Method of improving flowability of adipic acid
View Patent ↗A method of improving flowability of adipic acid includes adding to the adipic acid at a relatively low temperature a flowability improving agent, such as an acyclic saturated monobasic acid containing 10 to 22 carbon atoms or an acyclic saturated dibasic acid containing 10 to 14 carbon atoms.
1. A method of improving flowability of adipic acid comprising adding to the adipic acid downstream of a dryer used in a process for making said adipic acid and at a temperature of about 20 to about 35° C., an agent that improves flowability of the adipic acid, which agent is an acyclic saturated monobasic acid containing 10 to 22 carbon atoms or an acyclic saturated dibasic acid containing 10 to 14 carbon atoms wherein the agent is added as a dry powder.
2. A method of claim 1 , wherein said flowability improving agent is decanoic acid, undecanoic acid, lauric acid, tridecanoic acid, myristic acid, pentadecylic acid, palmitic acid, margaric acid, stearic acid, nonyldecanoic acid, arachic acid, behenic acid, decanedioic acid, undecanedioic acid, dodecanedioic acid, tetradecanedioic acid or a mixture thereof.
3. A method of claim 1 , wherein said flowability improving agent is 1,12-dodecanedioic acid.
4. A method of claim 1 , wherein said flowability improving agent is added in the vicinity of the exit of a dryer used in a process for making the adipic acid.
5. A method of claim 4 , wherein said flowability improving agent is added at the exit of the dryer.
6. A method of claim 1 , wherein said flowability improving agent is added to a conveyor downstream of a dryer used in a process for making the adipic acid.
7. A method of claim 1 , wherein said conveyor is a screw conveyor.
8. A method of claim 1 , wherein the adipic acid is pure adipic acid.
9. A method of claim 1 , wherein about 50 ppm to about 600 ppm of said flowability improving agent is added to the adipic acid, based on the adipic acid.