 12,209,220
Granted Patent B2
US 12,209,220 · App. 18/456,985 · Granted Jan 28, 2025

Using stimulus to convert coal to mesophase pitch and carbon fibers

Inventor: Charles Agee Atkins (Sheridan, WY)
Assignee: CARBON HOLDINGS INTELLECTUAL PROPERTIES, LLC
C10C3/002C01B32/05C01B32/154C01B32/184C01B32/26C10B19/00C10B53/04C10B55/00C10C1/00C10C1/04D01F9/12
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Quick Facts
Patent No.
US 12,209,220
App. No.
18/456,985
Granted
Jan 28, 2025
Kind
B2
Abstract

A method for forming mesophase pitch can include applying a stimulus to a first amount of coal tar to form a first amount of mesophase pitch. The stimulus can include one or more of an electromagnetic field (“EMF”) or a magnetic field. The method can further include evaluating a characteristic of the first amount of mesophase pitch, changing a parameter of the stimulus in response to evaluating the characteristic of the first amount of mesophase pitch, and applying the stimulus exhibiting the changed parameters to a second amount of coal tar to form mesophase pitch.

Claims (31)

1. A method for forming mesophase pitch, comprising:

continuously providing coal tar to a reactor;

applying a stimulus to an amount of the coal tar, the stimulus comprising an electromagnetic field (“EMF”), wherein the EMF has a wavelength of from about 1 mm to about 1 m; and

continuously forming mesophase pitch from the coal tar.

2. The method of claim 1 , further comprising forming the amount of coal tar by at least one of:

reducing a particle size of an amount of coal to form coal powder; sieving the coal powder;

pyrolyzing the amount of coal and extracting the amount of coal tar from the pyrolyzed coal; or

distilling the amount of coal tar to remove one or more contaminants therefrom.

3. The method of claim 1 , wherein the EMF comprises a pulsed EMF.

4. The method of claim 1 , wherein applying the stimulus to the amount of coal tar comprises:

applying a first EMF to the amount of coal tar, the first EMF having a first property; and applying a second EMF to the amount of coal tar, the second EMF having a second property that is different from the first property.

5. The method of claim 1 , wherein applying the stimulus to the amount of coal tar heats the amount of coal tar to a temperature of from about 100° C. to about 300° C.

6. The method of claim 1 , further comprising:

evaluating a characteristic of the amount of coal tar or the mesophase pitch; and

changing a parameter of the stimulus applied to the amount coal tar in response to evaluating the characteristic of the amount of coal tar or the mesophase pitch.

7. The method of claim 1 , further comprising forming the mesophase pitch into graphene, fullerene, diamond, or carbon fibers.

8. The method of claim 1 , further comprising air blowing the mesophase pitch.

9. The method of claim 1 , further comprising subjecting the mesophase pitch to a thermal process.

10. A method for processing coal tar, comprising:

evaluating a characteristic of an amount of coal or an amount of coal tar formed from the amount of coal;

selecting one or more parameters of a stimulus in response to evaluating the characteristic; and

applying a stimulus having the one or more parameters to the amount of coal tar to form mesophase pitch, the stimulus comprising an electromagnetic field (“EMF”), wherein the EMF has a wavelength of from about 1 mm to about 1 m.

11. The method of claim 10 , wherein:

selecting one or more parameters of the stimulus comprises selecting at least one of a wavelength, an intensity, or mode of the EMF.

12. A method for forming mesophase pitch, comprising:

applying a stimulus to a first amount of coal tar to form a first amount of mesophase pitch, the stimulus comprising one or more of an electromagnetic field (“EMF”), wherein the EMF has a wavelength of from about 1 mm to about 1 m;

evaluating a characteristic of the first amount of mesophase pitch;

changing a parameter of the stimulus in response to evaluating the characteristic of the first amount of mesophase pitch; and

applying the stimulus exhibiting the changed parameters to a second amount of coal tar to form a second amount of mesophase pitch.

13. The method of claim 12 , wherein:

the parameter of the stimulus comprises at least one of a wavelength, an intensity, or mode of the EMF.

Assignments (2)
SECURITY INTEREST Recorded Dec 30, 2025
From: CARBON HOLDINGS INTELLECTUAL PROPERTIES LLC
To: KEYBANK NATIONAL ASSOCIATION, A NATIONAL BANKING ASSOCIATION
Reel/Frame 073335/0331 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 23, 2024
From: ATKINS, CHARLES AGEE
To: CARBON HOLDINGS INTELLECTUAL PROPERTIES, LLC
Reel/Frame 068667/0628 →
Continuity (4)
Continuation 17863191 · Jul 12, 2022
Continuation 16826069 · Mar 20, 2020
Provisional Application 62821331 · Mar 20, 2019
Related Publication 20240026225A1 · Jan 25, 2024
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