IP Library Granted Patent US 12,181,388
Granted Patent B2
US 12,181,388 · App. 18/623,376 · Granted Dec 31, 2024

Device for tissue section immobilization and retention

Inventors: Yuji Ishitsuka (San Diego, CA); Zhenmin Hong (San Diego, CA); Eli N. Glezer (Del Mar, CA); Hu Cang (San Diego, CA); William Dempsey (San Diego, CA); Weiqiao Ding (San Diego, CA); Jaekyung Koh (San Diego, CA); Mohammad Vatankhah Varnosfaderani (San Marcos, CA)
Assignee: Singular Genomics Systems, Inc.
G01N1/30A61L27/28A61L27/52C12Q1/6841C12Q1/6874G01N1/06G01N1/28G01N1/286G01N1/312G01N1/36G01N23/2251G02B21/34G01N2001/2873G01N2001/288G01N2001/315
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Quick Facts
Patent No.
US 12,181,388
App. No.
18/623,376
Granted
Dec 31, 2024
Kind
B2
Abstract

Disclosed herein, inter alia, are devices and methods for transfer and analyses of tissue sections using carrier substrates.

Claims (29)

1. A device comprising:

a solid support comprising a plurality of discrete tissue samples attached to the solid support, wherein each discrete tissue sample comprises

a tissue section comprising a width of about 1 mm to about 10 mm and a thickness of about 1 μm to about 50 μm; and

a hydrogel substrate attached to the tissue section,

wherein the hydrogel substrate of each tissue section does not contact other tissue sections.

2. The device of claim 1 , wherein each tissue section is a formalin-fixed and paraffin embedded (FFPE) tissue section.

3. The device of claim 1 , wherein each tissue section is a frozen tissue section.

4. The device of claim 1 , wherein a length, width, and/or diameter of each tissue section is about 4 mm to about 10 mm.

5. The device of claim 1 , wherein a thickness of each tissue section is about 1 μm to about 20 μm.

6. The device of claim 1 , wherein a thickness of each tissue section is less than 6 μm, 7 μm, 8 μm, 9 μm or 10 μm.

7. The device of claim 1 , wherein each tissue section comprises breast tissue, lung tissue, colon tissue, lymph tissue, kidney tissue, bone tissue, tonsil tissue, or brain tissue.

8. The device of claim 1 , wherein each tissue section bonds to the hydrogel substrate via a first bond having a first adhesion strength, and wherein the tissue section bonds to the solid support via a second bond having a second adhesion strength, wherein the second adhesion strength is greater than the first adhesion strength.

9. The device of claim 1 , wherein the hydrogel substrate comprises a compression modulus greater than about 100 kPa.

10. The device of claim 1 , wherein the hydrogel substrate comprises a compression modulus of about 5 kPa to about 30 kPa.

11. The device of claim 1 , wherein the hydrogel substrate comprises agarose, amylose, or amylopectin.

12. The device of claim 1 , wherein the hydrogel substrate comprises 2% to 5% agarose.

13. The device of claim 1 wherein the hydrogel substrate comprises 3% to 20% acrylamide.

14. The device of claim 1 , wherein the hydrogel substrate comprises poly(2-hydroxyethyl methacrylate) (PHEMA); 2-hydroxyethyl methacrylate (HEMA); polyethylene glycol methacrylate (PEGMA); a copolymer of methacrylic acid (MAA) and polyethylene glycol methacrylate (PEGMA); or poly(N-isopropyl acrylamide) (PNIPAM).

15. The device of claim 1 , wherein the hydrogel substrate comprises poly(hydroxyethyl methacrylate) (PHEMA), poly(glyceryl methacrylate) (PGMA), poly(hydroxypropyl methacrylate) (PHPMA), polyacrylamide (PAM), polymethacrylamide (PMAM), polyvinyl alcohol (PVA), polyacrylic acid (PAA), polyvinyl pyrrolidone (PVP), poly(ε-caprolactone) (PCL), poly(ethyleneimine) (PEI), poly(N,N-dimethylacrylamide) (PDMAM), poly(2-methoxyethyl acrylate) (PMEA), or a copolymer thereof.

16. The device of claim 1 , wherein the solid support is glass.

17. The device of claim 16 , wherein the solid support comprises collagen type I, fibronectin, laminin, or poly-lysine.

18. The device of claim 16 , wherein the solid support comprises (3-aminopropyl)triethoxysilane (APTES), (3-Aminopropyl)trimethoxysilane (APTMS), γ-Aminopropylsilatrane (APS), N-(6-aminohexyl)aminomethyltriethoxysilane (AHAMTES), polyethylenimine (PEI), 5,6-epoxyhexyltriethoxysilane, or triethoxysilylbutyraldehyde, or a combination thereof.

19. The device of claim 1 , further comprising a fluorescent particle between the solid support and each tissue section.

20. The device of claim 1 , wherein the solid support comprises 2, 4, 6, 12, 24, 48, or 96 discrete tissue samples.

21. The device of claim 1 , wherein each discrete tissue sample is separated by an interstitial region.

22. The device of claim 1 , wherein each discrete tissue sample is separated from each other by at least 1 mm.

23. The device of claim 1 , wherein each discrete tissue sample is separated from each other by about 1 mm to about 10 mm.

24. A device comprising:

a solid support comprising a plurality of discrete tissue portions attached to the solid support at a first adhesion strength, wherein each tissue portion comprises a tissue section comprising a thickness of about 1 μm to about 50 μm and a polymer substrate bound to the tissue section at a second adhesion strength, wherein the first adhesion strength is greater than the second adhesion strength and wherein each polymer substrate does not contact other tissue sections.

Assignments (2)
SECURITY INTEREST Recorded Mar 7, 2025
From: SINGULAR GENOMICS SYSTEMS, INC.
To: FIRST-CITIZENS BANK & TRUST COMPANY
Reel/Frame 070440/0465 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 20, 2024
From: KOH, JAEKYUNG; CANG, HU; DEMPSEY, WILLIAM; ISHITSUKA, YUJI; VARNOSFADERANI, MOHAMMAD VATANKHAH; GLEZER, ELI N.; HONG, ZHENMIN; DING, WEIQIAO
To: SINGULAR GENOMICS SYSTEMS, INC.
Reel/Frame 067469/0580 →
Continuity (6)
Continuation PCTUS2022078462 · Oct 20, 2022
Provisional Application 63350854 · Jun 9, 2022
Provisional Application 63350858 · Jun 9, 2022
Provisional Application 63297077 · Jan 6, 2022
Provisional Application 63271456 · Oct 25, 2021
Related Publication 20240280446A1 · Aug 22, 2024
Cited By (2)
US 12,298,211 US 12,669,416