Method for producing soft magnetic powdered core
View Patent ↗A method for producing a soft magnetic powdered core comprises a mixing step for forming a raw powder by adding a thermoplastic resin powder to a soft magnetic powder and mixing them, a compacting step for forming a compact by compacting the raw powder into a predetermined shape, a melting and setting step for the resin in which the resin of the compact is melted by heating to at least the melting point of the thermoplastic resin and the melted resin is set by cooling to a room temperature, and a crystallizing step for the resin in which the set resin is heated to not less than the exothermic onset temperature and not more than the endothermic onset temperature, which are measured by DSC analysis of the thermoplastic resin, and is cooled to a room temperature.
1. A method for producing a soft magnetic powdered core, comprising:
a mixing step for forming a raw powder by adding 0.005 to 1 vol. % of a thermoplastic resin powder having a median size of not more than 50 μm to a soft magnetic powder coated with an electrical insulating film on a surface thereof; the thermoplastic resin powder comprised of a thermoplastic resin; and mixing the thermoplastic resin powder and the soft magnetic powder together;
a compacting step for forming a compact by compacting the raw powder into a predetermined shape;
a melting and setting step for the thermoplastic resin in which the thermoplastic resin of the compact is melted by heating the compact in one of a nitrogen gas atmosphere and an inert gas atmosphere to at least a melting point of the thermoplastic resin; and setting the melted thermoplastic resin by cooling the melted thermoplastic resin to room temperature; and
a recrystallizing step for the thermoplastic resin in which the set thermoplastic resin is heated in an air atmosphere to a temperature range not less than an exothermic onset temperature measured by differential scanning calorimetry (DSC) analysis of the thermoplastic resin and to a temperature range not more than an endothermic onset temperature measured by DSC analysis of the thermoplastic resin, and cooling the set resin to room temperature.
2. The method for producing a soft magnetic powdered core according to claim 1 ,
wherein the recrystallizing step for the thermoplastic resin is performed in a temperature range of not less than an exothermic peak temperature measured by DSC analysis of the thermoplastic resin and not more than an exothermic end temperature measured by DSC analysis of the thermoplastic resin, or in a temperature range of ±10° C. of the exothermic peak temperature measured by DSC analysis of the thermoplastic resin.
3. A method for producing a soft magnetic powdered core, comprising:
a mixing step for forming a raw powder by adding 0.005 to 1 vol. % of a thermoplastic resin powder having a median size of not more than 50 μm to a soft magnetic powder coated with an electrical insulating film on a surface thereof; the thermoplastic resin powder comprised of a thermoplastic resin; and mixing the thermoplastic resin powder and the soft magnetic powder together;
a compacting step for forming a compact by compacting the raw powder into a predetermined shape; and
a melting and setting step for the thermoplastic resin in which the thermoplastic resin of the compact is melted by heating the compact in one of a nitrogen gas atmosphere and an inert gas atmosphere to at least a melting point of the thermoplastic resin; and the compact is maintained in a temperature range of not more than an exothermic onset temperature measured by differential scanning calorimetry (DSC) analysis of the thermoplastic resin and not less than an exothermic end temperature measured by DSC analysis of the thermoplastic resin, and a set thermoplastic resin is cooled to room temperature in an air atmosphere.
4. A method for producing a soft magnetic powdered core, comprising:
a mixing step for forming a raw powder by adding 0.005 to 1 vol. % of a thermoplastic resin powder having a median size of not more than 50 μm to a soft magnetic powder coated with an electrical insulating film on a surface thereof; the thermoplastic resin powder comprised of a thermoplastic resin; and mixing the thermoplastic resin powder and the soft magnetic powder together;
a compacting step for forming a compact by compacting the raw powder into a predetermined shape; and
a crystallizing step for the thermoplastic resin in which the compact is heated in an air atmosphere to a temperature range not less than an exothermic onset temperature measured by differential scanning calorimetry (DSC) analysis of the thermoplastic resin and not more than an endothermic onset temperature measured by DSC analysis of the thermoplastic resin, and is cooled to room temperature.