IP Library Granted Patent US 8,080,071
Granted Patent B1
US 8,080,071 · App. 12/394,356 · Granted Dec 20, 2011

Polycrystalline diamond compact, methods of fabricating same, and applications therefor

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Quick Facts
Patent No.
US 8,080,071
App. No.
12/394,356
Granted
Dec 20, 2011
Kind
B1
Abstract

Embodiments of the invention relate to polycrystalline diamond compacts (“PDCs”) comprising a polycrystalline diamond (“PCD”) table including a catalyst material therein that has been implanted with ions (e.g., carbon ions) and/or infiltrated from a host material implanted with carbon ions. In an embodiment, a PDC comprises a substrate and a PCD table bonded to the substrate. The PCD table includes a plurality of bonded diamond grains defining a plurality of interstitial regions. The PCD table includes an upper surface from which a region inwardly extends. At least a portion of the interstitial regions of the region includes a catalyst material disposed therein. At least a portion of the catalyst material may be at least saturated with carbon.

Claims (26)

1. A method of fabricating a polycrystalline diamond compact, comprising:

implanting carbon ions into a cementing constituent of a region of a substrate; infiltrating a plurality of diamond particles with the implanted cementing constituents from the substrate; and

sintering the plurality of diamond particles in the presence of the infiltrated and implanted cementing constituent to form a polycrystalline diamond table.

2. The method of claim 1 wherein implanting carbon ions into a cementing constituent of a region of a substrate comprises implanting a dose of the carbon ions into the cementing constituent exhibiting a concentration of about 10 15 ions per cm 2 to about 10 18 ions per cm 2 .

3. The method of claim 1 wherein the substrate comprises a cemented carbide substrate including the cementing constituent therein.

4. The method of claim 1 wherein the substrate comprises titanium carbide, niobium carbide, tantalum carbide, vanadium carbide, tungsten carbide, or combinations thereof cemented with the cementing constituent, and wherein the cementing constituent comprises iron, nickel, cobalt, or alloys thereof.

5. The method of claim 1 wherein the substrate comprises an interfacial surface, and the region of the substrate extends inwardly from the interfacial surface to a depth of about 1 nm to about 1500 nm.

6. The method of claim 5 wherein the depth is about 300 nm to about 800 nm.

7. The method of claim 1 wherein implanting carbon ions into a cementing constituent of a region of a substrate comprises at least saturating the cementing constituent of the region of the substrate with the carbon ions.

8. The method of claim 1 wherein implanting carbon ions into a cementing constituent of a region of a substrate comprises supersaturating the cementing constituent of the region of the substrate with the carbon ions.

9. The method of claim 1 wherein at least a portion of the cementing constituent of the region of the substrate implanted with the carbon ions comprises carbon fibrules.

10. The method of claim 1 wherein sintering the plurality of diamond particles in the presence of the infiltrated and implanted cementing constituent to form a polycrystalline diamond table comprises subjecting the substrate and the plurality of diamond particles to a high-pressure/high-temperature process under diamond-stable conditions.

11. The method of claim 1 , further comprising implanting carbon ions into the infiltrated cementing constituent of the polycrystalline diamond table.

12. A method of fabricating a polycrystalline diamond compact, comprising:

implanting carbon ions into a cementing constituent of a region of a cemented carbide substrate;

positioning an at least partially leached polycrystalline diamond table adjacent to the region of the cemented carbide substrate implanted with the carbon ions to form an assembly;

subjecting the assembly to a high-pressure/high-temperature process; and

at least partially infiltrating the at least partially leached polycrystalline diamond table with at least some of the cementing constituent from the region of the cemented carbide substrate, in response to the high-pressure/high-temperature process, to form an at least partially infiltrated polycrystalline diamond table.

13. The method of claim 12 , further comprising at least partially removing the at least some of the cementing constituent present in the at least partially infiltrated polycrystalline diamond table.

14. The method of claim 12 , further comprising implanting carbon ions into the infiltrated cementing constituent.

15. The method of claim 12 wherein the cemented carbide substrate comprise titanium carbide, niobium carbide, tantalum carbide, vanadium carbide, tungsten carbide, or combination thereof cemented with the cementing constituent, and wherein the cementing constituent comprises iron, nickel, cobalt, or alloys thereof.

16. The method of claim 12 , wherein the cemented carbide substrate comprises an interfacial surface, and the region of the cemented carbide substrate extends inwardly from the interfacial surface to a depth of about 1 nm to about 1500 nm.

17. The method of claim 16 wherein the depth is about 300 nm to about 800 nm.

18. The method of claim 12 wherein implanting carbon ions into a cementing constituent of a region of a cemented carbide substrate comprises at least saturating the cementing constituent of the region of the cemented carbide substrate with the carbon ions.

19. The method of claim 12 wherein implanting carbon ions into a cementing constituent of a region of a cemented carbide substrate comprises supersaturating the cementing constituent of the region of the cemented carbide substrate with the carbon ions.

20. The method of claim 12 wherein at least a portion of the cementing constituent of the region of the cemented carbide substrate implanted with the carbon ions comprises carbon fibrules.

Assignments (6)
SECURITY INTEREST Recorded Jul 18, 2025
From: US SYNTHETIC CORPORATION
To: KEYBANK NATIONAL ASSOCIATION
Reel/Frame 074973/0089 →
RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jul 17, 2025
From: JPMORGAN CHASE BANK, N.A.
To: CHAMPIONX LLC; APERGY ESP SYSTEMS, LLC; APERGY BMCS ACQUISITION CORP; HARBISON-FISCHER, INC.; NORRIS RODS, INC.,; NORRIS RODS, INC.,; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; US SYNTHETIC CORPORATION
Reel/Frame 072004/0019 →
RELEASE OF SECURITY INTEREST Recorded Jun 7, 2022
From: BANK OF AMERICA, N.A.
To: ACE DOWNHOLE, LLC; HARBISON-FISCHER, INC.; NORRIS RODS, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; THETA OILFIELD SERVICES, INC.; APERGY BMCS ACQUISITION CORP.; NORRISEAL-WELLMARK, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
Reel/Frame 060305/0001 →
SECURITY INTEREST Recorded Jun 5, 2020
From: ACE DOWNHOLE, LLC; APERGY BMCS ACQUISITION CORP.; HARBISON-FISCHER, INC.; NORRIS RODS, INC.; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; THETA OILFIELD SERVICES, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
To: BANK OF AMERICA, N.A.
Reel/Frame 053790/0001 →
SECURITY AGREEMENT Recorded May 9, 2018
From: APERGY (DELAWARE) FORMATION, INC.; APERGY BMCS ACQUISITION CORP.; APERGY ENERGY AUTOMATION, LLC; HARBISON-FISCHER, INC.; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 046117/0015 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 27, 2009
From: VAIL, MICHAEL A.
To: US SYNTHETIC CORPORATION
Reel/Frame 022323/0074 →