APPARATUS AND METHOD FOR GROWTH OF GADOLINIUM GALLIUM GARNET CRYSTAL
A gadolinium gallium garnet single crystal and method of forming said crystal is disclosed. The single gadolinium gallium garnet crystal can have a diameter of greater than 102 mm and a density of dislocations of less than 1 cm −2 in a central 80% of the crystal.
1 . A gadolinium gallium garnet single crystal, comprising:
a single gadolinium gallium garnet crystal having a diameter greater than 102 mm and a density of dislocations of less than 1 cm −2 in a central 80% of the crystal.
2 . The gadolinium gallium garnet crystal of claim 1 , wherein the diameter of the gadolinium gallium garnet based single crystal is greater than 105 mm.
3 . The gadolinium gallium garnet crystal of claim 1 , wherein the diameter of the gadolinium gallium garnet based single crystal is greater than 115 mm.
4 . The gadolinium gallium garnet crystal of claim 1 , wherein the diameter of the gadolinium gallium garnet based single crystal is greater than 120 mm.
5 . The gadolinium gallium garnet crystal of claim 1 , wherein the diameter of the gadolinium gallium garnet based single crystal is greater than 150 mm.
6 . The gadolinium gallium garnet crystal of claim 1 , wherein the diameter of the gadolinium gallium garnet based single crystal is not greater than 1000 mm.
7 . The gadolinium gallium garnet crystal of claim 1 , wherein the gadolinium gallium garnet crystal has a density of dislocation of less than 0.5 dislocation/cm −2 in the central 80% of the crystal.
8 . A method of growing a gadolinium gallium garnet crystal, comprising:
bringing a seed crystal in contact with a gadolinium gallium garnet base melt;
pulling the seed crystal to grow the gadolinium gallium garnet based single crystal; and
cooling the gadolinium gallium garnet based single crystal after it has reached a diameter that is greater than 102 mm, wherein the gadolinium gallium garnet based single crystal has a density of dislocations of less than 1 cm −2 in a central 80% of the crystal.
9 . The method of claim 8 , wherein the diameter of the gadolinium gallium garnet based single crystal is greater than 105 mm.
10 . The method of claim 8 , wherein the diameter of the gadolinium gallium garnet based single crystal is greater than 115 mm.
11 . The method of claim 8 , wherein the diameter of the gadolinium gallium garnet based single crystal is greater than 120 mm.
12 . The method of claim 8 , wherein the diameter of the gadolinium gallium garnet based single crystal is greater than 150 mm.
13 . The method of claim 8 , wherein the diameter of the gadolinium gallium garnet based single crystal is not greater than 1000 mm.
14 . The method of claim 8 , wherein the crystal was grown using a Czochralski method.
15 . The method of claim 8 , wherein cooling is carried out at a rate not greater than about 300° C./hr.
16 . The method of claim 8 , wherein cooling is carried out at a rate not greater than about 200° C./hr.
17 . The method of claim 8 , wherein cooling is carried out at a rate not greater than about 150° C./hr.
18 . The method of claim 8 , wherein cooling is carried out at a rate not greater than about 100° C./hr.
19 . The method of claim 8 , wherein cooling is carried out at a rate not greater than about 50° C./hr.
20 . The method of claim 8 , wherein the gadolinium gallium garnet base melt is within a crucible, wherein the crucible comprises iridium.