RECOVERABLE IMPREGNATION SEALANT
A sealant for use in vacuum pressure impregnation, wherein the sealant includes at least one monomer that is at least partially hydrophilic, at least one monomer that is at least partially hydrophobic, and wherein the sealant has a density less than the density of water.
1 . A liquid sealant for use in vacuum pressure impregnation, wherein the sealant includes at least one monomer that is at least partially hydrophilic, at least one monomer that is at least partially hydrophobic, and wherein the sealant has a density less than the density of water.
2 . The liquid sealant of claim 1 that includes C 12 -C 14 alkyl methacrylate (LMA) as a partially hydrophobic monomer.
3 . The liquid sealant of claim 1 that includes 1, 12-dodecane diol dimethacrylate (C 12 DMA) as a partially hydrophobic monomer.
4 . The liquid sealant of claim 2 , wherein the LMA has a density of 0.87 of the density of water.
5 . The liquid sealant of claim 3 , wherein the C 12 DMA has a density of 0.95 of the density of water.
6 . The liquid sealant of claim 1 that includes trimethylolpropane trimethacrylate (TMPTMA) as a partially hydrophilic monomer.
7 . The liquid sealant of claim 6 , wherein the TMPTMA has a water solubility of 0.01 g/l.
8 . The liquid sealant of claim 1 that includes triethyleneglycol dimethacrylate (TEGDMA) as a partially hydrophilic monomer.
9 . The liquid sealant of claim 8 , wherein the TEGDMA has a water solubility of 3.5 g/l.
10 . The liquid sealant of claim 1 that includes diethyleneglycol dimethacrylate (DEGDMA) as a partially hydrophilic monomer.
11 . The liquid sealant of claim 10 , wherein the DEGDMA has a water solubility of 0.58 g/l.
12 . The liquid sealant of claim 1 that includes bisphenol A ethoxylated dimethacrylate as a partially hydrophilic monomer.
13 . The liquid sealant of claim 12 , wherein the bisphenol A ethoxylated dimethacrylate has a very low solubility in water.
14 . The liquid sealant of claim 1 that includes bis [2-(meth acryloyloxy) ethyl] phosphate as a hydrophilic monomer and adhesion promoter.
15 . The liquid sealant of claim 14 , wherein the bis [2-(meth acryloyloxy) ethyl] phosphate is soluble in water.
16 . The liquid sealant of claim 1 that has a viscosity of 6.5-12.0 cps at 23° C.
17 . The liquid sealant of claim 1 that has a density of 0.930-0.955 g/cm 3 .
18 . The liquid sealant of claim 1 that a hardness of 60-75 Shore D when cured.
19 . The liquid sealant of claim 1 that has a density of 1.02-1.05 g/cm 3 .
20 . The liquid sealant of claim 1 that is formulated such that 98% or more of the sealant floats to the surface of water at 23° C. within 2 hours after the sealant is dispersed in water at 23° C.
21 . The liquid sealant of claim 1 that can be recycled and reused up to five times while maintaining sufficient curing properties for a part in which the liquid sealant is impregnated.
22 . The liquid sealant of claim 1 , wherein after being dispersed in water at 23° C., 0.5% or less by weight of the sealant remains dispersed in the water at 23° C. after 5 minutes.
23 . The liquid sealant of claim 1 that includes a radical initiator.
24 . The liquid sealant of claim 1 that is configured to cure in 10 minutes or less after being impregnated in a part and the part is then placed in hot water or steam at 80° C.-100° C.
25 . The liquid sealant of claim 1 that has a viscosity from 5.0-15.0 cps at 23° C.
26 . The liquid sealant of claim 1 that has a gel time of from 2.5 minutes to 4.0 minutes in a 90° C. water bath.
27 . A part impregnated with the liquid sealant of claim 1 , wherein the part is comprised of metal or graphite.
28 . The part of claim 24 that is cured in 10 minutes or less when immersed in water at 80° C.-100° C.